30results about How to "Easy and economical to operate" patented technology

The present invention provides a refrigeration door, and method for making the same, for controlling condensation, providing thermal insulation, with a desired amount of visible transmittance, without using electricity to heat the door. The energy-free refrigeration door of the present invention includes a door frame housing and an insulating glass unit comprising inner, middle and outer sheets of glass. A first sealant assembly disposed around the periphery of the inner and middle sheets of glass forms a first chamber between the inner and middle sheets of glass. A second sealant assembly disposed around the periphery of the middle and outer sheets of glass forms a second chamber between the middle and outer sheets of glass. A gas, such as krypton, air, or argon is held in the first and second chambers. The outer sheet of glass and inner sheet of glass each have an unexposed surface that faces the middle sheet of glass. A low emissivity coating is disposed on the unexposed surfaces of the inner and outer sheets of glass so that the glass door as a whole has a U value that prevents formation of condensation on the outer surface of the outer sheet of the glass door, without the application of electricity to heat the door, while also providing the desired evaporation rate of condensation from the inner side of the inner sheet of the glass door.

Process and apparatus for cooling free-flowing granulate is provided in which the granulate trickles from top to bottom by gravity in a fixed container with movable cooling surfaces attached internally.

The invention discloses a structure and a preparation method of a porphyrin compound containing a long chain alkyloxyphenyl group and a phenanthrene ring group. The above tetraphenanthroporphyrin derivative is generated from long chain alkyloxyaryl aldehyde and phenanthrene ring conjugated pyrrole through a one-step reaction under the catalysis of propionic acid under heating refluxing conditions. The preparation method has the advantages of simple reaction steps, short reaction time, good selectivity and high yield.

A dust arrester includes a housing with air inlet and air outlet, wherein the ambient air containing dust particles can be introduced into the housing via the air inlet and discharged from the housing via the air outlet. The dust arrester further includes a water trough placed in the bottom of the housing and a chaos effect generator including a nozzle and a material. The nozzle can spray water supplied from the water trough. The water sprayed interacts with the material to generate a chaos condition, so that the dust particles can be removed from the introduced air under the chaos condition.

A coating method for a work piece includes the steps of: coating a coating film as a base color layer on a treating surface of the work piece, wherein the coating film has a predetermined color provided thereon; coating a first transparent protective layer on the coating film to protect the coating film; attaching a sticker layer having a predetermined character pattern on the first transparent protective layer under a water treatment such that the character pattern of the sticker layer is projected from the coating film to form a three-dimensional appearance; and coating a second transparent protective layer on the first transparent protective layer to sealedly enclose the sticker layer between the first transparent protective layer and the second protective layer so as to form a three-dimensional customary coating layer on the work piece.

The invention discloses a meso site arylamino monosubstituted porphyrin derivative and a preparation method thereof. The meso site arylamino monosubstituted porphyrin derivative comprises compounds 1a, 1b and 1c. The preparation method comprises the following steps: under argon protection, aromatic aldehyde and dibromo-1,19-dideoxy-3,8,12,17-tetraethyl-2,7,13,18-tetramethyl (biladien-a, c) generate the meso site arylamino monosubstituted porphyrin derivative under the catalytic action of p-toluenesulfonic acid. The porphyrin derivative provided by the invention can be used as an electron donor and has wide application prospects in the aspects of organic field effect tubes, molecular antennas, photo-energy converters, photoelectric conversion materials, molecular switches, molecular wires, organic solar cells, organic electroluminescent materials, nonlinear optical materials, molecular recognition, medicines and the like. The preparation method has the advantages of convenient and economical operation, good reaction selectivity, high yield, little pollution, and the like.

The invention discloses a pyridine fused norcorrole compound and a preparation method thereof. The pyridine fused norcorrole compound has a structural formula as shown in formula (1). The preparation method mainly comprises the following steps: weighing a certain amount of amido norcorrole and aromatic aldehyde, putting into a reactor, adding newly steamed toluene solution to the reactor, stirring at 110 DEG C for 5-8 h, and tracking the reaction by a chromatographic method; cooling to room temperature after the reaction is completed, separating directly with a chromatography column, eluting with methylene chloride and normal hexane as eluents, collecting second brown color product as a crude product, and concentrating and drying the crude product to obtain the compound. The pyridine fused norcorrole compound and the preparation method thereof have the following advantages: the reaction conditions are stable, the yield is high, the operation is simple and safe, and batch production can be realized.

The invention discloses preparation and application of a photocatalyst Ag / AgBr, and belongs to the technical field of nanocatalysts. According to the method, 1-butyl-3-methylimidazole bromine ([BMIM]Br) is prepared from N-methylimidazole and n-butyl bromide under certain conditions, wherein a preparation method comprises the steps that a certain amount of N-methylimidazole and a certain amount of n-butyl bromide are weighed and put into a round-bottom flask to be stirred and refluxed for a period of time in a high-temperature water bath to obtain faint yellow thick liquid, and 1-butyl-3-methylimidazole bromine ([BMIM]Br) which is collected after cooling has the very high catalytic activity in preparation of the photocatalyst Ag-AgBr by serving as a precursor.

