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54results about How to "Analysis and detection are accurate" patented technology

Method, device and equipment for text detection and analysis based on depth neural network

The invention discloses a text detection and analysis method, a device and equipment based on a depth neural network, belonging to the technical field of depth learning and image processing. The method comprises the following steps of: performing template labeling to generate labeling template information; using the preset depth neural network detection model to detect and classify the text regionof the image to be detected, and generating the text region information with categories; template matching being performed according to the label template information and the text area information with categories to generate structured information data. The invention can realize fast and accurate detection and analysis according to various fields in a bill image, has the characteristics of real-time, accuracy, universality, robustness and expandability for the detection and analysis of a document image, and can be widely applied to the field of image text detection, analysis and recognition containing a plurality of texts.
Owner:ZHONGAN INFORMATION TECH SERVICES CO LTD

Smoke gas on-line monitoring system and smoke gas on-line monitoring method

The invention relates to a smoke gas on-line monitoring system and a smoke gas on-line monitoring method, and aims at providing the smoke gas monitoring system and the monitoring method which have the advantages of being simple in structure, high in automation degree and accurate in monitoring. The system comprises a pitot pitometer, a smoke gas sampler, a particulate matter monitor, sampling pipelines and demarcating pipelines, wherein the pitot pitometer, the smoke gas sampler and the particulate matter monitor are all provided with anti-purging devices, signal receiving terminals of all the anti-purging devices are respectively connected with a central controller, and all the anti-purging devices are controlled by the central controller to regularly purge. Smoke gas collected by the smoke gas sampler successively passes through a first refrigerator, a gas filter, a second refrigerator and a membrane type filter, the collected smoke gas is cooled and filtered by the first refrigerator, the gas filter, the second refrigerator and the membrane type filter, and the rest smoke gas finally obtained is fed into a multicomponent gas analysis instrument to be analyzed and detected. For the system, whole calibrated pipelines and partial calibrated pipelines are also arranged, so that the analysis instrument in a line can be wholly calibrated and partially calibrated.
Owner:汇众翔环保科技股份有限公司

Blood preservation agent for protecting free DNA and application of blood preservation agent

The invention belongs to preservation agents of blood samples and in particular relates to a blood preservation agent for protecting free DNA. Every 100ml of the preservation agent comprises the following components: 6.0-8.8g of an anticoagulant, 0.1-2.0g of a natural preservative, 4.8-11.7g of a DNA enzyme inhibitor, 5.0-10.0g of glucose, 5.0-8.0g of an antihemolytic agent, 0.1-0.5g of purine and the balance of buffer solution, totaling 100ml. The preservation agent disclosed by the invention can achieve the effects of effectively preventing blood cells from rupturing to release genome DNA so as to cause pollution, preventing degradation of free DNA in the plasma and providing a stable environment for the free DNA in the plasma. Moreover, the preservation agent is safe and non-toxic to the human body and environment and is favorable for accurate detection and analysis of the free DNA.
Owner:广州奇辉生物科技有限公司

On-line coal quality laser detection and analysis system

The invention relates to an on-line coal quality laser detection and analysis system, which comprises an automatic coal-sampling unit, a continuous coal sample-tableting unit and a coal laser detection and analysis unit that are connected in sequence through cables, a conveyer belt and a manipulator; the conveyer belt connects the automatic coal-sampling unit with a pulverized coal sample bin of the continuous coal sample-tableting unit; the continuous coal sample-tableting unit comprises a sample-tableting disc, and a hydraulic head and a filling port are arranged on the top of the sample-tableting disc; a pulverized coal sample feed station and a filling station are arranged on the sample-tableting disc, and a pulverized coal tablet ejection station is arranged under the sample-tableting disc; the coal laser detection and analysis unit comprises a three-dimensional point location numerical control platform, a travelling unit is connected to the three-dimensional point location numerical control platform, and an optical focusing element, a pulsed laser and a laser detection and analysis instrument are arranged on the top of the three-dimensional point location numerical control platform. The on-line coal quality laser detection and analysis system can implement automatic sampling, automatic sample tableting and automatic laser detection and analysis in the process of coal transportation.
Owner:山东利普斯智慧能源科技有限公司

