35results about How to "Condition control is simple" patented technology

The invention relates to an ultraphonic elastic imaging body model comprising polyacrylamide hydrogel and a scatterer, wherein the polyacrylamide hydrogel forms a reticular structure to wrap the scatterer. The elasticity (or the rigidity) of the ultraphonic elastic imaging body model can be freely regulated within a larger range by regulating the concentration of an acrylamide monomer and the sound attenuation coefficient can be changed to accord with the standard of ultraphonic elastic imaging by regulating the proportion of the scatterer.

The invention relates to an energy-saving type two-tower stripping method for treating waste water containing acid gas and ammonia, which belongs to the technical field of waste water treatment. The method comprises the following steps of: dividing the waste water which is to be treated and contains acid and ammonia into a cold part and a hot part, and respectively introducing the cold part and the hot part into a deacidification tower from the upper part and the middle upper part of the deacidification tower of a stripping type waste water treatment device, wherein acid gas is introduced into an acid recoverer after being stripped from the top of the deacidification tower; collecting kettle liquid waste water from the bottom of the deacidification tower; introducing the kettle liquid waste water into a deamination tower from the middle upper part of the deamination tower so that ammoniac steam is stripped from the top of the deamination tower; meanwhile, collecting kettle liquid from the bottom of the deamination tower. The heat used by a tower kettle reboiler is derived from the ammoniac steam extracted from the deamination tower; the sulfur residue quantity of the treated waste water is lower than 50mg / L, and the total ammonia content is lower than 100mg / L; and the method provided by the invention has the advantages of simple and easily controlled process, mature technology, low processing cost and energy saving and can be widely applied to various occasions for treating the waste water containing acid and ammonia.

The invention provides a monascus mutant strain, namely Monascus purpureus yang Ty622, and a method for preparing monascus yellow pigment by submerged fermentation of the strain. The method comprises the steps of: selection and breeding of strain, seed culture, large-capacity tank fermentation and extraction of monascus yellow pigment, wherein the seed culture and the fermentation are implemented in a specifically manufactured culture medium, and multistage fermentation is performed in a large-capacity pot fermentation tank, followed by fermentation; the technological conditions of fermentation are as below: the temperature is from 32 to 36 DEG C, the stirring rotational speed is 200 to 400r / min; the ventilation quantity at earlier stage is from 400 to 500L.min and is then regulated to 500 to 600L.min at middle / later stages. The invention further provides an article prepared according to the above method. The preparation method according to the invention has simple technology and is easy for industrialized production, and the resultant fermented liquid has high content of monascus yellow pigment and low content of citrinin.

The invention relates to a method for preparing n-tetradecane under normal pressure, which comprises the following steps of: (1) mixing glacial acetic acid, zinc powder and alkyl halides of the same grade; (2) dripping hydrochloric acid into the mixture, refluxing, precipitating and separating to obtain a liquid crude product of the n-tetradecane; (3) washing by using acid and alkali to obtain purified liquid of the n-tetradecane; and (4) distilling under reduced pressure to obtain a finished product of the n-tetradecane. The production process is simple, the zinc powder, bromoalkane and the hydrochloric acid are added at the temperature of below 110 DEG C under normal pressure, high-temperature and high-pressure reactions are not performed, and the process has low requirement on production equipment and low danger. In the method, a one-step synthetic mode of reducing the alkyl halides by using hydrogen atoms is adopted, and diethyl ether is replaced by sulfuric acid to remove unsaturated hydrocarbons and alcohols, the safety factor is high, and the condition is easy to control.

The invention provides a process for preparing [(phenylsulfonyl) difluoromethyl] trimethyl silane (TMS-CF2SO2Ph) which comprises, in organic solvent at -78 deg. C to room temperature and at the presence of C1-C4 lithium alkyl or 4-dimethylamino, using difluoromethyl phenyl sulfone or difluoro halogenated methylbenzene sulfone as raw material, and reacting with trimethylchlorosilane. The invention realizes easy operation, and the prepared [(phenylsulfonyl) difluoromethyl] trimethyl silane can catalyze carbonyl compounds for difluoro methylation reaction.

The invention relates to a method for detecting photochemical activity of a carbon nano tube by utilizing a transient absorption spectrum technology and belongs to the field of photochemical activity detection of carbon nano tubes. The method comprises the following steps: a, preparing aqueous solution of the carbon nano tube, ultrasonically treating the aqueous solution of the carbon nano tube, standing, and taking supernatant liquid of the aqueous solution of the carbon nano tube as a detection object; b, analyzing photochemical properties of the aqueous solution of the carbon nano tube under illumination conditions by utilizing a laser flash photolysis instrument; and c, verifying and analyzing a characteristic peak of the transient absorption spectrum of the carbon nano tube obtained by the laser flash photolysis instrument in step b by utilizing a pulse radiolysis device. According to the detection method, aiming at a special carbon-based nano material such as the carbon nano tube, the photochemical activity particles in the aqueous solution can be conveniently and reliably detected, the carbon nano tube is insensitive to interference of an external environment, and a carbon nano tube sample is not required to be excessively modified and treated in the earlier stage.

