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Acidic visco-elastic fluid, its preparation method and application thereof
InactiveCN102453481AGood sand carryingHigh viscoelasticityDrilling compositionFracturing fluidSURFACTANT BLEND
Owner:CHINA UNIV OF PETROLEUM (BEIJING)
Acrylamide polymer thickener and preparation method thereof, and fracturing fluid
ActiveCN106146730AHigh temperature resistanceImprove high temperature resistanceDrilling compositionPolymer scienceFracturing fluid
The invention provides an acrylamide polymer thickener and a preparation method thereof, and a fracturing fluid, wherein the acrylamide polymer thickener is composed of the components by the mass percentage: 20%-45% of a hydrophilic propenyl monomer, 4%-6% of a hydrophobic propenyl monomer, 1%-2% of an emulsifier, 0.2%-0.5% of an initiator, a latent crosslinking agent and the balance water, wherein the latent crosslinking agent accounts for 0.5%-1.8% of the total mass of the hydrophilic propenyl monomer and the hydrophobic propenyl monomer; the acrylamide polymer thickener provided by the invention solves the technical problems in the prior art that a polymer thickener has poor temperature resistance and salt tolerance and poor shearing stability, and the prepared acrylamide polymer thickener has high-temperature performance, and can effectively meet the requirements of on-site construction of slick water fracturing.
Owner:PETROCHINA CO LTD
Preparation method and fracturing construction method of locally and continuously mixed clean fracturing fluid additive
ActiveCN102031102AGood sand carryingEasy to getFluid removalDrilling compositionFracturing fluidProcess engineering
The invention discloses a preparation method and a fracturing construction method of a locally and continuously mixed clean fracturing fluid additive. The invention is characterized in that the preparation of the locally and continuously mixed clean fracturing fluid additive comprises four steps, and the purposes of local and continuous mixing and continuous construction of the prepared clean fracturing fluid additive can be realized without preparation in a fluid preparation station or a well filed in advance. Thus, both the preparation method and the fracturing construction method of the locally and continuously mixed clean fracturing fluid additive are very simple and convenient.
Owner:RES INST OF SHAANXI YANCHANG PETROLEUM GRP
Clean carbon dioxide foam fracturing fluid and preparation method thereof
ActiveCN104531129AFine foamImprove foam stabilityDrilling compositionPotassium persulfatePolymer science
The invention discloses clean carbon dioxide foam fracturing fluid and a preparation method thereof, and relates to the technical field of oilfield chemistry and fracturing production increase. The carbon dioxide foam fracturing fluid is mainly composed of a base solution, a foaming agent, a gel breaker and liquid carbon dioxide with the mass ratio being 100 to 0.15-0.45 to 0.02-0.08 to 100-900. The base solution is formed by 0.2%-0.55% of a thickening agent and water. The thickening agent is mainly formed by bisacrylamide, vinyl pyrrolidone, kation unsaturated monomer, anion unsaturated monomer, an initiator, sodium carbonate, an emulsifying agent and a hydrotropy agent. The foaming agent is mainly formed by hexadecyl dimethyl tertiary amine, dimethyl sulfate, caustic soda flakes, potassium persulfate and solvent. The clean carbon dioxide foam fracturing fluid has the advantages of being high in foam stability, high in temperature resistance and shear resistance, high in sand-carrying performance, wide in applicable temperature range, extremely low in residue content, high in backflow performance, and small in secondary damage to a reservoir after fracturing, thereby improving the fracturing effect and increasing the reservoir productivity.