Flue gas online monitoring system and monitoring method

The invention relates to a smoke gas on-line monitoring system and a smoke gas on-line monitoring method, and aims at providing the smoke gas monitoring system and the monitoring method which have the advantages of being simple in structure, high in automation degree and accurate in monitoring. The system comprises a pitot pitometer, a smoke gas sampler, a particulate matter monitor, sampling pipelines and demarcating pipelines, wherein the pitot pitometer, the smoke gas sampler and the particulate matter monitor are all provided with anti-purging devices, signal receiving terminals of all the anti-purging devices are respectively connected with a central controller, and all the anti-purging devices are controlled by the central controller to regularly purge. Smoke gas collected by the smoke gas sampler successively passes through a first refrigerator, a gas filter, a second refrigerator and a membrane type filter, the collected smoke gas is cooled and filtered by the first refrigerator, the gas filter, the second refrigerator and the membrane type filter, and the rest smoke gas finally obtained is fed into a multicomponent gas analysis instrument to be analyzed and detected. For the system, whole calibrated pipelines and partial calibrated pipelines are also arranged, so that the analysis instrument in a line can be wholly calibrated and partially calibrated.
Owner:汇众翔环保科技股份有限公司

Tire cutter

The invention discloses a tire cutter, which comprises a frame, a clamp, a cutting cutter and a cutting driving device, wherein the clamp can be movably arranged on the side wall of the frame in a longitudinal direction and a transverse direction on the basis of a using direction; the cutting cutter is rotationally positioned at the lower end of the upper side wall of the frame in the circumferential direction; the cutting driving device can drive the cutting cutter to rotate; an axial end face of the cutting cutter is parallel to the transverse feeding direction of the clamp; and the clamp can fix a tire axially and radially. In the tire cutter, the cutting cutter is matched with the clamp which can move in the transverse direction and the longitudinal direction, so the axial section of the tire can be cut accurately and quickly; and the axial section is smooth and convenient to detect, so the detection and analysis of the tire are more accurate.
Owner:健伦精密机械(中国)有限公司

Indoor toilet environment intelligent control system

PendingCN111830876AAchieve real-time dynamic balance effectOptimal balanceProgramme controlMeasurement devicesComputer scienceEnvironmental data
The invention discloses anindoor toilet environment intelligent control system, which comprises a detection platform, an intelligent control platform, an execution platform, an alarm platform and a management platform, wherein the detection platform is various environmental data sensing detection equipment distributed in an indoor toilet; the execution platform is various environment data regulation and control equipmentdistributed in an indoor toilet; the intelligent control platform is used for carrying out self-checking processing on the collected environment data of the indoor toilet; thealarm platform is used for triggering to generate an alarm signal; and the management platform is used for receiving, querying and managing the environment data of the indoor toilet. According to theindoor toilet environment intelligent control system, a double self-checking mode is utilized, abnormal environment data existing in an indoor toilet can be comprehensively and accurately analyzed anddetected, the real-time dynamic balance effect of the indoor toilet environment is achieved through regulation and control operation of dynamic balance, and the indoor toilet environment is ensured to be in the optimal balance state.
Owner:白兴龙

Intelligent detection equipment and method for cement base material pore structure

The invention discloses an intelligent detection device and method for a cement base material pore structure. The device comprises a sample loading system, an image acquisition system and an image recognition and analysis system, the sample loading system is composed of a workbench, two longitudinal sliding tables, a transverse sliding table and a storage table, and the image acquisition system iscomposed of a vertical rod, two hoops, a microscopic support, a microscope, a camera, a universal frame support, a universal telescopic cantilever support and a light source; the image recognition and analysis system is composed of a display module, a storage module and a processing module. According to the present invention, the mutual cooperation among the components is utilized so as to conveniently sample the sample image, and the detection method uses the pore image intelligent identification system to carry out a series of processing on the image sample so as to obtain the parameters and analyze to obtain the pore characteristics. The intelligent detection device and method for the cement base material hole structure are reasonable in structural design, easy to operate, high in detection efficiency and capable of effectively reducing the detection cost.
Owner:南京白鲨测绘科技有限公司

