The invention provides a treatment process of
nickel-containing
alloy powder in a
hydrochloric acid system. The treatment process comprises the following steps that (1) presoaking of the
nickel-containing
alloy powder is carried out, specifically, the
nickel-containing
alloy powder, concentrated
hydrochloric acid and water are mixed, and then heated, stirred and presoaked; (2) high-pressure
oxygen introduction and leaching is carried out, specifically, prepreg is poured into a high-pressure kettle, heating is carried out,
oxygen is introduced to react for a certain time, cooling and liquid-
solid separation are carried out, leaching residues are produced and stacked, and leaching liquid enters a next process; (3)
neutralization and
impurity removal are carried out, specifically, the pH value of the leaching liquid is adjusted by using
nickel carbonate, a
neutralization solution and
neutralization slag are produced, and the neutralization
slag returns to the leaching process; (4)
cobalt extraction with resin is carried out, specifically,
cobalt ions in the neutralization solution is adsorbed with the resin to produce
cobalt carbonate precipitate and cobalt-extracted liquid; and (5) product preparation is carried out, specifically,
nickel carbonate is prepared from a small part of cobalt-extracted liquid for a neutralization and
impurity removal process, the rest liquid is concentrated and pyrolyzed,
hydrochloric acid is produced for recycling, and
nickel oxide is taken as a final product. According to the treatment process, the
nickel oxide product is produced through the leaching, purifying and pyrolyzing processes, meanwhile, hydrochloric acid and a neutralizing and
impurity-removing
reagent are recycled, and the treatment process is clean and
environmentally friendly.