Owner:CHENGDU BAICHUN PETROLEUM TECH
Formula and preparation method suitable for preparing fracturing fluid from continental facies shale gas well fracturing flow-back fluid treatment water
InactiveCN104610954ASolve the problem of large water consumptionConserve waterDrilling compositionSoil scienceFracturing fluid
The invention discloses a formula and a preparation method suitable for preparing fracturing fluid from continental facies shale gas well fracturing flow-back fluid treatment water, belonging to the technical field of oilfield chemistry. The formula for preparing the fracturing fluid from the continental facies shale gas well fracturing flow-back fluid treatment water is provided aiming at the deficiencies existing in the prior art. The formula consists of base fluid and a cross-linking agent, wherein the cross-linking agent is an anti-temperature mineralization-degree-resistant cross-linking agent, and the formula comprises 0.4%-0.6% of cross-linking agent and the balance of base fluid; the base fluid consists of the following components in percentage by mass: 0.4%-0.45% percent of hydroxypropylguar gum, 0.3%-0.5% of gas well clean up additive, 1%-2% of stabilizer, 0.1%-0.15% of bactericide, 0.1%-0.2% of modifier, 0.03%-0.05% of antisludging agent, 0.6%-0.8% of gel breaker and the balance of the continental facies shale gas well fracturing flow-back fluid treatment water. The cyclic utilization of the continental facies shale gas well fracturing flow-back fluid treatment water is realized through the formula of the fracturing fluid, and the prepared fracturing fluid has good sand-carrying property.
Owner:RES INST OF SHAANXI YANCHANG PETROLEUM GRP
Fracturing fluid prepared by recovery waste water of crude oil and preparation method of fracturing fluid
ActiveCN103074049AAlleviate needsSolve processing problemsDrilling compositionCross-linkFracturing fluid
The invention discloses an association polymer fracturing fluid prepared by recovery waste water of crude oil. The fracturing fluid comprises the following components: 0.2-1.4wt% of thickening agent, 0.01-0.1wt% of thickening assistant, 0.05-0.1% of metal ion stabilizing agent, 0.02-0.05wt% of water block preventive, 0.05-0.2wt% of high-temperature stabilizing agent, 1-2wt% of clay stabilizing agent and the balance of the recovery waste water of the crude oil. Compared with the prior art, the fracturing fluid has the benefits that the fracturing fluid system adopts an association polymer as a primary thickening agent, no cross-linking agent is used, structural viscosity is formed by the synergetic effect of the association polymer and an ampholytic surfactant, and the fracturing fluid has the characteristics of temperature resistance, good salt tolerance, shear resistance, bacterial corrosion resistance and low friction, and has a good solid carrying behavior when the viscosity is greater than 20mPa*s.
Owner:CHENGDU BAICHUN PETROLEUM TECH +1
Supercritical carbon dioxide based fracturing liquid system and application thereof
ActiveCN103540308AViscosity value adjustableGood sand carryingFluid removalDrilling compositionEnvironmental resistanceAdhesive
Owner:CHINA NAT PETROLEUM CORP CHUANQING DRILLING ENG CO LTD +1
Cross-linkable high-temperature-resistant residue-free polybasic copolymerizable fracturing fluid and preparation method thereof
ActiveCN104178102AHigh apparent viscosityImprove structural strengthDrilling compositionCross-linkPolymer science
The invention discloses a cross-linkable high-temperature-resistant residue-free polybasic copolymerizable fracturing fluid and a preparation method thereof. The preparation method comprises the following steps of (1) preparing a thickener for the fracturing fluid; (2) preparing a cross-linking agent for the fracturing fluid; (3) preparing a gel breaker for the fracturing fluid and (4) preparing the cross-linkable high-temperature-resistant residue-free polybasic copolymerizable fracturing fluid. The fracturing fluid prepared by adopting the preparation method has the characteristics of excellent viscoelasticity, temperature resistance and shear resistance, sand-carrying performance and wide applicable temperature range; the fracturing fluid can well meet the requirement on the fracturing construction, and the content of the residue is very low; after the fracturing, the secondary harm to a reservoir is small and thus the fracturing effect is improved and the production capacity of the reservoir is increased.
