The invention relates to the field of
alloy grain
size measurement, and particularly discloses a method for measuring the uniformity of a nanocrystalline hard
alloy. The method comprises three steps of:
sample preparation, observation and statistics. The
sample preparation comprises mirror
polishing and metallographic
corrosion steps, wherein the metallographic
corrosion comprises the steps of: first-time WC
corrosion,
cobalt-phase corrosion and second-time WC corrosion. In the observation step, a field emission
scanning electron microscope is used, and a 20000-40000-time microscopic structurepicture is shot through back scattering
electron imaging. The statistics is characterized in that measurement
software is used for measuring the grain size of each grain of the
alloy, counting data and drawing a grain size
distribution diagram to represent the uniformity of the alloy. The method is suitable for measuring the uniformity of the WC / Co hard alloy taking Co as a binding phase, and isfurther suitable for measuring the uniformity of the nanocrystalline hard alloy taking any one of cubic phase
carbide, TiC and Ti (C.N) as an inhibitor. By applying the method, the measurement of theuniformity of the nanocrystalline hard alloy can be simply and quickly completed, and the
image resolution can be remarkably improved.