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37 results about "Ferromagnetic nanoparticles" patented technology

Aqueous soluble ferrimagnets stabilized by block copolymers

The present invention relates to a water-soluble polymer complex that includes a water-soluble block copolymer and a magnetic nanoparticle, wherein the water-soluble polymer complex has a nonzero net magnetic moment in the absence of an applied magnetic field at ambient temperatures. The water-soluble block copolymer is preferably a diblock or triblock copolymer and the magnetic nanoparticle is preferably a ferrimagnetic or ferromagnetic nanoparticle. The water-soluble complexes may be derivatized with reactive groups and conjugated to biomolecules. Exemplary water-soluble polymer complexes covered under the scope of the invention include PEG112-b-PAA40 modified CoFe2O4; NH2-PEG112-b-PAA40 modified CoFe2O4; PNIPAM68-b-PAA28 modified CoFe2O4; and mPEG-b-PCL-b-PAA modified CoFe2O4.
Owner:IBM CORP

Preparation of ferromagnetic nanoparticle and application thereof in extraction and removal of micro-plastics

The invention belongs to the technical field of environmental pollution research and environmental protection technology, and in particular relates to a ferromagnetic nanoparticle and preparation thereof and an application in removal of micro-plastics in the environment based on the nanoparticle. The surface of an iron nanoparticle is modified with methoxysilane to form siloxane bonds (-Si-O-Si-), and alkyl chains face outward to form a hydrophobic iron nanoparticle. The ferromagnetic nanomaterial is applied to extract and remove micro-plastics in an environmental sample. The method has wide adaptability, reliable method, simple operation and relatively low cost, can be used for extracting and identifying micro-plastics in environmental pollution (water, soil, sediment) researches, can be used for removing micro-plastics in environmental water body, sewage, and drinking water, provides a new solution for the micro-plastic environmental pollution field research and the environmental management, and is suitable for further development and application.
Owner:YANTAI INST OF COASTAL ZONE RES CHINESE ACAD OF SCI

Novel magnetic sealing material and preparation method thereof

InactiveCN107446546AUniform and stable dispersionSolve the problem of not being able to disperse existing magnetic particles into the carrier liquidOther chemical processesMagnetic liquidsMicroparticleFluorocarbon
The invention discloses a novel magnetic sealing material, which is formed by nucleus-shell-grafting group particles. The nucleus is ferromagnetic nanoparticles with the particle size being 5 to 100nm; the shell is an inert metal oxide layer or a resin layer covering the surface of the nucleus; hydroxide radical, carboxyl, amidogen or hydrosulphonyl on the shell can be chemically grafted with groups; the thickness of the shell is 1 to 100nm; the grafting group is a fluorocarbon chain grafted on the inert metal oxide layer or the resin layer; the cover degree of the fluorocarbon chain on the shell surface is 5 to 95 percent. The invention provides the novel magnetic sealing material used as magnetic particles in magnetic fluid, so that the magnetic particles can be directly, stably and uniformly dispersed into carrier liquid, and cannot be settled or agglomerated, and the magnetic sealing effect of the magnetic fluid is better.
Owner:SICHUAN UNIVERSITY OF SCIENCE AND ENGINEERING +1

Method for preparing magnetic nanoparticles with improved quality

The invention discloses a method for preparing magnetic nanoparticles with improved quality. The method comprises the following steps: weighing a soluble trivalent iron salt and sodium acetate to be dissolved in ethylene glycol so as to obtain yellow transparent liquid; adding trisodium citrate, a polyvinylpyrrolidone dispersing agent and an alkaline additive, and mechanically stirring at a room temperature; and adding the obtained mixed liquid into a reactor to be reacted, naturally cooling the product, washing with ethanol and water, and performing vacuum drying, thereby obtaining the magnetic nanoparticles. According to the method for preparing magnetic nanoparticles disclosed by the invention, ferroferric oxide magnetic nanoparticles are synthesized by a solvothermal method, synthesisis completed at a time under high temperature and high pressure, later crystallization treatment is not needed, the obtained powder is narrow in particle size distribution and pure in components, andanhydrous sodium acetate with excellent electrostatic stability is selected as the alkaline additive, so that agglomeration of the magnetic nanoparticles is effectively avoided. Therefore, the prepared ferroferric oxide magnetic nanoparticles are excellent in stability and have excellent monodispersity, superparamagnetism and particle size uniformity in water.
Owner:成都华田生物技术有限公司

A magnetic composite-cyanide decomposing enzyme composite nanoparticle, its preparation method and application, and its method for treating electroplating wastewater

The invention discloses a magnetic compound-cyanide decomposing enzyme composite nanoparticle, its preparation method and application, and a method for treating electroplating wastewater by using it. The raw materials for making the composite nanoparticle include: spinel ferromagnetic nanoparticle, magnetic oxide Nanoparticles, SiO 2 Nanoparticles, cyanide decomposing enzyme, first polymer compound, second polymer compound, silane, amine compound, nucleoside monophosphate disodium salt, first inorganic metal salt, second inorganic metal salt; The stone ferromagnet is modified by amino groups, by wrapping SiO 2 The magnetic oxide nanoparticles are modified by epoxy groups, and then the metal adsorption coupling is carried out through the first inorganic metal and the enzyme, which increases the way and amount of enzyme coupling, and stabilizes the enzyme activity and applicable pH range and temperature range. At the same time, the magnetic substance can be used to absorb heavy metal ions or dyes and achieve the effect of decomposing cyanide, reducing the amount of flocculant used and the amount of sludge after treatment.
Owner:山东普尼奥水处理科技有限公司