Owner:CHENGDU BAICHUN PETROLEUM TECH
Low-cost water-based clean fracturing fluid and gel breaking fluid used for fracturing
The invention provides a water-based clean fracturing fluid for fracturing. The fracturing fluid is formed by a small canonic antiswelling agent, organic sodium salt, a cationic surface active agent and water, wherein the concentration of the small canonic antiswelling agent is 0.4 percent by mass, the concentration of the organic sodium salt is 0.06 to 0.18 percent by mass, the concentration of the cationic surface active agent is 0.2 to 0.6 percent by mass, the mass ratio of the cationic surface active agent and the organic sodium salt is 1:0.3, the organic sodium salt is sodium salicylate, and the cationic surface active agent is any one or the mixture of 16-18 alkyl-3-methylammonium chloride. The invention can well solve the pollution problem of the fracturing fluid to the coal bed, simultaneously improve the sand-carrying performance of the fracturing fluid greatly, the price thereof is only 1.5 to 2.0 times of active water fracturing fluid and is far lower than that of guargum fracturing fluid and common clean fracturing fluid.
Owner:CHINA UNITED COALBED METHANE NAT ENGRES CENT
Acidic water repellent associated matter fracturing fluid
ActiveCN102206484ALess residueGood anti-expansion effectDrilling compositionDemulsifierSalt resistance
The invention relates to acidic water repellent associated matter fracturing fluid. The fracturing fluid consists of crosslinked fluid and original fluid, wherein the crosslinked fluid comprise the following components in percentage by weight: 0.2 to 0.5 percent of acidic crosslinked agent, 0.01 to 0.035 percent of crosslinked regulator A, 0.02 to 0.3 percent of crosslinked regulator B, 0.02 to 0.2 percent of gelbreaker and the balance of water; and the original fluid comprises the following components in percentage by weight: 0.3 to 0.7 percent of FS-927 polymer, 1 to 4 percent of potassium chloride, 0.5 to 1.5 percent of MJ-1 high-temperature discharge aiding agent, 0 to 2.5 percent of JTY-100 fluid loss agent, 1 percent of PR-1 demulsifier, 0 to 0.02 percent of temperature stabilizer and the balance of water. The fracturing fluid has the advantages of high crosslinking delaying performance, temperature resistance, salt resistance and shearing resistance, high sand carrying capacity, small damages to stratum, low friction resistance, low residue amount and good expansion preventing effect, can easily break gel and flow back, and breaks through the traditional concept that retarded crosslinking polymer fracturing fluid has temperature resistance and sheering resistance which can be realized at the temperature of not more than 100 DEG C.
Owner:PETROCHINA CO LTD
Fracturing fluid
ActiveCN103666437AGood sand carryingGood temperature and shear resistanceDrilling compositionCarrying capacityFracturing fluid
The invention relates to a fracturing fluid which comprises a base fluid A and a base fluid B, wherein the base fluid A is prepared from a thickening agent, a hydrotropy thickening agent, a clay stabilizer, a discharge aiding agent, a sterilizing agent, a demulsifying agent, a low-temperature activator and water; the base fluid B is prepared from a low-molecular weight polymer, the clay stabilizer, the discharge aiding agent, the sterilizing agent, the demulsifying agent, the low-temperature activator and the water. When fracturing construction is carried out, the base fluid A and the base fluid B are mixed in proportion, the low-molecular weight polymer and a thickening agent molecule are mutually wound in a stirring process to form a certain space reticular structure for effective thickening, and the hydrotropy thickening agent compresses a winding structure through electric repulsion so that a gel is further thickened and forms good solid carrying capacity; the shearing is carried out at 50 DEG C and 170S-1,3.5MPa for 60 minutes, the viscosity is more than 50 mPa.s, an oxidized type gel breaker is added according to the proportion of 0.01%-0.20% in a wedge shape, the gel can be thoroughly broken within 2 hours, and the viscosity of gel breaking liquid is less than 5 mPa.s.