Polycarbonate testing method

The invention discloses a polycarbonate testing method, which comprises the following steps that: A) testing the volatile ingredients of polycarbonate, and determining the amount of volatile ingredients in the polycarbonate; B) testing a PDI (Poly-Dispersity Index) and pH (Potential of Hydrogen), and carrying out the second step when the amount of the volatile ingredients is small than 10, the PDIis smaller than 2.8 and a pH value is 6.2-7.3; C) carrying out through-machine evaluation testing: when MI (Melt Index)% is less than 10% and an IMP level is A or B or C, carrying out the third step;D) carrying out poaching testing; E) carrying out thermo-oxidative aging testing: when a mechanical property retention rate after poaching aging testing is greater than or equal to 75% and a thermo-oxidative aging testing color change [Delta]E value is smaller than 3, carrying out the fourth step; F) carrying out damp-heat aging testing; and / or G) carrying out xenon lamp ageing testing. The invention aims to provide a simple polycarbonate detection process for enterprises, and whether polycarbonate conforms to the production requirements of production even special application occasions or not can be quickly and accurately detected and analyzed.
Owner:KINGFA SCI & TECH CO LTD +1

Method for analyzing and detecting trace metal ion impurities in dimethyl diallyl ammonium chloride monomers

The invention discloses a method for analyzing and detecting trace metal ion impurities in dimethyl diallyl ammonium chloride (DMDAAC) monomers. According to the method, an organic solvent chelating extraction-flame atomic absorption spectroscopy method is adopted to measure the contents of multiple trace metal ions in DMDAAC monomers of a DMDAAC monomer solution with a high salt content, and avoids the difficult operation and result errors caused by direct injection of a sample with a high salt content. By utilizing the synergistic effect of a complexing agent, three metal ions (Fe, Cu, and Ni) can be complexed, extracted, separated, analyzed, and tested at the same time. The provided method has the advantages that the operation is simple and convenient, the analysis precision is high, and the contents of several trace metal ion impurities in DMDAAC monomers can be accurately, rapidly, and reliably analyzed and detected. The provide method has an important scientific meaning and industrial practical value for industrial manufacturing of high purity DMDAAC monomers, establishment of national / international standards of DMDAAC monomers, and research on the activity of DMDAAC monomers in polymerization reactions.
Owner:NANJING UNIV OF SCI & TECH

Analysis system for methane and non-methane total hydrocarbons and analysis method thereof

The invention relates to an analysis system for methane and non-methane total hydrocarbons and an analysis method thereof. The analysis system comprises a multi-channel injection valve, a quantitativetube, an air suction pump, a high carbon adsorption unit, a low carbon separation unit and a hydrogen flame ionization detector; the analysis system forms a first state, a second state and a third state which are all switchable through the multi-channel injection valve. The analysis system can achieve the purpose of continuously and accurately analyzing and detecting the methane and non-methane total hydrocarbons completely without oxygen interference.
Owner:BEIJING SDL TECH

Method for separating and enriching trifluralin herbicide in soil

The invention discloses a method for separating and enriching a trifluralin herbicide in soil. The method comprises the steps: mixing isooctyl acrylate, divinylbenzene, Span80 and C7H8, and adding azodiisobutyronitrile to form an organic phase; adding acrylamide into a polyvinylpyrrolidone / graphene oxide aqueous solution, and then adding nano SiO2 to form an aqueous phase; adding the aqueous phaseto the organic phase to form a high internal phase emulsion; drying, thermopolymerizing and washing the high internal phase emulsion, and carbonizing for 2 hours at the temperature of 600 DEG C; drip-washing a carbonized monolithic column with an acetonitrile aqueous solution, eluating the trifluralin herbicide target enriched on the carbonized monolithic column by an acetic acid / acetonitrile solution, and collecting an eluate; and blowing the eluate to dry with liquid nitrogen, redissolving with acetonitrile to obtain a to-be-measured solution, and completing the separation and enrichment ofthe trifluralin herbicide in the soil sample. The method has good extraction and enrichment ability for the trifluralin herbicide, and can be applied to extraction, enrichment and separation analysisof the trace trifluralin herbicide in the soil sample.
Owner:GUILIN UNIVERSITY OF TECHNOLOGY

