The invention relates to a method for detecting
deuterium content in
deuterium depleted water. The method comprises the following steps of: reducing the
deuterium depleted water into
hydrogen with a
reducing agent; introducing a sample and performing chromatographic detection on the sample, wherein high-purity
hydrogen is used as a carrier gas by a gas chromatograph; separating HD peak from the sample gas through gas
chromatographic column, wherein the
peak area is directly proportional to the deuterium content in the sample gas; establishing a
standard curve according to the ultra-low deuterium content in the standard
heavy water sample and the area of the HD peak; reversely extending the
standard curve to the range of the
deuterium depleted water; and calculating the deuterium content in the water according to the area of the HD peak in the
deuterium depleted water. Compared with the prior art, the invention overcomes the disadvantages of difficult separation at the low
liquid nitrogen temperature during the measurement of
hydrogen isotopes through the
gas chromatography and complex measurement and error of
volume correction factor in the area normalization method, breaks through the limitation that external standard method cannot be performed in the absence of standard
deuterium depleted water sample, ensures high analysis precision and accuracy, small equipment investment, convenient operation and low analysis cost and makes the quantitative analysis of the deuterium content during the production of the deuterium depleted water convenient.