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89 results about "Alkylresorcinol" patented technology

Alkylresorcinols, also known as resorcinolic lipids, are phenolic lipids composed of long aliphatic chains and resorcinol-type phenolic rings.

Preparation method of 4-alkylresorcinol

The invention discloses a preparation method of 4-alkylresorcinol. The preparation method comprises the steps: carrying out a reaction on resorcinol and alkyl acid to prepare acyl resorcinol, and then, catalyzing a hydrogenation reaction to obtain 4-alkylresorcinol. By using the method, the dosages of a catalyst and alkyl groups are controlled in an acylation process, so that the yield is remarkably increased, byproducts are reduced, and the production cost is reduced; and hydrogen reduction is adopted in a reduction process, and a high-toxicity and high-pollution zinc amalgam reducing agent is prevented from being used, so that the preparation method is green and environment-friendly; and the aftertreatment is simple, the prepared product is high in purity, the total yield of the two steps reaches up to 77%, and the preparation method has a remarkable significance for industrial production of 4-alkylresorcinol.
Owner:SPEC CHEM IND INC

External Preparation For Skin

An external preparation for skin containing an alkylresorcinol and being excellent in temperature stability (especially high-temperature stability) and photostability. More particularly an external preparation for skin comprising (a) from 0.01 to 5% by mass of 4-isobutyl resorcinol or a salt thereof, and (b) from 0.01 to 5% by mass of one or more selected from L-ascorbic acid or a salt thereof and a 3-O-alkyl-L-ascorbic acid or a salt thereof. If desired, (c) one or more compounds selected from (c-1) a sterol skeleton-having compound (e.g., POE phytosterols, POE cholestanols), (c-2) a vitamin E derivative, (c-3) a compound such as polyglycerin fatty acid esters, polyoxybutene-polyglycerin alkyl ethers, sucrose fatty acid esters, and (c-4) a sorbitan skeleton-having compound may be incorporated in the preparation.
Owner:SHISEIDO CO LTD

Heat insulation waterproof paint of butadiene styrene rubber modified by nanometer SiO2 and preparation method thereof

The invention relates to heat insulation waterproof paint of butadiene styrene rubber modified by nanometer SiO2. The paint is prepared from the following raw materials in parts by weight: 100 parts of butadiene styrene rubber emulsion, 8 to 10 parts of chloroprene rubber emulsion, 15 to 20 parts of hydroxyethyl methylacrylate, 8 to 10 parts of alkyl resorcinol formaldehyde resin, 1 to 2 parts of hexakis methoxymethyl melamine, 3 to 5 parts of titanium dioxide, 3 to 5 parts of talcum powder, 1 to 2 parts of sodium tripolyphosphate, 2 to 3 parts of tributyl phosphate, 1 to 2 parts of texanol, 0.5 to 1 part of 1,2-benzoisothiazolinone-3-ketone, 1 to 2 parts of hydroxymethyl cellulose, 8 to 10 parts of hollow glass micro beads, 3 to 4 parts of 25-percent ammonium hydroxide, 40 to 50 parts of absolute ethyl alcohol, 3 to 5 parts of ethyl orthosilicate, 5 to 8 parts of hydroxyl silicone oil, 1 to 2 parts of white carbon black, 0.5 to 1 part of dibutyltin dilaurate and a proper amount of deionized water. The paint has the advantages that the manufacturing price is low; good heat insulation effects and lighting degrees are realized; the construction is simple and convenient; the application prospects are good.
Owner:ANHUI LENCAQI BUILDING MATERIAL

Heat-insulation and waterproof paint of asbestos fiber enhanced butadiene styrene rubber and preparation method of heat-insulation and waterproof paint

The invention provides heat-insulation and waterproof paint of asbestos fiber enhanced butadiene styrene rubber. The heat-insulation and waterproof paint is prepared from the following raw materials in parts by weight: 100 parts of butadiene styrene rubber emulsion, 8 to 10 parts of neoprene emulsion, 15 to 20 parts of hydroxyethyl methacrylate, 8 to 10 parts of alkyl resorcinol formaldehyde resin, 1 to 2 parts of hexakis(methoxymethyl)melamine, 3 to 5 parts of asbestos fiber, 3 to 5 parts of calcium carbonate powder, 1 to 2 parts of sodium tripolyphosphate, 2 to 3 parts of caustic soda, 1 to 2 parts of texanol, 3 to 4 parts of ammonium dihydrogen phosphate, 0.5 to 1 part of 1,2-benzisothiazolin-3-one, 1 to 2 parts of hydroxymethyl cellulose, 8 to 10 parts of hollow glass micro-bead and a proper amount of de-ionized water. The heat-insulation and waterproof paint provided by the invention is low in construction cost, has good heat-insulation effect and lighting degree, is simple and convenient to construct and has a good application prospect.
Owner:ANHUI LENCAQI BUILDING MATERIAL

Wheat aleurone layer content extracted by adopting pure physical dry process

The invention relates to wheat aleurone layer content (namely wheat aleurone layer powder) extracted by adopting a pure physical dry process. The wheat aleurone layer content is rich in wheat aleurone layer, content of dietary fiber is more than 25.0%, in every 100g of wheat aleurone layer content, content of alkylresorcinol is more than 80mg, content of pentosan is more than 15.0g, and content of phosphorus is more than 700mg. The wheat aleurone layer content is obtained by carrying out pure physical stripping on wheat bran by virtue of an eddy shearing device rotating at a high speed, so that the wheat aleurone layer content can be completely, rapidly and fully stripped from wheat bran particles, and cellular morphology and various nutrition ingredients of the wheat aleurone layer content can be well remained.
Owner:SHANDONG ZHISHIFANG FOOD TECH

Method for synthesizing 4-alkylresorcinol through solvent-free system

The invention relates to the technical field of organic synthesis, in particular to a method for synthesizing 4-alkylresorcinol through a solvent-free system. The method comprises the following stepsthat (1) resorcinol, zinc chloride and alkyl acid are evenly mixed, heated and stirred for a reaction, after cooling, water is added to precipitate a solid, filtering, drying and recrystallization areconducted, and thus 4-acylresorcinol is obtained; (2) the 4-acylresorcinol is dissolved into trifluoroacetic acid, triethyl silicane is added dropwise, heating and stirring are conducted for a reaction, cooling and standing are conducted for layering, an organic layer is extracted and dried, filtration and concentration are conducted to obtain a crude product, recrystallization is conducted, andthe 4-alkylresorcinol is obtained. According to the method, a triethyl silicane / trifluoroacetic acid system is applied to synthesis of the 4-alkylresorcinol for the first time, the reaction conditionis gentler and easier to control, and a post-treatment method is simple; and the system does not contain a solvent, water materials generated during industrial amplification are also greatly reduced,and thus the whole process is more environment friendly.
Owner:上海贤鼎生物科技有限公司
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