Owner:PETROCHINA CO LTD
Self heat-generating and gas-generating clean fracturing fluid
InactiveCN102952535ALess harmfulImprove seepage capacityDrilling compositionPolymer scienceFiltration
The invention relates to a self heat-generating and gas-generating clean fracturing fluid comprising the raw materials of, by mass: 0.2-0.5% of a thickening agent, 2-4% of a structural enhancer, 2-15% of a heat generating agent A, 2-10% of a heat generating agent B, 2% of a structural enhancer solvent, 1-5% of a heat generating catalyst, 0.1-1% of a cleanup additive, 0.05-1.0% of a gel breaker, 0.05-0.15% of a broken plastic additive, and balance of water. The fracturing fluid has good temperature resistance, good shearing resistance, and sand-carrying property. The fluid can automatically generate heat and gas, such that the fracturing fluid is foamed in stratum. The fluid has low filtration loss. Gel breaking can be carried out with conventional persulfate and stratum oil, gas, and water dual gel breaking manner. Quick flow-back after pressure can be realized, and low-pressure oil and gas well self-spraying flow-back effect can be greatly improved. No residue and low harm is caused. The fracturing fluid can be used in fracturing modification of middle-shallow-stratum high-pour-point oil, crude oil with high viscosity, and low-pressure low-permeability oil and gas reservoirs.
Owner:PETROCHINA CO LTD
Emulsion type drag reduction thickener used for oil and gas well fracturing, and preparation method thereof
InactiveCN106939159AImprove performanceSimple processDrilling compositionPotassium persulfateReduction rate
The invention discloses a preparation method of an emulsion type drag reduction thickener used for a fracturing fluid. The method comprises the following steps: weighing raw materials comprising acrylamide, functional monomers, span80, potassium persulfate, cyclohexane, OP-10 and deionized water; stirring and mixing a dispersant and cyclohexane in a polymerization monomer; and carrying out initiation and polymerization to form the emulsion type drag reduction thickener. Compared with the prior art, the method has disclosed in the invention the advantages of simple process and environmental protection; and the emulsion type drag reduction thickener has stable performances, the highest reservoir temperature can reach 150 DEG C, the drag reduction rate is 70% or above, and the above one product solves two problems of a drag reduction stage and a sand carrying stage.
Owner:北京希涛技术开发有限公司
Fracturing fluid prepared by utilizing fracturing flow-back fluid and preparation method thereof
InactiveCN105131932ACompletely broken glueAchieve recyclingDrilling compositionPolymer scienceFracturing fluid
The invention provides a fracturing fluid prepared by utilizing a fracturing flow-back fluid and a preparation method thereof. The fracturing flow-back fluid is not processed or subjected to simple processing and then is directly used to prepare the fracturing fluid. The fracturing fluid is composed of a thickening agent and other auxiliary agents, and employs a crosslinking agent compatible with a guar gum thickening agent used for the flow-back fluid and a crosslinking promoter. The formula crosslinking time 1-3 min is adjustable, the temperature resistance is 120 DEG C or more, and the system frictional resistance is reduced by 20% or more compared with a common hydroxypropyl guar gum fracturing liquid. The fracturing liquid preparation method realizes cyclic utilization of the fracturing flow-back fluid, and the prepared fracturing liquid possesses good performances.
Owner:昆山京昆油田化学科技有限公司
Inverse-phase micro-emulsion polymer fracturing fluid system with online construction function
ActiveCN108559479AGood resistance reduction effectEasy to reuseDrilling compositionMethacrylatePolymer science
Owner:SOUTHWEST PETROLEUM UNIV +1
Preparation and application of anionic clean fracturing liquid and gel breaker thereof
InactiveCN106566521AGood effectGood sand carryingFluid removalDrilling compositionFracturing fluidSURFACTANT BLEND
The invention relates to the technical field of oil filed fracturing, and specifically relates to an anionic clean fracturing liquid, which is composed of 0.5 to 10% of anionic surfactant, 5 to 20% of counter-ion salts, and the balance being water. The provided clean fracturing liquid preserves all advantages of conventional clean fracturing liquids. The species of additives can be reduced and the requirements on liquid blending equipment can be lowered by using the clean fracturing liquid. The fracturing liquid can be used in oil fields with a high mineralization degree. The gel breaking time can be well controlled by using a gel breaker and the cost is reduced.
