The invention discloses a preparation method and application of SiO2-APTES-La composite
aerogel, and belongs to the technical field of
fuel oil processing. The preparation method comprises the steps of mixing absolute ethyl
alcohol, tetraethoxysilane and deionized water to obtain a solution A, carrying out magnetic stirring
hydrolysis under acidic conditions, adding
ammonia water to adjust the pHvalue, slowly adding APTES, standing to obtain a gel, aging, crushing, carrying out
solvent replacement to dissolve
lanthanum nitrate in absolute ethyl
alcohol to obtain a solution B, standing the
mixed solution A and the
mixed solution B, and
drying the
mixed solution A and the mixed solution B under normal pressure to obtain the SiO2-APTES-La composite
aerogel. According to the invention, a
fixed bed adsorption device is quantitatively filled with the SiO2-APTES-La composite
aerogel, thiophenic
sulfide-containing simulated
gasoline is injected at normal temperature and a certain
airspeed, the adsorbed simulated
gasoline is collected at an outlet at the lower end of a reaction device, and chromatographic analysis is carried out. The preparation method of the SiO2-APTES-La composite aerogel adsorbent is simple, the cost is low, the adsorbent can be repeatedly used, the economic benefit is high, the environment-friendly effect is achieved, the adsorption condition is mild, and the requirement for adsorption equipment is low.