The invention relates to a process for synthesizing difluoro methanol product yield including difluoro methanol from difluoro-methylation reaction of ((phenylsulfonyl) difluoromethyl) trimethyl silicane adding carbonyl compound (aldehyde or ketone), the process consists of fluorinion-initiated (phenylsulfonyl) difluoromethyl methylation reaction and magnesium-participated reduction de-sulfonation reaction, The advantages of the disclosed process include simple process, high yield, economy and reaction environment friendliness.

The invention relates to an ultraphonic elastic imaging body model comprising polyacrylamide hydrogel and a scatterer, wherein the polyacrylamide hydrogel forms a reticular structure to wrap the scatterer which is powered graphite having a particle size of 20 micron or less. The elasticity (or the rigidity) of the ultraphonic elastic imaging body model can be freely regulated within a larger range by regulating the concentration of an acrylamide monomer and the sound attenuation coefficient can be changed to accord with the standard of ultraphonic elastic imaging by regulating the proportion of the scatterer.

The invention discloses a method for recycling treatment of a rinsing solution during production of a bleaching powder concentrate. The method comprises the following steps: (1) adding a pickling solution into the rinsing solution at 25-80 DEG C while stirring to ensure that the pH value is equal to 4-5, and stirring uniformly to obtain an orange red sticky substance; (2) adding the pickling solution while stirring to ensure that the orange red sticky substance becomes block liquid; (3) adding the rinsing solution while stirring to ensure that the pH value is equal to 7-7.5 and the black liquid gradually becomes liquid containing orange red particles and generates chlorine, stirring continuously, and collecting chlorine; and (4) filtering the liquid containing the orange red particles to obtain a colorless, clarified and transparent neutral liquid and a red brown filter cake, washing the filter cake, and drying, grinding and firing to obtain iron oxide red. The method disclosed by the invention can be used for treating two types of industrial wastewater, and iron oxide red and chlorine are obtained at the same time, so that the method is green and environment-friendly. The method is short in treatment time, simple to operate, low in energy consumption, and suitable for treatment and production manners under industrial conditions.

The invention discloses a composite lithium ion electrode material. A preparation method of the electrode material comprises the steps: taking FeC2O4.2H2O, Li2CO3, NH4H2PO4, a Mn powder and a Ce powder as raw materials, preparing the raw materials according to the atomic ratio of Li1-xCexFe1-yMnyPO4 and mixing, then carrying out ball milling, keeping the temperature of the mixture after ball milling constant for 5 hours or more in the environment with the temperature of 300 DEG C, keeping the temperature constant for 10 hours or more in the environment with the temperature of 600 DEG C, allowing the mixture to undergo a reaction and sintering at high temperature, naturally cooling, collecting a powder, and thus obtaining the product.

The invention discloses a treatment method of an ultraviolet-resistant aromatic high-performance fiber. The method comprises the steps that an ultraviolet-resistant treating agent is prepared into a treating solution with the bath ratio of 15-50 to 1 according to the fiber weight of 1.5-5%, even stirring is performed, the pH of the ultraviolet-resistant treating agent is regulated to be 5-7, then the aromatic high-performance fiber is put in the ultraviolet-resistant treating agent, and treatment is performed according to the steps and conditions of a conventional high temperature and high pressure dyeing process (shown in the description). By the adoption of the treatment method, the aromatic high-performance fiber can play a lasting ultraviolet-resistant function, can also synchronously achieve corresponding fiber dyeing, the strength retention rate of the fiber subjected to ultraviolet irradiation is effectively improved, an operation process is simple, and the conditions are easy to control. The method is suitable for industrialized production.

The invention discloses a method for preparing fluorescent powder with controllable luminescence characteristics and the obtained fluorescent powder. The preparation steps are: obtaining (Eu 3+ x+y A + y m 1‑x‑2y ) 2 SiO 4 Phosphor powder, the phosphor is obtained by microwave reduction method to obtain Eu 2+ , Eu 3+ Double-doped silicate phosphor——(Eu 2+ x Eu 3+ y A + y m 1‑x‑2y ) 2 SiO 4 . The preparation process of the present invention is simplified, fast, low energy consumption, process parameters are easy to control and adjust, condition control is simple and the adjustable range is large, and the controllable modulation of the light output performance of the fluorescent powder can be realized to meet different lighting requirements. Phosphor powder has a short production cycle, high production efficiency, and low requirements for equipment and conditions, which is conducive to the realization of material device integration and integrated design, so it has the potential for industrialization and mass production.