Owner:EAST CHINA UNIV OF SCI & TECH
Organic aluminum-zirconium crosslinking agent and preparation method thereof, and low-molecular polymer fracturing fluid
InactiveCN104371699AImprove high temperature resistanceFacilitate cross-linkingDrilling compositionSolubilityFracturing fluid
The invention discloses an organic aluminum-zirconium crosslinking agent and a preparation method thereof, and a low-molecular polymer fracturing fluid. The crosslinking agent is prepared by reacting the following raw materials in parts by weight: 15-25 parts of zirconium salt, 15-25 parts of aluminum salt, 150-250 parts of polyalcohol, 75-85 parts of organic acid, 15-25 parts of gluconate and 55-65 parts of water. The organic aluminum-zirconium crosslinking agent has excellent high temperature resistance, and has favorable crosslinking effect under the conditions of high temperature and high salinity. The organic aluminum-zirconium crosslinking agent is stable under the condition of low pH value, can implement acid crosslinking, and ensures the normal proceeding of the acid fracturing. The organic aluminum-zirconium crosslinking agent has favorable compatibility with polymers and high crosslinking capacity; and the fracturing fluid formed by compounding the organic aluminum-zirconium crosslinking agent with polymers has the advantages of stable gel, excellent solid carrying capacity, excellent viscosity breaking performance and excellent shearing resistance under high-temperature conditions. The organic aluminum-zirconium crosslinking agent has the characteristics of high solubility, no pollution and low damage degree to the reservoir, and has wide application prospects.
Owner:CHINA PETROLEUM & CHEM CORP +1
Multifunctional composite fracturing liquid system
ActiveCN105219372AStrong shear resistanceSimple recipeDrilling compositionHigh concentrationOrganic synthesis
The invention provides a multifunctional composite fracturing liquid system. The multifunctional composite fracturing liquid system comprises resistance reduction water and high-viscosity sand carrying liquid, wherein the resistance reduction water comprises 0.02 to 0.15 percent by weight of the resistance reduction agent; the high-viscosity sand carrying liquid comprises 0.2 to 0.75 percent by weight of a thickening agent; the resistance reduction agent and the thickening agent are identical aggregation polymer and are natural modified aggregation polymer and / or organic synthetic aggregation polymer. The low-concentration aggregation polymer having good resistance reduction performance and the high-concentration aggregation polymer having good sand carrying performance are used for forming the multifunctional composite fracturing liquid system; compared with the existing composite fracturing liquid system, the multifunctional composite fracturing liquid system has characteristics of fewer types of additives, simple formula and simple preparation process; meanwhile, the system has good resistance reduction performance, shear resistance and sand carrying performance; return liquid of the system can be reused after being treated in a way such as flocculating, precipitating and filtering, and the utilization rate of water for fracturing is increased.
Owner:SICHUAN GUANGYA POLYMER CHEM
High-temperature-resistant full-suspension low-damage fracturing fluid and preparation method thereof
The invention discloses a high-temperature-resistant full-suspension low-damage fracturing fluid, which comprises the following components in percentage by weight: 0.3-0.5% of a low-damage thickeningagent, 0.1-0.4% of a multifunctional stabilizer, 0.1-0.3% of a regulator, 0.4-0.8% of a suspension synergist and the balance of clear water or saline water; the preparation method of the fracturing fluid comprises the following steps of: 1, adding the low-damage thickening agent, the multifunctional stabilizer and the regulator into clear water or saline water under a stirring condition, uniformlystirring, and swelling for 2 to 4 hours to obtain fracturing fluid base liquid; 2, fully mixing the fracturing fluid base liquid and the suspension synergist to form the full suspension fracturing fluid with excellent sand carrying performance and temperature resistance under the combined action of physical crosslinking and chemical crosslinking. The fracturing fluid is superstrong structure fluid formed by carrying out physical crosslinking and chemical crosslinking on acrylamide polymer and suspension synergist together, and the temperature resistance can reach 150 DEG C; the sand carryingperformance is excellent, the strong spatial structure can completely suspend a proppant, and the influence of temperature is small.
