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48results about How to "Eliminate production safety hazards" patented technology

Equipment spot inspection method, device and server

The invention is applicable to the technical field of equipment spot inspection and provides an equipment spot inspection method, device and a server. The method comprises steps: corresponding two-dimensional code information is compiled for each piece of to-be-inspected equipment and the two-dimensional code information of each piece of to-be-inspected equipment is imported to an equipment spot inspection system, wherein the two-dimensional code information comprises the identity information and the temperature standard data of the to-be-inspected equipment; the spot inspection information ofa test device is received, wherein the spot inspection information is the information generated by the test device according to the identity information and the spot inspection temperature data of the to-be-inspected equipment; and the spot inspection temperature data is compared with the corresponding standard temperature data of the to-be-inspected equipment, and the comparison result is transmitted to the test device and a corresponding intelligent terminal. According to the equipment spot inspection method, the device and the server, the spot inspection information can be stored in real time during an equipment spot inspection process, the spot inspection information is fed back to a technician, the technician can timely eliminate hidden production dangers, and the equipment spot inspection working efficiency is improved.
Owner:邯郸新兴发电有限责任公司

Roadway surrounding rock separation layer displacement monitor

The invention provides a roadway surrounding rock separation layer displacement monitor, which comprises a shell, a preventer plate, two sets of separation layer displacement transmission mechanisms, a separation layer displacement sensing unit and an information acquisition processing unit, wherein the separation layer displacement transmission mechanism comprises a displacement bracing wire, a transmission shaft, a driving wheel, a driving band, a take-up reel, a roll-up spring and a lock device; the separation layer displacement sensing unit comprises a support circuit board, a T platform, a grating and a photoelectric coupler; the preventer plate is provided with a leakage hole; and one end of the displacement bracing wire is fixed in the stratum and the other end thereof is clamped inside a T slot of the take-up reel. The monitor of the invention has the beneficial effects of having simple manufacturing technology and structure, convenient operation, improving displacement inspection accuracy, being applied to construction processes of mine exploitation, building, water conservancy, roads and the like, effectively and automatically monitoring surrounding rock mass, roadway roof and floor, dam bodies, side slopes and the like in real time, and timely eliminating potential safety hazard of production; and the monitor of the invention can provide basis for the roadway and the support rock mass design.
Owner:安里千

Rod type strata displacement monitor and system

InactiveCN101526351ADisplacement monitoring is suitable forHigh precisionUsing optical meansProfile tracingGratingMonitoring system
The invention provides a rod type strata displacement monitor, which comprises a displacement sensing unit and an information acquiring and processing unit, wherein the displacement sensing unit comprises a sensor framework, a displacement transmission mechanism, a grating displacement detector unit which uses a grating detection method to convert displacement to an electric signal, and a displacement direction recognizer unit. The invention also provides a strata displacement monitoring system using the rod type strata displacement monitor, wherein the system is provided with a plurality of rod type strata displacement monitors and an underground information conversion and communication substation. A plurality of rod type strata displacement monitors can be arranged in series connection in the same borehole; and compared with the prior displacement detector with a pulling thread, the rod type strata displacement monitor not only solves the problem of reducing the measuring accuracy caused by natural prolonging of the pulling thread, but also can automatically distinguish the displacement direction and improve the strata displacement detection accuracy.
Owner:安里千

Full automatic multi-map puncher system used for book page die punching

The invention discloses a full automatic multi-map puncher system used for book page die punching. The system comprises a delivery platform, a punching platform, an automatic pushing device and an automatic page turning device, the punching platform and the automatic page turning device are arranged on the same side of the delivery platform, placing grooves which are used for placing books are reserved between the punching platform and the delivery platform and between the automatic page turning device and the delivery platform, and the automatic pushing device is arranged on the delivery platform. By means of the system, multi-map books can be embedded in the placing grooves to be delivered on the delivery platform through the automatic pushing device to the punching platform, page turning of the multi-map books can be achieved through the automatic page turning device in the delivery process, fully automatic production line die punching production of the multi-map books can be achieved, the labor intensity of operators is greatly reduced to save a large amount of labor force, production safety potential hazards are eliminated, the production speed is accelerated, and the die punching production efficiency of the multi-map books is greatly improved.
Owner:HESHAN ASTROS PRINTING

