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157results about How to "Improve rubbing fastness" patented technology

Method for preparing polyacrylate/amino modified oxidized graphene compound leather finishing agent by adopting ultrasonic-assisted method

The invention relates to a method for preparing a polyacrylate / amino modified oxidized graphene compound leather finishing agent by adopting an ultrasonic-assisted method. The method for preparing the polyacrylate / amino modified oxidized graphene compound leather finishing agent by adopting the ultrasonic-assisted method comprises the following steps: carrying out ultrasonic dispersion on oxidized graphene, sulfur dichloride and dimethylformamide; adding dimethylformamide, carrying out spiral evaporating, adding triethylamine and ammonia water, carrying out ice bath reaction and suction filtration, and washing; adding sodium hydroxide and bromine, carrying out ice bath reaction, then adding products obtained through suction filtration, stirring, carrying out suction filtration, and washing to obtain amino modified oxidized graphene; mixing sodium dodecyl sulphate, polyvinyl alcohol 400 and deionized water, dropwise adding part of methyl methacrylate, butyl acrylate, acrylic acid, hydroxyethyl acrylate and an initiating agent, warming, and then dropwise adding the rest part, so that polyacrylate emulsion is obtained; and regulating pH of the polyacrylate emulsion, then adding the amino modified oxidized graphene, and carrying out ultrasonic dispersion, so that the product polyacrylate / amino modified oxidized graphene compound leather finishing agent is obtained. The method for preparing the polyacrylate / amino modified oxidized graphene compound leather finishing agent by adopting the ultrasonic-assisted method has the advantages that defects of polyacrylate are overcome by utilizing physical and mechanical advantages of graphene and application performance of the polyacrylate / amino modified oxidized graphene compound leather finishing agent is effectively enhanced.
Owner:SHAANXI UNIV OF SCI & TECH

Graphene functional cotton fabric and preparation method thereof

The invention provides a graphene functional cotton fabric and a preparation method thereof, which belong to the technical fields of intelligent wearing and functional textile. The graphene functional cotton fabric is characterized in that graphene oxide is subjected to amination or sulfhydrylation modification, then is composited with a multi-active reactive dye to obtain a graphene oxide reactive dye, the cotton fabric is subjected to dip dyeing in the graphene oxide reactive dye under ultrasonic condition to obtain the graphene oxide cotton fabric, and the graphene functional cotton fabric is reduced by a reducing agent. The graphene functional cotton fabric integrates dyeing and conductivity functions, endows the common cotton fabric with excellent electricity function of graphene, and stability, high temperature resistance and friction color fastness are obviously increased.
Owner:山东利特纳米技术有限公司

Reactive red dye with high washing fastness and rubbing fastness and preparation method of reactive red dye

The invention discloses a reactive red dye with high washing fastness and rubbing fastness and a preparation method of the reactive red dye. Acetanilide reacts with chlorosulfonic acid and sulfoxide chloride to generate acetylsulfanilyl chloride; acetylsulfanilyl chloride is condensed with a sulfide generate by reacting a 2-chlorethamin hydrochloride with mercaptoethanol to obtain thioether; the thioether is oxidized and esterified to obtain 2-[2-(4-aminobenzenesulfonamido) ethyl sulfuryl] hydroxyethyl sulfate which is primarily condensed with cyanuric chloride and secondarily condensed with H acid to obtain a condensation compound; the condensation compound is cooled and then coupled with the diazonium salt of 1.5 acid under an alkaline condition, and the product is filtered and then the filtrate is collected and is subjected to direct spray drying to obtain a semi-finished product. The reactive red dye has the characteristics of bright color, high solubility high substantivity, high compatibility, high lifting power, high fixation rate, excellent diversified fastness and the like. The reactive red dye is suitable for dyeing, printing and pad dyeing of cellulosic fibers, protein fibers, viscose and polyarmide fibers, and higher than common types in rubbing fastness and washing fastness by 0.5 to 1 level.
Owner:TAIXING JINYUN DYESTUFF
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