Medicinal application of epimedin C in treatment on diabetic liver injury

ActiveCN111494360ARelieve typical symptomsRaise HDL-C levelOrganic active ingredientsMetabolism disorderGlutamic-Pyruvic TransaminaseEpimedin C
The invention discloses a medicinal application of epimedin C in treatment on diabetic liver injury, and belongs to the technical field of biological medicines. The invention discloses that epimedin Ccan improve the cholesterol level of high-density lipoprotein in the liver of a diabetic model animal for the first time, the cholesterol level of low-density lipoprotein in the liver is reduced, theproblem of lipid metabolism disorder is relieved, a liver index is reduced, the activity of superoxide dismutase and glutathione peroxidase in the liver is enhanced, the content of malondialdehyde isreduced, the oxidative stress state of the liver is improved, normal forms and structures of hepatocytes and tissues are maintained, the activity levels of glutamic-pyruvic transaminase and glutamicoxalacetic transaminase in the liver are reduced, and liver function repair is promoted, so that the epimedin C can be used for preparing medicines for treating diabetic liver injury. The epimedin C is used for preparing the medicine for treating diabetic liver injury in the form of a medicinal preparation, and comprises buccal tablets, coated tablets and hard capsules. The invention provides a basis for treatment on diabetic liver injury, and also provides an idea for deep development and utilization of epimedium resources.
Owner:陕西新修本草健康产业有限公司

Moxa smoke enrichment device and moxa smoke enrichment analysis method

The invention provides a moxa smoke enrichment device. The moxa smoke enrichment device comprises a blower device, a moxa smoke bin and a moxa smoke absorption device which are sequentially connectedthrough a pipeline, wherein the blower device comprises an air inlet pump, and the air inlet pump is communicated with the moxa smoke bin; the moxa smoke bin is communicated with the moxa smoke absorption device; the moxa smoke absorption device comprises a first absorption device, a second absorption device, a third absorption device, a fourth absorption device and a fifth absorption device whichare sequentially connected through a pipeline; the moxa smoke absorption device is also connected with an air outlet pump; and a contamination device is further arranged in the moxa smoke bin. The invention further comprises a moxa smoke enrichment analysis method, which comprises the steps of carrying out GC-MS component analysis on moxa smoke absorbed by all solvents in the moxa smoke absorption device, utilizing a mass spectrum retrieval standard library NIST11.L, and calculating the relative percentage content of chemical components by using a peak area normalization method. The moxa smoke enrichment device provided by the invention not only enriches moxa smoke components, but also can carry out contamination experiments at the same time, and provides conditions for subsequent analysis of chemical components of moxa smoke and animal toxicology analysis.
Owner:JIANGXI UNIVERSITY OF TRADITIONAL CHINESE MEDICINE

Application of compound as blocking reagent for glycosyl on antibody

The invention relates to the detection of protein glycosyl, in particular to an application of a compound as a blocking reagent for glycosyl on an antibody. To solve the problem of the interference ofthe glycosyl of a current antibody on detection, a compound used as a blocking reagent for the glycosyl on the antibody is provided, and the compound is selected from one of alpha-semicarbazide, acetylhydrazine, sulfur acetohydrazide, thiosemicarbazide, asparagine hydrazide, tyrosine hydrazine, N (benzyloxycarbonyl)-L-valyl-L-tyrosine hydrazide, or N (benzyloxycarbonyl) glycinic hydrazide. The compound used as the blocking reagent for the glycosyl on the antibody has the advantages of being capable of conducting petreatment of antibodies, avoiding binding of plant lectins to antibodies, guaranteeing accurate quantification of the glycosyl on captured proteins, being simple in the process of blocking the antibodies with one step reaction needed, shortening the reaction process of existingblocked antibodies, and significantly reducing costs.
Owner:嵊州宝康医疗科技有限公司