Purification method of antioxidant rosmarinic acid for tobacco

Belonging to the technical field of tobacco additives, the invention discloses a purification method of an antioxidant rosmarinic acid for tobacco. The purification method is carried out according to the steps of: (1) performing primary purification: first passing a rosmarinic acid-containing extraction solution A through a 30nm inorganic membrane, then passing it through an organic spiral-wound membrane with molecular weight cut-off of 3000, thus obtaining the filtrate B; (2) making sample loading preparation: subjecting the filtrate B to reverse osmosis membrane concentration to obtain a concentrated sample C; (3) conducting fine purification: carrying out chromatographic separation on the concentrated sample C by a gel column and collecting rosmarinic acid fraction; and (4) further concentrating and purifying the collected rosmarinic acid fraction by a pressure reduction distillation method and a recrystallization method in the prior art so as to make the rosmarinic acid content reach 80%-95%. The method provided in the invention is simple, safe, pollution-free, and is easy to implement.
Owner:HUBEI CHINA TOBACCO IND

Construction method of engineering bacteria with constitutive expression of dextranase and preparation method of enzyme

The invention discloses a construction method for constitutive expression engineering bacteria of dextranase and a preparation method for enzyme. The construction method for the constitutive expression engineering bacteria comprises the following steps of: (1) inserting an obtained gene in a multi cloning site of an expression vector pGAPZalphaA to construct a recombinant plasmid pGAPZalphaA-dex;and (2) linearly transforming the recombinant plasmid to Pichia pastoris KM71H, and screening positive clone bacteria. The engineering bacteria are used in a preparation method for the dextranase. Bythe invention, the gene of the dextranase is effectively expressed in the Pichia pastoris successfully, a cheap carbon source is taken as a raw material, flammable and explosive methanol is not needed in the fermentation process, potential production safety hazards are eliminated, a fermentation process for the dextranase is enlarged, and the cost is reduced to the greatest extent.
Owner:GUANGDONG PROVINCIAL BIOENGINEERING INST (GUANGZHOU SUGARCANE IND RES INST)

Tool for mounting ejector-body

The invention discloses a tool for mounting an ejector-body. The tool comprises a handle, wherein a push rod seat which is movably inserted into an inner cavity of the ejector-body is arranged at one end of the handle; a first ejector block and a second ejector block which can move back and forth and are adaptive to the size of an inner hole on the side wall of the ejector-body are arranged on two sides of the push rod seat below the handle; a compression spring is arranged between the first ejector block and the second ejector block; a plug screw which jointly lock the first ejector block, the compression spring and the second ejector block is arranged on the push rod seat located on one side of the second ejector block; and push rods which are connected to the first ejector block and the second ejector block and perpendicularly protrude out of the top of the push rod seat for controlling the first ejector block and the second ejector block to move back and forth are arranged on the first ejector block and the second ejector block, respectively. The tool disclosed by the invention is simple in structure. By designing the push rod seat, which can be inserted into the inner cavity of the ejector-body, with stretchable ejector blocks, the ejector-body is quickly, simply and conveniently mounted by locating by virtue of the ejector blocks and the inner hole on the side of the ejector-body.
Owner:GUANGXI YUCHAI MASCH CO LTD