Owner:SOUTHWEST PETROLEUM UNIV +2
High-temperature-resistant thickening agent for fracturing fluid, and preparation method and application thereof
InactiveCN111019042AExcellent high temperature resistance and salt resistanceGood solubilityDrilling compositionFunctional monomerMaterials science
The invention discloses a high-temperature-resistant thickening agent for a fracturing fluid, and a preparation method and an application thereof. The high-temperature-resistant thickening agent for the fracturing fluid and is characterized in that the thickening agent comprises acrylamide, a salt-resistant functional monomer and a temperature-sensitive functional monomer free radical; and the molar ratio of the acrylamide to the salt-resistant functional monomer to the temperature-sensitive functional monomer is 1:(0.01-0.08):(0.05-0.15). A temperature-sensitive unit and a salt-resistant unitare introduced into an acrylamide molecular chain in a solution copolymerization mode, so that the copolymer is endowed with excellent high-temperature resistance and salt resistance and also has good solubility, viscoelasticity and sand carrying property.
Owner:四川盛年同缔实业有限公司
Guar gum cleaning fracturing fluid with micro residue and weak damage
InactiveCN106905948AUse low concentrationReduce harmDrilling compositionPolymer scienceSulfate radicals
The invention relates to guar gum cleaning fracturing fluid with micro residue and weak damage. The guar gum cleaning fracturing fluid with micro residue and weak damage is composed of base liquid, a cross-linking agent and a gel breaker, the base liquid is composed of hydroxypropyl guar gum, a cleanup additive, an anti-swelling stabilizing agent, a fracturing bactericide, a fracturing de-emulsifier, a scale inhibitor and water. According to the invention, a guar gum multinucleated cross-linking agent with low amount is used, delay crosslinking effect is strong, guar gum concentration is greatly reduced, glue breaking residue amount is reduced, a multifunctional scale inhibitor is cooperated for preventing fouling generated by water used for fracturing liquid and stratum water, a selective polymer fracturing catalyst capable of thoroughly breaking glue and no generating sulfate radical is selected, liquid viscosity and residue content are reduced, the surface tension of the gel breaker after gel is broken is lower, the gel breaker is easily discharged, the formed guar gum multinucleated cross-linking agent has good temperature and shearing sustainability, and excellent proppant carrying capacity.
Owner:SHAANXI RES DESIGN INST OF PETROLEUM CHEM IND
Crosslinking agent system, low-concentration polymer crosslinked fracturing fluid and preparation methods of crosslinking agent system and low-concentration polymer crosslinked fracturing fluid
InactiveCN108179008AImprove efficacyLower seepage capacity of the groundDrilling compositionPolymer scienceFracturing fluid
The invention provides a crosslinking agent system, a low-concentration polymer crosslinked fracturing fluid and preparation methods of the crosslinking agent system and the low-concentration polymercrosslinked fracturing fluid. The low-concentration polymer crosslinked fracturing fluid has both high viscoelasticity of the existing polymer fracturing fluid and low damage of a clean fracturing fluid. The economical efficiency of the fracturing fluid is improved by means of low concentration, and accordingly, the low-concentration polymer crosslinked fracturing fluid is more popular with oilfields on the premise of cost decreasing, benefit increasing and reservoir protecting. A prepared base fluid has the viscosity range of 10-24 mPa.s, and is easy to prepare and pump. Delayed crosslinkingtime is 30-120 s, gel can be formed after crosslinking, viscosity is enhanced three times or more, sand carrying is facilitated, and a supporting agent can be delivered to the far end of a fracture. Therefore, the low-concentration polymer crosslinked fracturing fluid inherits various advantages of the traditional fracturing fluid, and further, the sand carrying capability and fracture conductivity of the fracturing fluid can be improved effectively.
