The invention discloses a distillation rack capable of fixing distilling bottles of different sizes, which comprises a base, a fixing rod is arranged on the left side of the top of the base, and a placing plate is set on the bottom of the surface of the fixing rod, and the surface of the fixing rod is The top is covered with a fixing device, and the fixing device includes an upper splint and a lower splint, grooves are provided on the inner sides of the upper splint and the lower splint, and limit rods are provided on both sides of the groove on the upper splint. The bottom of the limiting rod is provided with a limiting plate, both sides of the limiting plate are provided with slide bars, and both sides of the groove on the lower splint are provided with limiting seats. The present invention cooperates with each other through the fixing device, the upper splint, the limit rod, the fixing nut, the fixing bolt, the groove, the limit seat, the spring, the limit plate, the sliding rod, the chute and the lower splint, and can be used when the distillation frame is in use. , to fix the distilling bottles of different sizes, so that it is more convenient to carry out the distilling bottles of different sizes.