The invention relates to a preparation method of a
zinc oxide visible-light-induced photocatalyst sensitized by squarylium
cyanine. The preparation method comprises the following steps: dissolving Zn(Ac)22H2O and glucose into deionized water; carrying out ultrasonic
processing to form a settled solution; after transferring the solution into a liner of a
polytetrafluoroethylene autoclave, performing
hydrothermal reaction for 12 to 24 hours at a temperature of 140 to 180 DEG C; after cooling to
room temperature, carrying out centrifugal washing on the obtained black
powder respectively with the deionized water and absolute ethyl
alcohol;
drying at a temperature of 60 DEG C to obtain a
zinc oxide and carbon composite precursor; placing the precursor into a
muffle furnace to calcine for 3 hours at a temperature of 400 to 600 DEG C, so as to obtain
zinc oxide microspheres; mixing the zinc oxide microspheres and the squarylium
cyanine as well as an
organic solvent; at a temperature of 30 to 60 DEG C, carrying out ultrasonic
processing on the mixture for 0.5 to 2 hours; then removing the
organic solvent under the condition of
pressure reduction; and finally,
drying the obtained
solid at a temperature of 60 DEG C. The zinc oxide visible-light-induced photocatalyst sensitized by the squarylium
cyanine can be used for
photocatalysis processing on organic pollutants in air, soil and
sewage.