A preparing method of a cassava polysaccharide-iron complex

The invention relates to a preparing method of a cassava polysaccharide-iron complex. The method includes subjecting cassava starch to oxidative degradation by utilizing hydrogen peroxide to obtain anapplicable oligosaccharide solution; then adding dropwise an iron trichloride solution and a sodium hydroxide solution into the oligosaccharide solution to perform a complexing reaction to obtain a cassava polysaccharide-iron complex synthesis solution; performing filtration to remove water-insoluble impurities to obtain a cassava polysaccharide-iron complex solution; desalting and concentratingthe solution by adopting an ultrafiltration membrane process; and subjecting a product to spray-drying or vacuum evaporation drying, and crushing to obtain a cassava polysaccharide-iron complex product. The hydrogen peroxide is adopted to perform oxidative degradation on the cassava starch so as to replace previous acid-method or enzyme-method degradation processes, and therefore generation of a side product that is glucose in the method is significantly reduced than that in acid methods, a higher yield of applicable oligosaccharide is obtained, and the degradation time is greatly shortened than that of enzyme methods, thus reducing the production cost. Sodium chloride removal utilizing an ethanol or methanol solvent is replaced, thus avoiding use of flammable and combustible substances such as ethanol or methanol and eliminating hidden safety risks. The prepared cassava polysaccharide-iron complex can be used as an iron supplementing agent for livestock and poultry.
Owner:GUANGXI RES INST OF CHEM IND CO LTD

Centrifugal fan

The invention discloses a centrifugal fan which comprises a fan shell, a wind collection ring, an impeller and a motor, wherein the fan shell is internally provided with the wind collection ring and the impeller, the motor is arranged outside the fan shell, an output shaft of the motor is connected with the impeller, and a first dripping pan and a second dripping pan are respectively arranged at the front side and the rear side of the fan shell; the first dripping pan is positioned below the wind collection ring; the second dripping pan is positioned below the output shaft of the motor; and oil drain pipes which are communicated with the dripping pans are arranged below the first dripping pan and the second dripping pan. According to the centrifugal pan, after the centrifugal fan is used for conveying oily substance-containing medium for a long time, a great amount of oil stains flow out along with the front side and the rear side of the fan shell, and flows in the first dripping pan and the second dripping pan in the first time, so that pollution to the ambient environment can be avoided, the occurrence of safety accidents such as fire disaster can be prevented, and hidden production safety hazard can be eliminated.
Owner:SUZHOU TAIHU FAN MFG

Assembly tooling for hose throttle

ActiveCN103273297APrevent leakageAvoiding Consistency Issues in Locking PositionsMetal working apparatusSolenoid valveAssembly line
The invention discloses an assembly tooling for a hose throttle. The assembly tooling comprises an air tube, a distribution box, an air source, wires, a movable sliding block, a guide rail, a control switch, a guide rod, a positioning groove, a first air cylinder, a second air cylinder, a time solenoid valve and a tooling table frame capable of holding the parts. The solenoid valve is connected with and controls actions of the first air cylinder and the second air cylinder, the guide rod is fixed with the movable sliding block, the guide rod aligns to the positioning groove and performs guiding, the first air cylinder is connected with the movable sliding block, the movable sliding block is mounted on the guide rail and can move along the guide rail, and the second air cylinder is perpendicular to the first air cylinder. By means of the assembly tooling, the production efficiency is high, the product quality can be guaranteed, and potential production safety hazards can be eliminated.
Owner:ANHUI ZHONGDING KEUMAH AUTO HOSE & PIPE ASSEMBLY

Detecting system for rapid sealing of concentration sensor and method thereof

The invention discloses a detecting system for rapid sealing of a concentration sensor and a method thereof. The detecting system comprises a prism head shell of the concentration sensor to be detected, a measurement bracket, a camera, an atmospheric pressure cavity, an automatic air feeding pressurizing device, an air cylinder and a main controller; the camera, the air cylinder and the automaticair feeding pressurizing device are all electrically connected with the main controller; the method of the system comprises the step that the main controller performs data analysis and comparison on atest image which is shot and uploaded by the camera and an initial image, and judges whether the sealing of the concentration sensor is qualified or not according to the data analysis and comparisonresult; all test data are recorded automatically; the automation degree is high; the manual cost is reduced; meanwhile, the test time is shortened; the production efficiency is improved; and the production potential safety hazard is reduced.
Owner:湖南楚一机电有限公司

