The invention provides a device and method for determining
zinc by electrothermal
evaporation atomic absorption spectrometry, including a sample boat, an electrothermal
evaporation device, a pre-enrichment device, a carrier gas path, a carrier gas
mass flow meter, a release gas path, a T Type atomizer-atomic absorption
spectrometer, the pre-concentration device is composed of
tungsten wire,
tungsten wire power base and pre-concentration device cavity, the
tungsten wire is installed on the tungsten wire power base, and the pre-concentration device is placed overhead Center of the device cavity. The
solid injection atomic absorption spectrometry for the determination of
zinc includes dehydrating and
ashing the sample to be tested in the air to obtain an inorganic residue; The
aerosol of the tungsten wire is in contact with the tungsten wire, and the
zinc is pre-enriched by the tungsten wire; the temperature of the tungsten wire rises to about 1800°C, and zinc atoms are released, and the zinc content is analyzed by an atomic absorption
spectrometer. The device solves the problem of matrix interference in the determination of zinc by electrothermal
evaporation atomic absorption spectrometry with
solid sample introduction, and its
advantage is that it can realize accurate and stable analysis of zinc content in the sample without digesting the sample.