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80 results about "Small-angle scattering" patented technology

Small-angle scattering (SAS) is a scattering technique based on deflection of collimated radiation away from the straight trajectory after it interacts with structures that are much larger than the wavelength of the radiation. The deflection is small (0.1-10°) hence the name small-angle. SAS techniques can give information about the size, shape and orientation of structures in a sample.

Hot stage for small-angle scattering experiment

The present invention provides a hot stage for small-angle scattering experiment. The hot stage includes an intake passage, a sealed window, a translucent window, an exhaust passage, a heating layer package wall, a heating layer, a sample chamber and a sample clamp layer. The hot stage for small angle scattering experiment has thermal station temperature in the range of -40 to 1200 DEG C; and the connecting lines between two end ports of the sample chamber and the edges of the transparent window have included angle of 4- 90 DEG with the axial parallel of the sample chamber. Surrounding heating on the sample chamber by the heating layer ensures uniform heating of the sample, and avoids the effects of the heating layer on neutron and X-ray path. The sealed window and translucent window uses quartz glass, sapphire or Kapton film with high transmittance of neutrons and X-rays, so as to achieve high transmittance of neutrons and X-ray, and ensure normal operation of the neutron and X-ray small-angle scattering experiments.
Owner:INST OF NUCLEAR PHYSICS & CHEM CHINA ACADEMY OF

Negative active material for secondary battery, process for producing same, and negative electrode and lithium-ion battery both obtained using same

The present invention relates to: a negative active material for secondary batteries which comprises a silicon oxide-based composite material, attains a high battery capacity, and has excellent charge / discharge cycling characteristics; a process for producing the negative active material; and a negative electrode and a lithium-ion battery both obtained using the negative active material. The silicon oxide-based composite material has a new structure and is directly obtained by burning, in an inert gas atmosphere, a polysilsesquioxane having a specific structure. The yielded silicon oxide-based composite material has graphitic carbon and is represented by the general formula SiOxCy (0.5<x<1.8, 1<y<5). In an examination by the X-ray small-angle scattering method, the composite material gives a spectrum which shows scattering in the range of 0.02 Å-1<q<0.2 Å-1. In an examination by Raman spectroscopy, the composite material gives a spectrum which shows scattering at 1,590 cm-1 (G band; graphite structure) and at 1,325 cm-1 (D band; amorphous carbon), the peak intensity ratio of crystalline carbon and amorphous carbon (ID / IG ratio) being in the range of 2.0-5.0. The silicon oxide-based composite material is used as a negative active material to form a negative electrode therefrom, and the negative electrode is used to form a lithium-ion secondary battery.
Owner:JNC CORP +1

Sample reservoir for carrying out in-situ characterization on crystallization process of molecular sieve based catalyst, and use method thereof

A sample reservoir for carrying out in-situ characterization on crystallization process of a molecular sieve based catalyst comprises a reservoir body, a press ring, a sealing pad, a window piece, a reservoir cover, a fastening element, an inner core and a thermocouple component. The sample reservoir allows X rays to pass through and studies the crystallization process of the molecular sieve based catalysts in an in-situ online manner by using XAFS (x-ray absorption fine structure), XRD (X-ray diffraction), SAXS (small angle X-ray scattering), SAXS / WAXS (small angle X-ray scattering and wide angle X-ray scattering) under the conditions of 0-300 DEG C and 0-3 MPa. The change of the catalyst structure is monitored during the processes.
Owner:SHANXI INST OF COAL CHEM CHINESE ACAD OF SCI

Single-beam double-lens laser particle analyzer

The invention discloses a single-beam dual-lens laser particle size analyzer, which adopts an emanative laser beam as the light source and arranges two lenses before and after a sample pool; wherein, the lens after the sample pool simultaneously has two functions, one is to change the emanative laser beam into parallel light (secondary collimation), and the other is to receive the backward large-angle scattered light (aggregation). The lens before the sample pool is used to receive the forward scattered light. Photodetectors are respectively arranged on the focal planes of the two lenses to receive the forward and backward scattered signals, so that the forward and backward scattered light can be simultaneously received; the forward scattered light and the backward scattered light are respectively treated, and a small-angle scattered light and large-angle scattered light combined treatment technology is introduced, so that the test range of the laser particle size analyzer can reach 0.01-2000 micron. Through the effect of the unique design of the single-beam optical path reaching the multi-beam optical path, the invention is characterized by large test range, simple structure, small size, low cost and high measurement accuracy.
Owner:丹东百特科技有限公司

Asphaltene aggregation in petroleum oil mixtures determined by small angle light scattering

