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33results about How to "Avoid complexation" patented technology

Grafted cyclodextrin

Thermoplastic polymer compositions, films, continues, closures, laminates can comprise a modified vinyl polymer said modified polymer having a moiety comprising a cyclodextrin compound. The cyclodextrin compound, locked into the polymer structure, can absorb impurities, permeants, or other undesirable volatile materials. The cooperation between the cyclodextrin grafted onto the thermoplastic polymer and the polymer structure can provide barrier properties to a film, web or other polymer structure. A permeant or a contaminant can be complexed or trapped within the polymer and held within the film or Web preventing the permeant or contaminant from passing into the interior of a container or enclosure.
Owner:VERDANT TECH LLC

Grafted cyclodextrin

Thermoplastic polymer compositions, films, continues, closures, laminates can comprise a modified vinyl polymer said modified polymer having a moiety comprising a cyclodextrin compound. The cyclodextrin compound, locked into the polymer structure, can absorb impurities, permeants, or other undesirable volatile materials. The cooperation between the cyclodextrin grafted onto the thermoplastic polymer and the polymer structure can provide barrier properties to a film, web or other polymer structure. A permeant or a contaminant can be complexed or trapped within the polymer and held within the film or Web preventing the permeant or contaminant from passing into the interior of a container or enclosure.
Owner:VERDANT TECH LLC

Mother solution of standard solution for chromatography of heavy metals in leather and preparation method of standard curve

The invention relates to a technology for fast determination of heavy metals in leather and particularly relates to a standard curve for fast determination of heavy metals in leather by X-ray fluorescence energy spectrum analysis and a mother solution of the standard solution, which is used for preparing the standard curve. The mother solution of the standard solution is prepared from a leather penetrating agent, phosphoric acid, nitric acid and the national standard solution of nine heavy metals. A method for preparing the standard curve comprises the following steps: (1) preparing the mother solution of the standard solution; (2) preparing a multi-gradient standard solution; (3) preparing a series of standard test samples of the heavy metals in the leather; (4) preparing circular sheets of the standard test samples to be tested of the leather; (5) detecting by X-ray fluorescence chromatography; (6) drawing the standard curve. The technology provided by the invention has the advantages that the detection precision of the nine heavy metal harmful substances in the leather can be improved to meet the requirements of a national standard, thus the advanced technology of the X-ray fluorescence chromatography can be applied to detection of the nine heavy metal harmful substances in the leather.
Owner:SICHUAN ENTRY EXIT INSPECTION & QUARANTINE BUREAU INSPECTION & QUARANTINE TECHN CENT

Method for synthesizing polysubstituted amino isoquinoline compound by cyclizing pyridine and alkyne under catalysis of rhodium

The invention discloses a method for synthesizing a polysubstituted aminoisoquinoline compound by cyclizing pyridine and alkyne under the catalysis of rhodium, which comprises the following steps: byusing a pentamethylcyclopentadienyl rhodium complex as a catalyst and a 2-aminopyridine derivative and an internal alkyne compound as raw materials, reacting in an organic solvent at 30-150 DEG C for1-24 hours, cooling the reaction solution after the reaction is finished, removing the organic solvent under reduced pressure; purifying the crude product through a silicon dioxide column, and elutingwith petroleum ether / ethyl acetate to obtain the pure polysubstituted aminoisoquinoline derivative. According to the method, a guide group (carbonyl) or a steric hindrance group (methyl) is introduced into the reaction to realize C-H bond activation and avoid the coordination effect of pyridine on the metal catalyst, and the regulation and control of the reaction activity and selectivity are efficiently realized through the regulation and control of the group with large steric hindrance. The obtained generation target products are high in selectivity, and the selectivity is 90% or above, byproducts are few, and the product separation cost is reduced, and the method is simple in synthesis process, mild in reaction condition and convenient for industrial production.
Owner:LANZHOU INST OF CHEM PHYSICS CHINESE ACAD OF SCI

Method for analyzing contents of fluorides in hazardous wastes

The invention provides a method for analyzing the contents of fluorides in hazardous wastes. According to the method, a pretreated sample is completely combusted in an enclosed space by adoption of anoxygen bomb combustion technology; one part of the fluorine element in the oxygen bomb is absorbed by absorption liquid in the oxygen bomb and the other part is absorbed by absorption liquid in a gasabsorption station through a gas form; the absorption liquid is combined to obtain fluoride extracting solution; and the extracting solution is treated to obtain to-be-tested sample solution. Fluorine ion series standard solution is prepared; and a standard curve is drawn for a negative logarithm (E(Mv)-log cF-(mg / L))of the concentration of fluorine ions via a potential value E. An ion chromatograph-fluoride ion selective electrode is utilized to measure the potential value of the to-be-tested sample solution; and the content of the fluorides is calculated via the standard curve according tothe measured potential value. The method is relatively high in test result correctness and is capable of greatly shortening the test time at the same time.
Owner:江门市崖门新财富环保工业有限公司

Gastrodin injection preparation and preparation method

The invention discloses a gastrodin injection preparation, which comprises the following components by weight: 5-10% of gastrodin, 0.01-0.1% of metal ion complexing agent, 0.6-1.2% of stabilizing agent, 1-2.5% of buffer and the balance of injection water. The invention also provides a preparation method of the gastrodin injection preparation. The gastrodin injection of the present invention can effectively stop the addition of visible foreign matter during a placing process of the gastrodin injection, the defective index of the visible foreign matter in a solution is reduced, the white point and white block precipitation are not generated, the expectation effect can be reached, thereby the treatment effect of gastrodin can be fully performed. The gastrodin injection preparation has the advantages of simple prescription, good stability, high clear degree, safe clinical usage, small adverse reaction and convenient industrial large batch production.
Owner:YANGZHOU ZHONGBAO PHARMA

