The invention discloses a technological method and device for semi-
coke production
wastewater resource utilization. The technological method comprises three steps, namely deep oil-water separation, high-efficiency complexing extraction dephenolization and
ammonia stilling, to be specific, firstly, separating and recycling a part of
coal tar from
wastewater when the
wastewater passes through an oil partitioning tank, recycling
coal tar in a precision filter and an oil-water separator in sequence after discharged water passes through a coarse filter; feeding the oil-removed semi-
coke wastewater and an extraction agent into an extraction
tower for extraction and dephenolization, feeding the extract phase and a
sodium hydroxide solution into a reverse extraction
tower for countercurrent contact reverse extraction, feeding an obtained
sodium phenolate solution into an acidification kettle, and adding
sulfuric acid for acidification to obtain crude
phenol; feeding dephenolized wastewater discharged from the bottom of the extraction
tower into a wastewater heater, feeding into an
ammonia cyanogen separator to be mixed with hot air from an
air heater to remove
ammonia after being heated by fume from the
air heater, and feeding an ammonia-containing
mixed gas discharged from the top of the ammonia-
cyanogen separator into an ammonia
water cooler for cooling to obtain ammonia water. By adopting the method and the device, precious resources such as
coal tar,
phenol and ammonia can be recycled from the semi-
coke production wastewater resource, and the biodegradability of the semi-
coke wastewater is improved.