Hydrogen gas recovering device of intermediate frequency furnace

The invention discloses a hydrogen reclaiming device for a medium frequency furnace, and relates to a hydrogen reclaiming device for the medium frequency furnace for producing tungsten and molybdenum. The hydrogen reclaiming device for the medium frequency furnace comprises the medium frequency furnace, and a water seal which is used for isolating hydrogen exhausted out of the medium frequency furnace from ambient air, and also comprises a gas-water separator which is used for removing the moisture in the hydrogen exhausted out of the water seal, and a hydrogen reclaiming processing system, wherein the medium frequency furnace, the water seal, the gas-water separator and the hydrogen reclaiming processing system are annularly connected with each other in turn through pipelines. The water seal in the hydrogen reclaiming device for the medium frequency furnace not only is used for isolating the hydrogen exhausted out of the medium frequency furnace from the ambient air, but also has the function of explosion protection and pressure relief; the gas-water separator is used for separating the moisture in the hydrogen exhausted out of the water seal; and the hydrogen reclaiming processing system reclaims the hydrogen which is subjected to gas-water separation by the gas-water separator, conveys the hydrogen to the medium frequency furnace for use, and has the functions of energy conservation and consumption reduction.
Owner:盛华伟

All-water-based rubber treating agent for shoe making industry

The invention discloses a full-water-based rubber treating agent for the shoe making industry. The treating agent the following raw materials in percentage by weight: 95%-99% of deionized water, 0.01%-0.04% of hydrophilic chlorinated rubber resin, 0.01%-0.04% of hydrophilic vinyl chloride-vinyl acetate resin, 0.01%-0.04% of modified organic acid, 0.01%-0.04% of inorganic acid, 0.5%-2% of an organic silicon surfactant, 0.5%-2% of a polysiloxane wetting agent and 0.01%-0.04% of an indicator. Modified aids with high adherence are introduced, the materials are dissolved for 1-2 hours under constant-speed stirring, so that the dispersing performance of the raw materials in polymer emulsion is modified, the surface treatment effect on rubber is improved, a full-water-based system is adopted, the problem of environmental pollution caused by the product is solved, the production cost is reduced, potential production safety hazards are eliminated, the treatment effect on rubber materials is good, and the later tension is greater than 4.5 kg / cm.
Owner:南宝树脂(佛山)有限公司

Method for removing sodium chloride from cassava starch polysaccharide-iron complex liquid

The invention relates to a method for removing sodium chloride from cassava starch polysaccharide-iron complex liquid. The method comprises the following steps: A, adding cassava starch and water intoa reaction kettle, heating and regulating pH value, adding hydrogen peroxide solution to degrade the cassava starch, so as to obtain oligosaccharide solution with the weight-average molecular weightof 3-27KDa, then adding ferric trichloride solution and alkali, and carrying out complex reaction, so that cassava starch polysaccharide iron liquid is obtained; B, carrying out ultrafiltration on thecassava starch polysaccharide iron liquid obtained in the step A, and intercepting micromolecular cassava starch polysaccharide iron complex with the molecular weight of 2.5-200KDa to remove part ofsodium chloride; C, carrying out nanofiltration on permeate liquid obtained in the step B, and intercepting micromolecular cassava starch polysaccharide iron complex with the molecular weight of 200 Da by virtue of a nanofiltration membrane to remove sodium chloride; and D, mixing interception liquids obtained in the steps B and C, and carrying out spray drying, so that solid cassava starch polysaccharide iron complex is obtained, and nanofiltration permeate liquid can be directly discharged. The method provided by the invention has the advantages that technology is simple, energy conservationand environmental protection are realized, conditions are mild, and continuous production can be easily realized; concentration of sodium chloride in the cassava starch polysaccharide-iron complex liquid can be lowered; and recovery rate of the cassava starch polysaccharide iron complex is higher than 99%; and removal rate of sodium chloride is higher than 98%.
Owner:GUANGXI RES INST OF CHEM IND CO LTD