Kit and use thereof

The invention discloses a kit. The kit comprises a probe, the probe is fixed on a solid matrix or is free in a solution, and the probe can specifically identify at least one part of regions in every gene of seventeen genes in table 1. The invention also provides a use of the kit, a method for constructing a target region sequencing library, a sequencing method, a method for detecting the variation of the target region, and a device for detecting the variation of the target region. The kit and / or the method or the device are / is used to once, simply, conveniently and highly-specifically obtain relevant gene sequences of stomach cancer and accurately detect and analyze the relevant gene sequences in order to make the detection and analysis result used for medication guidance and / or risk predication of the stomach cancer in an auxiliary manner.
Owner:BGI GUANGZHOU MEDICAL LAB CO LTD +1

Drug Application of Epimedin C in Treating Diabetic Liver Injury

The invention discloses the drug application of epimedin C for treating diabetic liver injury, and belongs to the technical field of biomedicine. The present invention discloses for the first time that epimedin C can increase the level of high-density lipoprotein cholesterol in the liver of diabetic model animals, reduce the level of low-density lipoprotein cholesterol in the liver, alleviate the problem of lipid metabolism disorder, reduce liver index, and enhance superoxide dismutase in the liver , Glutathione peroxidase activity, reduce malondialdehyde content, improve liver oxidative stress state, maintain normal shape and structure of liver cells and tissues, reduce liver alanine aminotransferase and aspartate aminotransferase activity levels, and promote liver function repair, Therefore, it can be used to prepare medicines for treating diabetic liver damage. Epimedin C prepares a medicine for treating diabetic liver damage and uses it in the form of pharmaceutical preparations, including buccal tablets, coated tablets and hard capsules. The invention provides a basis for the treatment of diabetic liver damage, and also provides ideas for the deep development and utilization of epimedium resources.
Owner:陕西新修本草健康产业有限公司

Chemical analysis test method for rapid determination of high content manganese in aluminum alloy

The present invention relates to the technical field of chemical analysis, and discloses a chemical analysis test method for rapid determination of high content manganese in aluminum alloy. The chemical analysis test method comprises the following steps of 1, weighing: weighing 0.2000-0.2500 g of an alloy sample in a 300 mL conical flask, adding 15 mL of phosphoric acid and 5 mL of nitric acid, completely decomposing the sample on a high temperature electric furnace, and taking down the sample when no large bubble exists on the liquid surface and white smoke is generated, 2, oxidizing, adding 1 mL of perchloric acid, continuously placing on the electric furnace, heating and dissolving, and heating until the liquid level is completely calm, and 3, cooling, taking down, cooling to 60-70 DEG C, adding sulfuric acid, diluting with water to 70-80 mL, and fully shaking to dissolve the viscous material. The method is short in detection time, accurate in detection result, low in cost, simple to operate, few in interference elements and suitable for rapid analysis of the stokehole, the used equipment is simple, the cost is low, and rapid and accurate analysis and detection of high-content manganese in the aluminum alloy are met.
Owner:NORTHWEST RES INST OF MINING & METALLURGY INST

Gas chromatography system and method for detecting detailed composition of automotive gasoline

The invention relates to a gas chromatography system and method for detecting detailed composition of vehicle gasoline. The system comprises a first detection channel and a second detection channel, the first detection channel comprises a first sample inlet, a first non-polar chromatographic column and a first detector; the first sample inlet is communicated with an inlet of the first non-polar chromatographic column, and an outlet of the first non-polar chromatographic column is communicated with an inlet of the first detector; the second detection channel comprises a second sample inlet, a second non-polar chromatographic column, a central cutting assembly, a third sub-channel and a fourth sub-channel; the third sub-channel comprises a damping column and a second detector which are communicated in sequence, and the fourth sub-channel comprises a polar chromatographic column and a third detector which are communicated in sequence. The system disclosed by the invention is compact in structure and can be used for measuring the detailed hydrocarbon composition and the content of added components of the automotive gasoline.
Owner:CHINA PETROLEUM & CHEM CORP +1

