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256results about "Fructose production" patented technology

Method for co-producing crystalline fructose and fructose corn syrup by taking wheat as raw material, and preparation method of wheat starch

ActiveCN103146849ASolve constraintsExpand the field of sourcesFructose productionGlucose productionBiotechnologyGluten
The invention discloses a process for co-producing crystalline fructose and F55 fructose corn syrup by taking wheat as a raw material and belongs to the technical field of starch sugar. The process comprises the following steps: grinding the wheat used as the raw material into powder, producing wheat starch by adopting a three-phase horizontal decanter production process, adding a compound enzymic preparation containing lipase into size mixing water to produce by-products such as wheat starch, vital gluten, pentosan and B starch, returning the B starch separated by a three-phase horizontal decanter to a starch finished product tank, subsequently mixing the B starch with A starch and performing a process of producing sugar; acquiring crystalline fructose by mixed wheat starch milk through processes of liquefying, recycling protein, saccharifying, efficiently isomerizing, separating chromatograph, concentrating, crystallizing and drying; and circularly crystallizing mother liquor for a certain number of times, and then compounding the mother liquor with F42 fructose corn syrup acquired by isomerizing to acquire an F55 fructose corn syrup product. By utilizing the preparation method, the problems of high material liquid viscosity, low product yield and poor quality caused by the process of producing starch by taking the wheat as the raw material and sugaring the wheat starch are solved, and the yield and purity of the product are effectively improved.
Owner:BAOLINGBAO BIOLOGY

Method for preparing high-concentration fructose syrup

The invention relates to a method for preparing high-concentration fructose syrup by hydrolyzing sucrose, which comprises the following steps: (1) decolorizing a high-concentration sucrose solution by using acid with dosage accounting for 0.1-1.0% of the high-concentration sucrose solution as the hydrolyst while adding 0.05-0.8% of powder active carbon, and carrying out the reaction at 50-80 DEG C for 15-75 minutes to obtain the high-concentration fructose syrup of which the concentration is more than or equal to 45%, wherein the degree of hydrolysis is more than or equal to 97%; (2) and removing acid radicals and a small amount of pigments in the fructose syrup by using weak-base anion-exchange resin, and removing cations by using a strong-acid cation exchange resin, thereby adjusting the pH value of the fructose syrup. Compared with the exisiting method, the method of the invention is simple and convenient. Through deep research into the hydrolysis conditions, the invention provides the hydrolysis conditions capable of ensuring the hydrolysis effect and reducing the production cost. In addition, the invention carries out the hydrolysis and the decoloring synchronously, thereby ensuring the appearance of the syrup and simplifying the production technology. Then, the acid radicals and the cations in the syrup are removed by using anion and cation exchange resins, thereby obtaining the qualified high-concentration fructose syrup.
Owner:ANHUI BBCA FERMENTATION TECH ENG RES

Phenylboronic acid modified magnetic nanoparticle, and preparation method and application thereof

The invention relates to a phenylboronic acid modified magnetic nanoparticle, and a preparation method and application of the phenylboronic acid modified magnetic nanoparticle, and belongs to the technical field of nano materials. Firstly, a magnetic silicon dioxide nanoparticle is prepared, a sulfydryl modified magnetic nanoparticle is prepared through a silanization reaction, the sulfydryl modified magnetic nanoparticle is then dissolved in ethyl alcohol, 4-vinyl phenylboronic acid and AIBN (azodiisobutyronitrile) are then added, the mixture is stirred and reacts in a water bath kettle, a product is magnetically separated, an obtained solid is washed through distilled water and ethyl alcohol and dried to obtain a final product of the phenylboronic acid modified magnetic nanoparticle; and the obtained material is used in enrichment and separation of fructose. The synthesized magnetic material has the advantages of excellent nuclear shell morphology, and can be rapidly separated in an externally applied magnetic field; the adsorption efficiency of fructose of a magnetic microsphere is 6 times that of glucose, the application effects of enrichment and separation of fructose are quite good, and meanwhile, the phenylboronic acid modified magnetic nanoparticle is excellent in repeatability.
Owner:JIANGSU UNIV

Application of ionic liquid to preparation of reducing sugar by cellulose hydrolysis

The invention relates to dissolution of straws and hydrolysis of celluloses, in particular to a method for preparing reducing sugar by dissolving the straws and hydrolyzing the celluloses in ionic liquid. The method comprises the following steps of: adding 1-ethyl-3-methylimidazole acetate serving as a straw solvent into Fe3+-containing aqueous solution and reacting in the presence of acidic ionic liquid serving as a catalyst under normal pressure at the temperature of between 110 and 140 DEG C for 0.5 to 5 hours; quenching with cold water; neutralizing with alkali liquor to prepare cellulose hydrolyzate; and measuring reducing sugar content by a 3,5-dinitrosalicylic acid method, wherein the reducing sugar in the hydrolyzate and the ionic liquid can be separated by an ion exchange method and the ionic liquid can be repeatedly used. Experiment results show that the reducing sugar yield is up to 93 percent to the maximum extent. Compared with the conventional straw cellulose hydrolysis method, the method has the advantages of solving the problems of complicated pretreatment, low hydrolysis activity, high corrosion to equipment, high cellulose solvent viscosity, inconvenience of operation and the like and providing a new approach for full utilization of the straws.
Owner:JIANGNAN UNIV

