The invention provides a nanometer
carbon fiber electrode preparation method, and firstly the method uses the carbon
fiber with
diameter of not more than 10mum attached with the silver glue and
metal thread to pass the capillary, and piercing a segment from the capillary; then, putting the carbon
fiber tip piercing from the capillary on the
flame to
etching to nanometer scale; then, withdrawing the carbon
fiber tip into the capillary; in capillary, injecting
epoxy resin, making the
carbon fiber electrode from the nanometer tip to the link part of carbon fiber and
metal thread buried and sealed by
epoxy resin; and finally, after
epoxy resin solidifying, carefully
polishing the front-end of capillary to
expose the nanometer tip of carbon fiber, and obtaining nanometer
carbon fiber electrode. The invention method is simple, low cost, and the prepared nanometer carbon fiber micro-
electrode has the advantages of tightly sealed, easy to update disk
electrode surface, strong shaking resistance, and so on.