Purifying device and method decarbonizing nitric acid industry tail gas to extract N2O

The invention relates to the technical field of chemical substance recycling and provides a purifying device and method decarbonizing nitric acid industry tail gas to extract N2O. The decarbonizing purifying device comprises a dryer provided with water-removing absorbent and pressure swing adsorption equipment provided with decarbonizing absorbent. The method includes: using a washing tower to wash raw material gas, using a buffer tank to remove free moisture in the raw material gas, using first compression cooling device to pressurize the raw material gas, using the dryer to dehydrate the raw material gas, and using the pressure swing absorption equipment to remove non-polar gas in the raw material gas. The method has the advantages that the physical immunity removing and high-pressure throttling refrigeration rectification process is used; compared with a method chemically decarbonizing other tail gas to recycle N2O, the method can avoid waste alkaline liquid secondary pollution and is low in cost and convenient and safe to operate.
Owner:杨刘月

Method for removing chlorate in electrolytic circulation light salt brine

The invention relates to the technical field of water treatment, particularly to a method for removing chlorate in electrolytic circulating light salt brine. The method comprises the following step: adding acetaldehyde into electrolytic circulating light salt brine without adding sulfite. The process provided by the invention has the advantages of high decomposition efficiency, low consumption andsimple process.
Owner:鄂尔多斯市瀚博科技有限公司

Construction method for constitutive expression engineering bacteria of dextranase and preparation method for enzyme

The invention discloses a construction method for constitutive expression engineering bacteria of dextranase and a preparation method for enzyme. The construction method for the constitutive expression engineering bacteria comprises the following steps of: (1) inserting an obtained gene in a multi cloning site of an expression vector pGAPZalphaA to construct a recombinant plasmid pGAPZalphaA-dex;and (2) linearly transforming the recombinant plasmid to Pichia pastoris KM71H, and screening positive clone bacteria. The engineering bacteria are used in a preparation method for the dextranase. Bythe invention, the gene of the dextranase is effectively expressed in the Pichia pastoris successfully, a cheap carbon source is taken as a raw material, flammable and explosive methanol is not needed in the fermentation process, potential production safety hazards are eliminated, a fermentation process for the dextranase is enlarged, and the cost is reduced to the greatest extent.
Owner:GUANGDONG PROVINCIAL BIOENGINEERING INST (GUANGZHOU SUGARCANE IND RES INST)

Preparation method of cassava polysaccharide iron

The invention relates to a method for preparing cassava polysaccharide iron. The method is to oxidize and degrade cassava starch with hydrogen oxide to obtain an applicable oligosaccharide solution, and then add ferric chloride and sodium hydroxide solution dropwise to perform a complex reaction to obtain cassava polysaccharide. The iron synthesis solution is then filtered to remove water-insoluble impurities to obtain cassava polysaccharide iron solution, which is then desalinated and concentrated by ultrafiltration membrane technology, spray dried or vacuum evaporated, dried and crushed, and finally cassava polysaccharide iron products are obtained. The present invention uses hydrogen peroxide to oxidize and degrade cassava starch to replace the previous acid or enzymatic degradation process, which not only can significantly reduce the generation of by-product glucose than the acid method, obtain a higher yield of applicable oligosaccharides, and is more efficient than the enzymatic method. The degradation time is greatly shortened, thereby reducing production costs; it also replaces the previous ethanol or methanol solvent method to remove sodium chloride, avoids the use of flammable and explosive materials such as ethanol or methanol, and eliminates hidden dangers in production safety. The cassava polysaccharide iron prepared by the invention can be used as an iron supplement for poultry and livestock.
Owner:GUANGXI RES INST OF CHEM IND CO LTD