Method for preparing reducing sugar by hydrolyzing biomass with super-critical/sub-critical water in two steps

The invention discloses a method for preparing a reducing sugar by hydrolyzing a biomass with super-critical / sub-critical water in two steps, which belongs to the technical field of new energy. The method is characterized in that the high-yield reducing sugar is prepared by hydrolyzing the biomass with the super-critical / sub-critical water through a two-step method, namely a low-temperature section and a high-temperature section. The hydrolysis reaction is performed under the following conditions that: the temperature is 180 to 230 DEG C; the reaction time is 0 to 60 minutes; and the solid-to-liquid ratio is 1:100-1:20. The method of the invention has the advantages that: under two-step method hydrolysis condition of the super-critical / sub-critical water, hemicelluloses in the biomass arereclaimed; the yield of the biologically hydrolyzed reducing sugar is obviously improved; according to different raw materials, the highest total yield of the reducing sugar can reach 40 to 60 percent; and the recovery rate of the raw material and the reducing sugar is over 70 percent.
Owner:DALIAN UNIV OF TECH

Method for hydrolyzing chitin and chitosan

The invention relates to a method for hydrolyzing chitin and chitosan, in particular to a method for jointly hydrolyzing chitin and chitosan through a physical method and a chemical method. The method for hydrolyzing chitin and chitosan comprises the following steps that: the chitin or chitosan is taken as a raw material, binary mixed ionic liquid is taken as a solvent for the chitin or chitosan,acid functionalized ionic liquid is taken as a catalyst for hydrolysis, a water and strong polar co-solvent is added, and hydrolysis reaction is performed under the microwave reaction condition; and the obtained product is analyzed through ion chromatography, gel permeation chromatography and infrared, and the content of total reducing sugar is measured by an Imoto method. The method for hydrolyzing chitin and chitosan has the advantages of high efficiency, environmental friendliness, and high yield.
Owner:苏州九一高科无纺设备有限公司

Preparation method of biochar-based solid acid and application of biochar-based solid acid to cellulose hydrolysis reaction

A preparation method of biological carbon-based solid acid and its application in cellulose hydrolysis reaction belong to the technical field of biomass resource utilization. The preparation method of the biological carbon-based solid acid comprises the following steps: under the conditions of normal temperature and pressure and air atmosphere, the organic strong acid is added dropwise to the biomass ionic liquid solution, and the synchronous "carbonization-nucleophilic substitution" reaction is carried out, and the reaction is carried out by water and acetone. Alternately washed and then dried to obtain a biocarbon-based solid acid. The raw material biomass used is cheap and has a wide range of sources. Using ionic liquid as a solvent, submicron carbon sphere supports with high specific surface area and abundant surface functional groups can be obtained by ion thermal carbonization, and the acid site loading capacity is high. The synthesis of the catalyst can be carried out in the normal pressure air atmosphere, the requirements for the reaction equipment are low, the operation is simple and easy, and the output of the catalyst is high. The obtained bio-carbon-based solid acid is used for the hydrolysis of cellulose, and has the advantages of mild reaction conditions, high yield of reducing sugar and glucose, and reusable catalyst.
Owner:DALIAN UNIV OF TECH

Preparation method of crystalline fructose

The invention relates to a preparation method of crystalline fructose, which sequentially comprises the following steps: carrying out chromatography separation on fructose-glucose syrup, carrying oution exchange and nanofiltration operation on the obtained fructose liquid, then respectively carrying out concentration through a double-effect plate type evaporator and a scraper evaporator, mixing the concentrated fructose liquid with ethanol and finally carrying out crystallization, centrifugal separation and drying, thereby obtaining the crystalline fructose. The prepration method of the crystalline fructose adopts the nanofiltration separation technology, removes impurities which affect the crystallization and the quality of a finished product before the crystallization, improves the product quality and the crystallization yield, combines the high-efficient plate type evaporator with the scraper evaporator, reduces the evaporation temperature of the fructose and the residence time inthe evaporators and effectively prevents the thermal decomposition and the complex reaction of the fructose. Compared with the prior art, the crystalline fructose produced by the method has the advantages of high purity of the fructose, uniform crystalline particles, good color and luster, high crystallization rate and low unit cost.
Owner:ANHUI BBCA FERMENTATION TECH ENG RES
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