The invention discloses a method for processing strobili of pinus massoniana. The method comprises the following steps: (1) fixation: spreading fresh strobili of pinus massoniana and sunning for 3-5 days; (2) degreasing: gathering and piling up the strobili fixed in the step (1), thoroughly watering the strobili, sealing the strobili with a film and bubbling for 3-5 days; and (3) airing: spreading and tedding the strobili bubbled in the step (2), wherein the strobili are turned 1-3 times every day and crack 5-7 days later; and collecting the seeds in time. According to the invention, through the preprocessing steps such as fixation, degreasing and the like for the strobili, the cracking time of the strobili of pinus massoniana is shortened, the opening is neat, and the seed yield is high.In the same conditions, the seed production time is shortened by 20-25 days, the method can be used for effectively responding to adverse weather such as low temperature, overcast and rainy days and the like in southern winter, and improving the strobili processing efficiency; and moreover, the operation is simple and convenient, the method is economical and practical, and the method is suitable for popularization and application in various scientific research and production institutions.

The invention discloses a (1R, 5R)-(-)-3-arylmethylene nopinone ultraviolet absorbent and a preparation method thereof. The ultraviolet absorbent is (1R, 5R)-(-)-3-(4'-hydroxylbenzylidene) nopinone, (1R, 5R)-(-)-3-(4'-hydroxyl-3'-methoxylbenzylidene) nopinone, (1R, 5R)-(-)-3-(2'-hydroxyl-3'-methoxylbenzylidene) nopinone, (1R, 5R)-(-)-3-(4'-chlorobenzylidene) nopinone or (1R, 5R)-(-)-3-(furan-2'-ylbenzylidene) nopinone. The preparation method of the ultraviolet absorbent comprises the following steps: beta-pinene which is cheap and easy to get is taken as a raw material; nopinone with a bicyclic structure similar with that of camphor is obtained through selective oxidation; and the aldol condensation is carried out on the nopinone and aromatic aldehyde with a different structure so as to synthesize the ultraviolet absorbent. The preparation method has the advantages of simple synthetic route, simplicity and convenience, and economy for operating, high yield, little pollution and the like, and the defect that the camphor has long synthetic route, and high cost and the like is overcome. The synthesized ultraviolet absorbent has the advantages of good ultraviolet absorption effect, wide range of ultraviolet absorption spectrum and good stability and the like, and thus, the ultraviolet absorbent can have an excellent application prospect in ultraviolet absorption.

The invention provides a carbon-based magnetic mesoporous composite microsphere and a preparation method thereof, belonging to the technical field of the preparation of an inorganic composite material. The diameter of the carbon-based magnetic mesoporous composite microsphere particle is 3-6 microns, the specific surface area of the microsphere is 270-315 m2 / g, the pore diameter is 4-8 nanometers, and the pore volume is 0.15-0.31 cm3 / g. The preparation method comprises the following steps: firstly, synthesizing an FexOy / carbon-based composite microsphere; and then, preparing the gamma-Fe2O3 / carbon-based magnetic mesoporous composite microsphere. The invention has the following obvious advantages: the FexOy / carbon-based composite microsphere is synthesized in one step, the activation and magnetization are synchronously carried out, and the obtained material has a simplex magnetic component, is in a mesoporous structure and has a large specific surface area. The preparation method of the mesoporous carbon-based magnetic composite microsphere is simple and easy to control magnetically, can be used as a micro adsorbent or magnetic targeted drug carrier, and has potential application value in delivery and separation processes.

The invention relates to a near-infrared BODIPY fluorescent dye and a preparation method thereof, which is synthesized by Knoevenagel condensation reaction of 2-formyl trisindene and BODIPY derivatives under the catalysis of p-toluenesulfonic acid and piperidine, and the maximum absorption and emission wavelengths Above 650nm in organic solvents. The preparation method has the advantages of simple reaction steps, mild reaction conditions, good selectivity and the like. This type of fluorescent dye has excellent photophysical properties such as high molar extinction coefficient, good solubility and photostability, and has good application prospects in cell imaging and biomarking.

The invention discloses equipment and a method for batch preparation of microcapsules. The equipment comprises a liquid supply container, wherein the liquid supply container is connected with a waterpump through a connecting pipe and is communicated to a rotary distributor; the upper part of the rotary distributor is connected with a fixed ring; the lower part of the rotary distributor corresponds to a receiving reaction vessel below the fixed ring; a plastic net is arranged inside the receiving reaction vessel; a Z-shaped plastic pipe communicated with the connecting pipe is arranged in an inner cavity of the rotary distributor; a motor is arranged on the side of the Z-shaped plastic pipe and is connected with a T-shaped shaft which extends inside a dosing short pipe together with the Z-shaped plastic pipe; two rotary distributing cross bars are connected onto the dosing short pipe; a plurality of tiny distributing holes are formed in the lower parts of the rotary distributing crossbars. The equipment disclosed by the invention has the advantages of simple flow, lower economic cost and capability of realizing batch production; the equipment can embed different thalli and enzymesand improve biological concentration; the prepared microcapsules can provide a good operation platform for production technologies and flows in the actual application field of microcapsule immobilization scientific experiments and chemical material production.

The invention relates to a Chinese medicinal preparation for treating cardiovascular and cerebrovascular diseases and its preparing process, wherein the preparation is prepared from red sage root, kudzu vine root and Chuanxiong rhizome through extracting and refining, charging medicinal auxiliary materials and mixing homogenously, finally making soft capsules and dripping pills.