The invention relates to a preparation method for high-purity
boric acid and nuclear-grade high-purity
boric acid, and belongs to the
fine chemical engineering technology field. The method comprises the following technological steps: first, industrial
boric acid is stirred with water, impurities of
calcium,
magnesium and
sodium are removed, and high-purity boric acid precursors are obtained after
solid-liquid separation; second, the high-purity boric acid precursors are dissolved in hot pure water and a boric acid solution containing H3BO3 with a concentration of 180g / L-280g / L is prepared, iron and heavy
metal are subjected to depth removal by utilization of composite additives, then
filtration, cooling
crystallization,
solid-liquid separation, washing and
drying are carried out, and the high-purity boric acid product is obtained. The high-purity boric acid product is dissolved in pure water, recrystallization is carried out for 1-2 times,
dehydration and
drying are carried out, and the nuclear-grade high-purity boric acid product is obtained. Through the preparation method, the high-purity boric acid products with different grades can be obtained, and the preparation method is advantaged by simple technology, easy operation and control, good reappearance, low production cost, and
environmental protection.