High-strength and high-conductivity CuAg alloy material and preparation method thereof
A high-strength, high-conductivity technology, applied in the direction of metal/alloy conductors, semiconductor devices, semiconductor/solid-state device components, etc.
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Embodiment 1
[0025] (1) The design of the chemical composition: copper and silver with a purity greater than 99.95% are used as raw materials, and CuAg6 is prepared by Ag 6wt% and the balance is copper.
[0026] (2) The smelting chamber and the directional solidification chamber are evacuated to a degree of 1 Pa, and then filled with argon for protection, and the air pressure is 0.04 MPa. The preheating temperature of the graphite crucible is 1100°C.
[0027] (4) Alloy melting. The alloy is melted in a vacuum induction furnace, heated and refined to make it fully alloyed, the temperature is controlled at 1200°C-1250°C, kept for 2 minutes, and poured into a graphite crucible through a funnel at a uniform speed.
[0028] (5) Pull down the graphite crucible. After all the metal is poured into the crucible, start the pull-down device to move the graphite crucible down at a constant speed, and the pull-down speed is 500 μm / S. After the temperature of the directional solidification chamber dr...
Embodiment 2
[0033] (1) Design of chemical composition: adopt copper and silver with a purity greater than 99.95% as raw materials, prepare CuAg9 by Ag 9wt%, and the balance is copper.
[0034] (2) The smelting chamber and the directional solidification chamber are evacuated to a vacuum degree of 1 Pa, and then filled with argon for protection, and the air pressure is 0.05 MPa. The preheating temperature of the graphite crucible is 1080°C.
[0035] (3) Alloy melting. The alloy is melted in a vacuum induction furnace, heated and refined to make it fully alloyed, the temperature is controlled at 1170°C-1220°C, kept for 2 minutes, and poured into a graphite crucible through a funnel at a uniform speed.
[0036] (4) Pull down the graphite crucible. After all the metal is poured into the crucible, start the pull-down device to move the graphite crucible down at a constant speed, and the pull-down speed is 300 μm / S. After the temperature of the directional solidification chamber drops below 1...
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