Owner:CHENGDU LEARN PRACTICES TECH CO LTD
Low-damage and ultralow-concentration guar gum fracturing fluid system, preparation method and application of guar gum fracturing fluid system
ActiveCN106085404AReduce concentrationReduced shear resistanceDrilling compositionCarrying capacityHeat resistance
Owner:CHINA PETROLEUM & CHEM CORP +1
Slickwater fracturing fluid suitable for being used at hypersalinity condition
InactiveCN108559477AGood drag reduction performanceSimple processDrilling compositionSalt resistanceStabilizing Agents
Provided is a slickwater fracturing fluid suitable for being used at a hypersalinity condition. The slickwater fracturing fluid is prepared from, by mass, 0.15-0.45% of polymer viscosifier, 0.05%-0.15% of chelating agent, 0.05%-0.15% of dispersing agent, 0.02%-0.05% of clay stabilizer, 0.30%-0.50% of structure stabilizer, 0.02%-0.06% of gel breaker and the balance water. The slickwater fracturingfluid has the advantages of being low in viscosity, friction and cost and easy to recycle, easily flowing back and the like; the problems are mainly solved that at the hypersalinity condition, polymers are poor in salt resistance and sand-carrying stability and does not easily disperse; the problem can also be solved that vegetable glue fracturing fluid easily rots; after being filtered, flow-backliquid can be further directly recycled, and requirements of large-scale fracturing construction of compact oil-gas reservoirs can be effectively met.
Owner:PETROCHINA CO LTD
High-density fracturing fluid capable of slowing crosslinking and resisting high temperature
ActiveCN103254885AGood temperature and shear resistanceIncrease pressureDrilling compositionCross-linkPolymer science
The invention relates to a high-density fracturing fluid capable of slowing crosslinking and resisting high temperature. The fracturing fluid is composed of a stock solution and a crosslinking liquid with a volume ratio of 10 : 1, wherein the stock solution comprises, by weight percent, 0.5-0.65 % of hydroxypropyl guar gum, 8-45 % of a weighting agent A, 6-30 % of a weighting agent B, 0.5-2 % of a ZJ-07 cleanup additive, 0.01-0.04 % of a pH-value conditioning agent A, and the balance being water; the crosslinking liquid comprises, by weight percent, 0.5-3 % of a cross-linking agent YGB, 1-2 % of a cross-linking agent HT, 0.1-0.4 % of a pH-value conditioning agent B, 0-0.35 % of a gel breaker and the balance being water. The fracturing fluid is good in temperature-resistance and shearing-resistance performances, wherein the temperature-resistance performance is up to 145 DEG C, and a viscosity is still more than 120 Pa*S after the liquid is sheared for 90 minutes under 145 DEG C and 170 S<-1>.
Owner:PETROCHINA CO LTD
Boron cross-linking agent for fracturing fluid and preparation method thereof and ultralow hydroxypropylguar gum concentration fracturing fluid prepared from boron cross-linking agent
InactiveCN105754574AIncreased cross-linking sitesSmall sizeDrilling compositionCross-linkPolymer science
The invention relates to a boron cross-linking agent for a fracturing fluid in the technical field of oil-gas field development and an ultralow hydroxypropylguar gum concentration fracturing fluid prepared from the boron cross-linking agent. The cross-linking agent comprises the following ingredients (by weight): 20-30 parts of an amide compound, 40-60 parts of water, 50-100 parts of glycol, 13-25 parts of boric acid, 20-30 parts of n-butanol and 30-40 parts of an aldehyde compound. The ultralow hydroxypropylguar gum concentration fracturing fluid contains (by volume): 98.6-98.9 parts of a hydroxypropylguar gum aqueous solution and 0.6-0.9 part of the boron cross-linking agent for a fracturing fluid. By the use of the cross-linking agent and under the precondition of guaranteeing performance of the fracturing fluid, hydroxypropylguar gum concentration can be reduced by more than 30%, thus lowering costs of the fracturing fluid and decreasing damage to the bottom layer.