A Malicious Code Analysis and Detection Method Based on Dynamic Semantic Features

The invention relates to a malicious code analysis and detection method based on dynamic semantic features. The method comprises the steps that (1) codes to be analyzed and detected in a malicious sample library are dynamically operated in a virtual environment, the operation process of the codes to be analyzed and detected in the malicious sample library is monitored, and the primitive characters of the codes to be analyzed and detected in the malicious sample library are extracted; (2) API name information standing for the semantic features of the codes is screened out; (3) an API sequence semantic feature set standing for the semantic features of the codes is established; (4) a semantic feature library with representative semantic features is selected; (5) similarity detection is carried out between the semantic feature set of the codes to be detected and the semantic feature library to obtain a detection result, namely, whether the codes to be detected are benign codes or malicious codes is detected. According to the malicious code analysis and detection method based on the dynamic semantic features, different semantic features can be established according to different samples, good universality is achieved, a method for selecting representative features is proposed, the semantic features of the codes can be expressed accurately, the analysis and detection on the malicious codes are more accurate, and detection cost is low.
Owner:INST OF INFORMATION ENG CHINESE ACAD OF SCI

Detection method of trace metal ions in dimethyl diallyl ammonium chloride monomer

The invention discloses a method for analyzing and detecting trace metal ion impurities in dimethyl diallyl ammonium chloride (DMDAAC) monomers. According to the method, an organic solvent chelating extraction-flame atomic absorption spectroscopy method is adopted to measure the contents of multiple trace metal ions in DMDAAC monomers of a DMDAAC monomer solution with a high salt content, and avoids the difficult operation and result errors caused by direct injection of a sample with a high salt content. By utilizing the synergistic effect of a complexing agent, three metal ions (Fe, Cu, and Ni) can be complexed, extracted, separated, analyzed, and tested at the same time. The provided method has the advantages that the operation is simple and convenient, the analysis precision is high, and the contents of several trace metal ion impurities in DMDAAC monomers can be accurately, rapidly, and reliably analyzed and detected. The provide method has an important scientific meaning and industrial practical value for industrial manufacturing of high purity DMDAAC monomers, establishment of national / international standards of DMDAAC monomers, and research on the activity of DMDAAC monomers in polymerization reactions.
Owner:NANJING UNIV OF SCI & TECH

Analysis and detection method for micropore failure reasons of soft-pack lithium batteries

The invention relates to a method for analyzing and detecting the cause of micropore failure of a soft-packed lithium battery. The specific implementation steps of the method are as follows: first cut off the area containing micropores in the ALF aluminum-plastic film, soak it in the electrolyte, and then place the Store at a temperature of 10°C to 150°C for 1‑60 days; when the polypropylene (PP) layer, nylon layer and other materials in the ALF aluminum-plastic film are separated from the aluminum layer, take out the aluminum layer; then soak the Place the aluminum layer under a microscope to observe whether the micropores are deformed toward the nylon layer, that is, it is determined that it is caused by the foreign matter of the punch particles; or it is deformed toward the PP layer, that is, it is determined that it is affected by external forces during the manufacturing process; That is to say, it is determined that it is caused by the deformation and stretching of the shell, and then the cause of the micropores in the aluminum layer is determined, so as to adjust the lithium battery production process and change the adverse production environment and conditions. The method of the invention is reasonable in design, simple in operation, accurate in analysis and detection, high in reliability, low in cost, high in benefit, and has remarkable application effects.
Owner:TIANJIN JUYUAN NEW ENERGY TECH CO LTD

Analysis system and analysis method for methane and non-methane total hydrocarbons

The invention relates to an analysis system and analysis method of methane and non-methane total hydrocarbons. The analysis system includes: a multi-channel sampling valve, a quantitative tube, an air pump, a high-carbon adsorption unit, a low-carbon separation unit, and a hydrogen flame ionization detector. The analysis system forms a switchable first state through the multi-channel sampling valve, second state and third state. The analysis system can realize the purpose of continuous complete anaerobic interference accurate analysis and detection of methane and non-methane total hydrocarbons.
Owner:BEIJING SDL TECH