Method for improving homogeneity of cement grinding aid

The invention relates to a method for improving the homogeneity of a cement grinding aid, belonging to the field of cement admixtures. The method mainly comprises the following steps: (I) a water treatment process; and (II) a compounding process for the grinding aid. The water treatment process comprises the following sub-steps: 1, feeding of a purifying agent; 2, sonic treatment; 3, filtration; and 4, thickening treatment of water. Parameters in the above sub-steps are that (1) the weight percentage of the purifying agent is 3 to 10 %; (2) ultrasonic frequency is 20-35 KHZ; (3) the weight percentage of a thickening agent is 2 to 10 %; and (4) time for sonic treatment is 10 to 30 min. The compounding process comprises the following sub-steps: adding water obtained after treatment by the process (I) into a container, dissolving a salt, and carrying out sonic treatment; and successively adding alcohol amine and industrial waste, carrying out stirring for 15 min and then carrying out sonic dispersion. The compounding process utilizes 10% to 20% of alcohol amine, 8% to 17% of the industrial salt, 20% to 30% of the industrial waste and 48% to 60% of water; and ultrasonic time in the process is 10 min to 30 min. The active ingredients of the grinding aid obtained in the invention are greatly improved, and the grinding aid is uniform and stable, does not settle, and has good application prospects.
Owner:北京丰乐宝科技有限公司 +1

Method for preparing trialkyl phosphate

The invention provides a method for preparing trialkyl phosphate, belonging to the chemical engineering field. The method comprises the steps of reacting by virtue of phosphorus oxyhalide and alcoholin an ice-water bath under the protection of inert gas, cooling a system to room temperature by taking ion exchange resin as a catalyst after the reaction, carrying out reduced pressure distillation to remove redundant alcohol and hydrochloric acid, further removing alcohol and acid in the system in one step by virtue of a bubbling method so as to obtain a trialkyl phosphate rough product, and carrying out reduced pressure rectification, so as to obtain a trialkyl phosphate purified product. By utilizing the catalyst, the compexing with trialkyl phosphate is avoided, so that the adverse effects caused by the complexing between a traditional catalyst and a product are effectively avoided, and the yield and purity of the product are increased; by further removing impurities in a bubbling manner, the impurities remained in the reduced pressure distillation process are effectively removed, so that the yield and purity of trialkyl phosphate are further increased; and the total yield of theproduct is more than 95.9%, and the purity of the product is more than 99.8%.
Owner:江苏中丽新材料有限公司

A method for improving the homogeneity of cement grinding aid

The invention relates to a method for improving the homogeneity of a cement grinding aid, belonging to the field of cement admixtures. The method mainly comprises the following steps: (I) a water treatment process; and (II) a compounding process for the grinding aid. The water treatment process comprises the following sub-steps: 1, feeding of a purifying agent; 2, sonic treatment; 3, filtration; and 4, thickening treatment of water. Parameters in the above sub-steps are that (1) the weight percentage of the purifying agent is 3 to 10 %; (2) ultrasonic frequency is 20-35 KHZ; (3) the weight percentage of a thickening agent is 2 to 10 %; and (4) time for sonic treatment is 10 to 30 min. The compounding process comprises the following sub-steps: adding water obtained after treatment by the process (I) into a container, dissolving a salt, and carrying out sonic treatment; and successively adding alcohol amine and industrial waste, carrying out stirring for 15 min and then carrying out sonic dispersion. The compounding process utilizes 10% to 20% of alcohol amine, 8% to 17% of the industrial salt, 20% to 30% of the industrial waste and 48% to 60% of water; and ultrasonic time in the process is 10 min to 30 min. The active ingredients of the grinding aid obtained in the invention are greatly improved, and the grinding aid is uniform and stable, does not settle, and has good application prospects.
Owner:北京丰乐宝科技有限公司 +1

Preparation method of purple sweet potato pigment

InactiveCN112442285AStable structureNo photothermal degradationSugar derivativesNatural dyesAcetic acidFreeze-drying
The invention discloses a preparation method of a purple sweet potato pigment. The method comprises the following steps: performing cleaning, airing and cutting. taking an acetic acid aqueous solutionas an extracting agent, carrying out crude extraction according to a solid-liquid ratio of 1: 4, carrying out freeze thawing treatment on the purple sweet potato strips twice, combining pigment crudeextracts, and carrying out vacuum concentration to obtain a pigment concentrated solution; treating the pigment concentrated solution with a graphene oxide dispersion solution, carrying out primary purification, and carrying out centrifugal separation to obtain supernatant; pre-treating and packing adsorption macroporous resin SP70 into a column, and injecting a supernate pigment liquid into a resin layer, wherein the sample loading flow rate is 3.0-3.5 BV/h; washing the resin layer after adsorption saturation with 2BV clear water, wherein an eluent is prepared from 70% ethanol and 0.5% acetic acid, the elution flow rate is 2.0-2.5 BV/h, and the elution volume is 5BV; and collecting eluate, and performing vacuum concentrating and freeze-drying to obtain a purple sweet potato anthocyanin pigment dry product. According to the method, an alcohol solvent is not used, the pigment extraction rate is increased through freeze thawing treatment, impurities such as proteins are removed throughthe adsorption effect of graphene oxide in the purification process, the anthocyanin complexing effect is avoided, the purification effect is improved, and the high-purity purple sweet potato anthocyanin pigment is obtained.
Owner:HUNAN TIANXIANG BIOTECHNOLOGY CO LTD +1
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