Owner:CHINA PETROLEUM & CHEM CORP +1
Anhydrous fracturing fluid suitable for shale gas and preparation method of anhydrous fracturing fluid
The invention belongs to the technical field of petrochemical engineering, and particularly relates to an anhydrous fracturing fluid suitable for shale gas and a preparation method of the anhydrous fracturing fluid. The anhydrous fracturing fluid suitable for shale gas is prepared from the following raw materials in percentage by mass: 0.5-2% of a crosslinking agent, 2-6% of a complex iron activator and the balance of a low carbon hydrocarbon; in a pressure vessel with a pressure of 0.8-3.0 MPa, the crosslinking agent is added into the low carbon hydrocarbon to be uniformly mixed, the complex iron activator is added to be stirred for 2-5 min, so that the anhydrous fracturing fluid suitable for shale gas is obtained; and the low carbon hydrocarbon is one or a mixture of more of propane, butane, n-hexane, n-heptane and kerosene. The anhydrous fracturing fluid suitable for shale gas easily flows back, has a good sand-carrying property, does not harm reservoirs, and can satisfy the needs of fracturing reconstruction of shale oil and gas and strong water-sensitive compact oil and gas reservoirs. A synthetic method is simple, and the content of an effective component dialkyl phosphate in a product is high, thereby facilitating the industrialization production of the anhydrous fracturing fluid.
Owner:SOUTHWEST PETROLEUM UNIV
Clean fracturing fluid for oil fields and preparation method thereof
ActiveCN105820805AImprove performanceLow temperature resistanceDrilling compositionOrganic acidFracturing fluid
The invention discloses clean fracturing fluid for oil fields and a preparation method thereof, belonging to the technical field of oil production engineering in the petroleum industry. The clean fracturing fluid can be obtained by synthesizing a gemini surfactant by using organic acids, an N,N-dimethylamino compound, an N,N'-diaminoalkylethylenediamine compound and halohydrin as raw materials and then stirring a water solution of the gemini surfactant and an ammonium chloride solution according to a certain proportion. Compared with traditional fracturing fluid, the clean fracturing fluid has good temperature and shear resistance and good sand-carrying property, dispenses with gel breakers and reverse discharge and is convenient to use.
Owner:HIGH & NEW TECH RES CENT OF HENAN ACAD OF SCI
High-temperature-resistant xanthan gum fracturing fluid and preparation method thereof
InactiveCN106800924AGood sand carryingImprove temperature and shear resistanceDrilling compositionFracturing fluidChloride
The invention provides a high-temperature-resistant xanthan gum fracturing fluid and a preparation method thereof. The fracturing fluid comprises the following components in parts by weight: 0.4-0.6 part of xanthan gum, 0.2-2 parts of temperature stabilizer and 1.0-3.0 parts of other auxiliary additives. The temperature stabilizer (composed of calcium chloride, potassium formate and the like) is added to promote the transformation of the xanthan gum structure to the double spiral structure, thereby enhancing the temperature resistance and shear resistance; and thus, the xanthan gum still has favorable solid-carrying behavior under the conditions of high temperature and high shear.
Owner:PETROCHINA CO LTD
Clean high-temperature water-base fracturing fluid
InactiveCN107674668AViscoelasticImprove temperature resistanceDrilling compositionWater basedCross-link
The invention provides clean high-temperature water-base fracturing fluid. The clean high-temperature water-base fracturing fluid comprises components including, by weight, 0.5%-6% of clay stabilizers, 2%-6% of accelerators, 0.01%-0.1% of bactericides, 0.6%-3.0% of alcohol with a low molecular weight, 0.4%-2% of zwitterionic surfactants, 0%-0.5% of polysaccharide compounds and the balance water. The components are mixed with one another to obtain the clean high-temperature water-base fracturing fluid. The clean high-temperature water-base fracturing fluid has the advantages that as proved by indoor evaluation, the temperature resistance of the clean high-temperature water-base fracturing fluid can reach 150 DEG C at least, and accordingly the clean high-temperature water-base fracturing fluid is superior to general clean fracturing fluid systems; the dosage of betaine is 0.4%-2% (a weight ratio) and is far lower than the dosage (2%-5%) of amphoteric surfactants in formulas for conventional fracturing fluid; the clean high-temperature water-base fracturing fluid is convenient to use and operate, excellent in sand suspension ability and superior to common cross-link guar gum and quaternary ammonium salt systems, and cross-link can be omitted.
Owner:河北中大永迪生物科技有限公司
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