The present invention includes a method to determine if asphaltenes are soluble or insoluble in a solution. The solution may be a petroleum oil, a mixture of petroleum oils, petroleum derived oils and mixtures or similar combinations in a solvent. The invention includes the steps of illuminating the solution with a laser, measuring the small angle scattered light as a function of angle away from the laser beam, and determining if the asphaltenes are soluble or insoluble in the solution.
Owner:EXXON RES & ENG CO

Radiation imaging system and image processing device

A radiation imaging system includes a radiation imaging device, a reconstruction unit and a detection unit. The reconstruction unit generates at least two of a differential phase image, an absorption image and a small-angle scattering image based on periodic pattern images of a subject obtained by the imaging device. The detection unit performs regression analysis on at least two images of (a) the differential phase image, a differential absorption image of the absorption image and a differential small-angle scattering image of the small-angle scattering image or (b) a phase image of the differential phase image, the absorption image and the small-angle scattering image; calculates a value of an indicator indicating a relationship between the at least two images; and detects image quality deterioration due to change in relative position of the imaging device and the subject based on the value.
Owner:KONICA MINOLTA INC

Microstructure analysis method of asphalt and modifier thereof

The invention relates to a microstructure analysis method of asphalt and a modifier thereof, and belongs to the technical field of microstructure analysis of modified asphalt. The problem that the microstructures of asphalt and the modifier thereof cannot be comprehensively, stereoscopically and clearly analyzed by using only one characterization method at present is solved. According to the microstructure analysis method provided by the invention, neutron small-angle scattering samples of an SBS modifier, matrix asphalt and SBS modified asphalt are prepared at first, a neutron small-angle scattering test is performed on the samples to obtain initial experimental data, and the initial experimental data are processed to obtain an absolute intensity scattering curve, and then different models are fitted through the absolute intensity scattering curves of the samples to quantitatively analyze the microstructures of the SBS modifier, the matrix asphalt and the SBS modified asphalt. Throughthe analysis of the microstructures of the asphalt and the modifier thereof, the modification mechanism of the SBS modified asphalt can be better revealed, and a relationship between the microstructure of the modified asphalt and the macroscopic properties thereof can be established, so that the performance of the SBS modified asphalt, and the service level and the service life of asphalt pavements can be better improved.
Owner:NANJING FORESTRY UNIV

Carbonaceous electrode material for secondary battery

InactiveUS20020039686A1Efficient use ofLarge charge-discharge capacityConductive materialCarbon preparation/purificationX-raySolvent
A carbonaceous electrode having improved capacities for doping and dedoping of a cell active substance, such as lithium, and suitable for a non-aqueous solvent-type secondary battery, is constituted by a carbonaceous material obtained by carbonizing an aromatic condensation polymer formed by condensation of an aromatic compound having a phenolic hydroxy group and an aldehyde. The carbonaceous material is characterized by an atomic ratio H / C between hydrogen atoms and carbon atoms of below 0.1, a carbon dioxide adsorption capacity of at least 10 ml / g, and an X-ray scattering intensity ratio IW / ID of at least 0.25, wherein IW and ID represent scattering intensities as measured in a wet state and a dry state, respectively, at a parameter s=2.sin theta / lambd of 0.5 nm-1, wherein theta denotes a scattering angle and lambd denotes a wavelength of X-rays in X-ray small-angle scattering measurement.
Owner:KUREHA KAGAKU KOGYO KK

Method for removing blurring effect in X-ray scattering and diffraction experiments

The invention discloses a method for removing blurring effect in X-ray scattering and diffraction experiments. The method comprises the steps of measuring the distribution of straight spots on a two-dimensional detector to obtain h (x, y), measuring the scattering data of an experimental sample to obtain g (x, y), performing Fourier transform on h (x, y) and g (x, y), respectively, thereby obtaining the distribution H (u, v) of the straight spots in the reciprocal space and the distribution G (u, v) of the scattering data in the reciprocal space, performing deconvolution processing on the experimental data H (u, v) and G (u, v) by use of a Wiener filtering algorithm to obtain the Fourier transform F (u, v) of blurring effect-removed data f (x, y), performing inverse fast Fourier transform on F (u, v) to obtain the blurring effect-removed data f (x, y), and adjusting the parameter alpha according to the results of f (x, y) until the desired deconvolution result is obtained. The method for removing the blurring effect in the X-ray scattering and diffraction experiments is used for performing the deconvolution processing on the experimental data. Due to the adoption of the method, the angle resolution of the X-ray small-angle scattering data can be increased and the experimental accuracy can be improved.
Owner:INST OF HIGH ENERGY PHYSICS CHINESE ACADEMY OF SCI
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