The present invention relates to the technical field of chemical analysis, and discloses a chemical analysis test method for rapid determination of high content
manganese in aluminum
alloy. The chemical analysis test method comprises the following steps of 1, weighing: weighing 0.2000-0.2500 g of an
alloy sample in a 300 mL conical flask, adding 15 mL of
phosphoric acid and 5 mL of
nitric acid, completely decomposing the sample on a high temperature electric furnace, and taking down the sample when no large bubble exists on the liquid surface and white
smoke is generated, 2, oxidizing, adding 1 mL of
perchloric acid, continuously placing on the electric furnace, heating and dissolving, and heating until the liquid level is completely calm, and 3, cooling, taking down, cooling to 60-70 DEG C, adding
sulfuric acid, diluting with water to 70-80 mL, and fully shaking to dissolve the
viscous material. The method is short in detection time, accurate in detection result, low in cost, simple to operate, few in interference elements and suitable for rapid analysis of the stokehole, the used equipment is simple, the cost is low, and rapid and accurate analysis and detection of high-content
manganese in the aluminum
alloy are met.