Injection lens automatic dyeing machine

The invention discloses an automatic dyeing machine for injection molding lenses, which comprises a frame, a transmission mechanism, a grasping mechanism, a lifting mechanism, a cleaning mechanism, a water cutting mechanism, a dyeing mechanism, a lens fixture and a programmable controller; a first cleaning area is formed in the frame , the water cutting area, the dyeing area and the second cleaning area; the lens fixture is set in the first cleaning area and the water cutting area through the cooperation of the transmission mechanism and the lifting mechanism, and is also set in the water cutting area and the water cutting area through the cooperation of the grabbing mechanism and the lifting mechanism. The dyeing area and the second cleaning area; the water cutting mechanism keeps the lens fixture in a static state during water cutting. During the water cutting process, the lens is still, and the water is cut by the water flow rising first and then falling to make the water cutting more thorough; the dyeing mechanism can cooperate with The dyeing car is assembled with the main dyeing tank and the dyeing auxiliary tank, so as to move the rack to replace the dyeing solution. The invention can realize the automation of the lens dyeing process, improve the dyeing efficiency of the lens, and improve the quality of the dyed lens.
Owner:艾普光学科技(厦门)有限公司

A fully automatic multi-stick punch system for punching book pages

The invention discloses a full automatic multi-map puncher system used for book page die punching. The system comprises a delivery platform, a punching platform, an automatic pushing device and an automatic page turning device, the punching platform and the automatic page turning device are arranged on the same side of the delivery platform, placing grooves which are used for placing books are reserved between the punching platform and the delivery platform and between the automatic page turning device and the delivery platform, and the automatic pushing device is arranged on the delivery platform. By means of the system, multi-map books can be embedded in the placing grooves to be delivered on the delivery platform through the automatic pushing device to the punching platform, page turning of the multi-map books can be achieved through the automatic page turning device in the delivery process, fully automatic production line die punching production of the multi-map books can be achieved, the labor intensity of operators is greatly reduced to save a large amount of labor force, production safety potential hazards are eliminated, the production speed is accelerated, and the die punching production efficiency of the multi-map books is greatly improved.
Owner:HESHAN ASTROS PRINTING

Opening device for electrode insulation shunting strips of solar cell module

An opening device for electrode insulation shunting strips of a solar cell module comprises a hand press, a clamp body, an insulation strip moving and fixing frame, an opening template, a tool clamping device and an opening blade. The insulation strip moving and fixing frame is placed on the clamp body, electrode shunting insulation strips are stacked in the insulation strip moving and fixing frame, and are subject to press fit through the opening template, the tool clamping device is fixedly mounted on a telescopic rod of the hand press, and the opening blade is mounted on the tool clamping device; a cutting edge is aligned with a tool setting groove, and when the insulation strip moving and fixing frame is located at the limit position, the opening blade is aligned with the opening positions of the electrode shunting insulation strips; mechanization of opening the electrode shunting insulation strips is achieved, manual opening errors are completely eradicated, opening accuracy is improved, mechanical opening production efficiency is high, and 15 to 25 strips can be cut at a time; and due to the device, workloads originally completed by three persons can be completed now within two hours, labor intensity is greatly reduced, and production safety hidden danger caused by manual opening pulling and scratching can be thoroughly eliminated.
Owner:JIANGSU ZHONGKE GUONENG PHOTOVOLTAIC TECH CO LTD

Plate and its manufacturing method

The invention relates to a plate-like part and a manufacturing method thereof. The plate-like part comprises a plate-like part body and reinforcing parts arranged inside the plate-like part body, and the outer surface of each reinforcing part is wrapped with a layer of medium. The manufacturing method includes the following steps that the outer surface of each reinforcing part is wrapped with the layer of medium; each reinforcing part is placed in a mold, and a first auxiliary structure and a second auxiliary structure are arranged at the two ends of each reinforcing part correspondingly and protrude out of the two end faces of the reinforcing part by a preset length in the axial direction of the reinforcing part; injection molding operation is carried out through the mold, so that the reinforcing parts are arranged inside the formed plate-like part body; and after injection molding, the auxiliary structures are removed. The plate-like part has the advantages of being good in pressure bearing effect, small in thickness and safe in production due to the adoption of the mode that the reinforcing parts are wrapped with the media in advance, the production cost is lowered, and the problem that a plate-like part obtained through existing production techniques is prone to shrinkage cracks is solved.
Owner:SHANGHAI HONGYAN RETURNABLE TRANSIT PACKAGINGS CO LTD

