The invention discloses a scanning electron microscope sample processing method for head sensory appendages of white ants. The method comprises the steps of putting white ants into a specially-made wind washing device, carrying out wind washing, feeding the white ants into a specially-made auxiliary vacuumizing device, carrying out vacuumizing operation to sink the white ants, carrying out front fixing and dissection, sequentially carrying out front rinsing under the view of a stereoscope and in an ultrasonic cleaner, carrying out rear fixing, rear rinsing and step-by-step gradient dehydration, putting the white ants into a specially-made filter paper cylinder, sealing the filter paper cylinder, putting the filter paper cylinder into a critical point drying frame, carrying out critical point drying, bonding samples close to a platform under the stereoscope, further dissecting target tissues of partial samples, carrying out secondary sample bonding, connecting the samples which are not subjected to secondary sample bonding with sample bonding adhesive tapes in a non-target observation region by virtue of a conductive silver adhesive, and carrying out all-direction gold sputtering after the conductive silver adhesive is dried. According to the scanning electron microscope sample processing method, multi-aspect technical problems in the background art that the surfaces of the samples are polluted, the samples are difficult to sink in fixation liquid and shrink to deform, different tissue parts of the samples are mutually shaded, and the samples are charged and discharged when being observed in an electron microscope are effectively solved, the cost for solving the problems is low, and the method has relatively high application value.