The invention provides a preparation method of an
oxygen-containing washing agent. The preparation method comprises the following steps of: A, adding 1-10 parts by weight of surfactant, 10-70 parts by weight of
sodium carbonate, 1-40 parts by weight of
sodium sulfate and a
raw material combination containing or not containing additional assistant into a reactor, wherein the additional assistant contains 0-20 parts by weight of
sodium bicarbonate, 0-30 parts by weight of silicious
sodium salt and 0-10 parts by weight of an anti-
dirt redeposition agent; and B, adding an aqueous
hydrogen peroxide solution in the reactor, controlling the
reaction temperature of the reactor to be 0-60 DEG C, shaping and
drying after reaction to obtain 100 parts by weight of the
oxygen-containing washing agent the
active oxygen content of which is 1-12.33%. The invention also provides the
oxygen-containing washing agent prepared by using the preparation method. The preparation method provided by the invention is safe and environment-friendly, and can prepare the oxygen-containing washing agent which has the advantages of uniform component distribution, variable
active oxygen content, stable performance,and excellent washing effect.