Filling head, carbon dioxide cracker and carbon dioxide cracker unit

The invention discloses a filling head, a carbon dioxide cracker comprising the filling head, and a carbon dioxide cracker unit. The filling head comprises a shell, wherein an axial anode, a central electrode and an axial cathode are arranged in the shell; the axial anode is connected to a detonating device; and the detonating device, the central electrode and the axial cathode are successively connected in series. The filling head disclosed by the invention can eliminate the production potential safety hazard of an electrified tube body, and safe detonation is achieved.
Owner:CCTEG CHINA COAL RES INST

Jacquard automatic edge separation screen cloth and manufacturing method thereof

PendingCN113802261AIntegrity of braid structureComplete and stable physical propertiesWarp knittingEngineeringWool
The invention discloses a jacquard automatic edge separation screen cloth, and belongs to the technical field of textile. The jacquard automatic edge separation screen cloth comprises a screen cloth body, the screen cloth body is integrally woven by jacquard warp knitting equipment and at least comprises at least two edge separation cloth, each edge separation cloth comprises a ground comb layer, a jacquard layer and edge sealing common layers, and at least one pair of edge sealing common layers are adjacently and longitudinally distributed on one side of the edge separation cloth. Under the condition that complete separation is not needed, the adjacent edge sealing common layers are connected in a staggered mode through a single yarn; under the condition that the length of the screen cloth needs to be shortened, at least one pair of edge sealing common layers which are formed by connecting single yarns in a staggered mode can be transversely arranged on the edge dividing cloth and are transversely distributed on the edge dividing cloth; and when the screen cloth needs to have a certain thickness during design, a wool high layer can be arranged on the edge dividing cloth.
Owner:信泰(石狮)科技有限公司

Process for chemical synthesis of 2-(cyanomethyl) thio acetyl chloride

A method for preparing 2-[(cyanomethyl)thio]acetyl chloride, taking 2-[(cyanomethyl)thio]acetic acid potassium salt and bis(trichloro methyl)carbonate as stock, putting them into organic dissolvent for reaction under the effect of catalyst for 8-16 hours, the temperature is -5~60 DEG C, separating and purifying to get the product.The consumption of chlorizating agent in said chemosynthesis method reduces greatly for the use of bis(trichloro methyl)carbonate, which can reduces the production cost and eliminates the potential safety hazard from the preparing source, and considerably decreases the yield of three wastes and increases the yield of products and promotes the quality as well; the dissolvent can be recovered which decreases pollution and production cost.
Owner:ZHEJIANG UNIV OF TECH

Purification method of antioxidant rosmarinic acid for tobacco

Belonging to the technical field of tobacco additives, the invention discloses a purification method of an antioxidant rosmarinic acid for tobacco. The purification method is carried out according to the steps of: (1) performing primary purification: first passing a rosmarinic acid-containing extraction solution A through a 30nm inorganic membrane, then passing it through an organic spiral-wound membrane with molecular weight cut-off of 3000, thus obtaining the filtrate B; (2) making sample loading preparation: subjecting the filtrate B to reverse osmosis membrane concentration to obtain a concentrated sample C; (3) conducting fine purification: carrying out chromatographic separation on the concentrated sample C by a gel column and collecting rosmarinic acid fraction; and (4) further concentrating and purifying the collected rosmarinic acid fraction by a pressure reduction distillation method and a recrystallization method in the prior art so as to make the rosmarinic acid content reach 80%-95%. The method provided in the invention is simple, safe, pollution-free, and is easy to implement.
Owner:HUBEI CHINA TOBACCO IND
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