The invention belongs to the field of
metal sulfide nano-materials, and particularly relates to a method for preparing a carbon-loaded
metal sulfide nanocomposite through electrostatic
spinning, whichcomprises the following steps: (1) preparing a
spinning precursor solution: respectively dissolving a
thiacalixarene metal cluster compound and a
spinning aid in DMF (
Dimethyl Formamide), and mixing;(2) preparing nano-fibers by electrostatic spinning: sucking the obtained spinning precursor solution into an
injector, adjusting the pump flow rate and
voltage of the
injector and the distance between a spinning needle and a receiving plate, spinning, and receiving a nano-
fiber felt by the receiving plate; (3) pre-oxidizing the nano-
fiber felt: pre-oxidizing the collected nano-
fiber felt; and (4) carbonizing in an N2
atmosphere: carbonizing the pre-oxidized nano-fiber felt, and naturally cooling to obtain the target product. The target product is ideal in electrochemical performance and goodin
capacitance characteristic, the flaky carbon material is directly used as an
electrode, additives or impurities such as a binding agent can be eliminated, and the energy capacity and performance are improved.