A kind of magnetic composite nanomaterial and its preparation method and application

The invention belongs to the field of nanometer materials, and specifically discloses a magnetic composite nanometer material, a preparation method and an application thereof. The raw materials for the preparation of the magnetic composite nanomaterial include Fe 3 o 4 Ferromagnetic nanoparticles, cellulose acetate and glyceryl trioleate, by modifying the surface of magnetic nanoparticles of cellulose acetate, and fixing glyceryl trioleate in the microporous structure of cellulose acetate; by controlling the ratio of solvent addition and temperature and other conditions, magnetic composite nanoparticles can be prepared. The preparation method of the magnetic composite nanomaterial is a chemical co-precipitation synthesis technology, which has the advantages of simple preparation process and equipment requirements, high stability of the produced material, and the obtained magnetic composite nanoparticle not only has a large specific surface area, but also has the advantages of being resistant to pollutants. The adsorption efficiency is fast, and it can be used for the adsorption of organic matter in sewage treatment; and there is less superparamagnetic interference to the material itself, and it can be quickly recovered under an external magnetic field, avoiding environmental pollution.
Owner:SOUTH CHINA INST OF ENVIRONMENTAL SCI MEP

Polylactic acid shell of electric energy metering box and preparation method of polylactic acid shell

ActiveCN114806117AHas a guiding roleGood energy storage and temperature regulationActive agentInjection molding machine
The invention discloses a polylactic acid shell of an electric energy metering box and a preparation method of the polylactic acid shell. The preparation method comprises the following steps: mixing the phase change material, the high-molecular surfactant and an alcohol-water mixed solution in a reaction container; starting a temperature control system to heat the reaction system to 30-100 DEG C under the condition of inert gas protective atmosphere; after the temperature of the reaction system is stable, adding a styrene monomer and an initiator, mixing and stirring at the stirring speed of 200-400r/min; when the reaction is carried out for 11-13 hours, ferromagnetic nanoparticles modified by a high-molecular surfactant are added, and the reaction is continued for 2-4 hours to obtain a phase change microcapsule; the preparation method comprises the following steps: putting polylactic acid into a dryer, and carrying out drying treatment at 55-65 DEG C for 22-26 hours to remove moisture; premixing polylactic acid and the phase change microcapsules, and performing melt extrusion and granulation through a double-screw extruder; and carrying out injection molding on the blended particles through an injection molding machine. Development of electrical branches can be effectively inhibited, the electrical aging process of the material is delayed, the service life of the material is prolonged, and the use safety is improved.
Owner:STATE GRID ZHEJIANG ELECTRIC POWER CO MARKETING SERVICE CENT +1

Magnetic fluid enhanced electromagnetic heating device and method for preventing and treating secondary hydrate around well

The invention provides a magnetofluid enhanced electromagnetic heating device and method for preventing and treating secondary hydrate around a well. At present, in the process of exploiting natural gas hydrates through a depressurization method, secondary hydrates or ice can be formed due to the fact that the temperature around a well is too low, a gas migration channel in sediment is blocked, and the gas production rate is affected. According to the device or method, a coil is arranged outside a shaft sleeve, and the coil generates a specific-frequency electromagnetic field radiated to stratum sediments. Under the action of the electromagnetic field, magnetite nano-particles naturally contained in the stratum sediment generate oscillating motion, and the aim of heating the stratum around the well is achieved due to heat generated by friction. In addition, in the hydraulic fracturing or slotting stage of the reservoir, the magnetofluid containing the ferromagnetic nanoparticles can be injected along with fracturing fluid, so that the magnetothermal effect of sediments is increased, and the heating effect is further enhanced. In this way, secondary hydrate or ice can be prevented from being formed around the well, pore channels in the sediment are kept unblocked, and therefore the exploitation efficiency of the natural gas hydrate is improved.
Owner:INST OF GEOLOGY & GEOPHYSICS CHINESE ACAD OF SCI

A preparation method of ferromagnetic nanoparticles grafted on the surface of polyglycidol

The invention relates to a preparation method of ferromagnetic nanoparticles grafted on surface of polyglycerol. Ferric oxalate pentahydrate is taken as a precursor compound, triethylene glycol is taken as a solvent, glycidol is taken as a surface modifier, the synthesis is performed through a one-pot process, and the method comprises the following steps: mixing an iron salt oxalate and the strongly polar high-boiling point solvent with a hydroxyl group, firstly reacting at the temperature of 200 DEG C for 1-10 hours, then reacting at the temperature of 280-350 DEG C for 1-10 hours, and naturally cooling to 25 DEG C-120 DEG C after the completion of the reaction; and then adding glycidol monomers, uniformly mixing, reacting at the temperature of 50-200 DEG C for 1-24 hours, then adding the polar organic solvent, precipitating, and separating obtained solids to get the ferromagnetic nanoparticles grafted on the surface of the polyglycerol. The preparation method disclosed by the invention has the advantages that compared with the two-step preparation of the ferromagnetic nanoparticles, the one-pot process preparation process is simple and easy to realize the large-scale industrial production; and the particle size of the ferromagnetic nanoparticles prepared by the method is 10-20nm, and the particle size distribution is uniform.
Owner:TIANJIN UNIVERSITY OF TECHNOLOGY
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