Common CT computer imaging omics stone component analysis system and method

The invention relates to the technical field of medical images, in particular to a common CT computer imaging omics stone component analysis system and method, and the system comprises a central processing system, a data collection unit, a data analysis module, printing equipment and a mobile phone terminal. The input end of the central processing system is unidirectionally and electrically connected with a system firewall, and the data collection unit is connected with the system firewall through a wireless network. Calculus components are analyzed through CT computer imaging omics and compared with data in a database, the defects of an existing calculus analysis method are overcome, and the calculus analysis method has the advantages that calculus can be detected and analyzed more accurately and effectively, data are prevented from being lost in the transmission process, and then detection errors can be reduced. The problem that at present, infrared spectrum detection analysis is mainly adopted for calculus component analysis, the infrared light absorption band characteristic of a calculus sample is not high enough, and certain errors exist in detection of some calculus components is solved.
Owner:澧县人民医院

Method for rapidly detecting 221 illegally added components in health food

The invention relates to a method for rapidly detecting 221 illegally added components in health food. The method comprises the following steps: (1) pretreatment of a detected object; (2) preparing 221 reference substance single standard stock solutions, and preparing a mixed standard working solution and a plurality of standard series solutions according to the concentration gradient; (4) establishing chromatographic separation conditions and mass spectrum conditions; establishing a first-level spectrum library; and establishing a secondary high-resolution mass spectrum database. The method has the beneficial effects that the ultra-high performance liquid chromatography-quadrupole-time-of-flight high-resolution mass spectrometry is used for establishing a method for detecting 221 illegally added chemical components in the health food, and a high-resolution mass spectrometry database of corresponding illegally added chemical substances is established. And compared with corresponding characteristic fragment ions in a high-resolution mass spectrum database, qualitative and quantitative risk screening and determination can be carried out on 221 illegally added chemical substances for health food supervision sampling inspection and risk monitoring. The method can be used for accurately analyzing and detecting illegal added components of the health care product in a more targeted, faster and more effective manner, so that the component detection and analysis are faster. The method is simple in process, high in detection precision and sensitive in detection.
Owner:天津市食品安全检测技术研究院

Method for simultaneously determining four effective components in Sihuangzhili Granules

The invention provides a method for simultaneously detecting four effective components in Sihuangzhili Granules, and belongs to the technical field of veterinary drug detection. According to the method, original standards and effective components of the Sihuangzhili Granules are taken as the basis; four effective components in the Sihuangzhili Granules are accurately analyzed and detected; the quality of the Sihuangzhili Granules can be further effectively controlled; the preparation quality is comprehensively evaluated; therefore, the stability of product quality and the safety and effectiveness of veterinary drugs are ensured to the greatest extent; the method has the advantages of strong specificity, high precision, good stability, high accuracy, simple operation, reagents and consumables cheap and easy to obtain, effective control of the production quality and the stability of the product, improvement of the quality and the market competitiveness of the product, and promotion and practical values in the pharmaceutical industry.
Owner:CHONGQING FANGTONG ANIMAL PHARMA

MALDI-TOF-MS based high-throughput analysis method for single-particle capsule drug

The invention discloses an MALDI-TOF-MS-based high-throughput analysis method for single-particle capsule drug. The method comprises the following steps: applying a sample of a drug main component standard substance solution on a target plate, drying, carrying out matrix sample application, and carrying out MALDI-TOF-MS analysis detection; adhering drug particles in a to-be-detected capsule to thetarget plate through a conductive double faced adhesive tape, and directly performing MALDI-TOF-MS analysis and detection; and identifying the authenticity of the to-be-detected capsule by comparingthe drug particles of the to-be-detected capsule with a MALDI-TOF-MS graph of the drug main component standard substance. When the MALDI-TOF-MS method is adopted for detecting the single-particle medicine, matrix is not used, pretreatment is not carried out, detection is directly carried out, use of an organic solvent is avoided to the maximum extent, and due to the fact that a complex pretreatment process is not needed, the analysis and detection time is greatly shortened.
Owner:SHANDONG ANALYSIS & TEST CENT
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