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272results about How to "High split efficiency" patented technology

Laser radar apparatus that measures direction and distance of an object

ActiveUS20080316463A1Improve beam splitting efficiencyImprove detection accuracyMirrorsOptical rangefindersOpticsRadar
There is provided a laser radar including laser beam generating means, photo detecting means, a mirror, light deflecting means, and rotation driving means. The laser beam generating means emits a laser beam having an axis thereof. The photo detecting means detects a reflected laser beam that is reflected back by an object. The mirror includes a through-hole that passes the laser beam and a reflecting surface that reflects a reflected laser beam reflected back by the object toward the photo detecting means. The light deflecting means deflects the laser beam toward a measuring region and reflects the reflected laser beam from the object toward the mirror. The rotation driving means rotates the light deflecting means so as to direct the laser beam toward the measuring region.
Owner:DENSO WAVE INC

Internet protocol security (IPSEC) tunnel data transmission method and device thereof

The invention relates to the communication field data transmission, in particular to an Internet protocol security (IPSEC) tunnel data transmission method and an IPSEC tunnel data transmission device. The invention provides the IPSEC tunnel data transmission method and the IPSEC tunnel data transmission device. Due to the fact that IP messages of the same kind are combined and compressed through a coprocessor and the like, an IPSEC tunnel model data are packaged to send by an outer network card. Due to the fact that after fragmentation IP message data are rebuilt, the coprocessor is uncompressed and the like, the rebuilt IP message data are divided into each different original IP message and sent through an inner network card, and a data transmission performance of an IPSEC tunnel can be largely improved. Data processing is carried out through the networks, a network data receiver and a network data sending device. The IPSEC tunnel data transmission method and the IPSEC tunnel data transmission device are mainly used in the field of the IPSEC tunnel data transmission.
Owner:中电科网络安全科技股份有限公司

Full-automatic board separating machine

The invention discloses a full-automatic board separating machine. The full-automatic board separating machine comprises a machine base, a feeding device, a waste material collecting mechanism, cutting tools, a moving device and a conveying device. The feeding device is used for conveying circuit boards to be cut, the waste material collecting mechanism is used for collecting cutting waste materials, the moving device is used for driving the cutting tools to move, and the conveying device is used for conveying the cut circuit boards. In this way, the feeding device, the waste material collecting mechanism for collecting the cutting waste materials, the cutting tools, the moving device driving the cutting tool to move and the conveying device for conveying the cut circuit boards are combined to form the board separating machine, the board separating machine achieves feeding, cutting, waste material collecting and circuit board conveying automation, and the sum of labor is reduced; the two cutting tools are used for cutting at the same time, and therefore the board separating efficiency is improved effectively; in addition, the driving mode of moving the cutting tools in multiple directions enlarges the cutting range, and the board separating machine can cut the large circuit boards and is wider in application range.
Owner:ACBEL ELECTRONICS DONG GUAN

Solar cell with small organic molecule mixture heterojunction and preparation method of solar cell

The invention relates to a solar cell with a small organic molecule mixture heterojunction, which comprises a transparent insulating layer, wherein a transparent electrode layer, a first buffer layer, a first photosensitive layer, a second photosensitive layer, a third photosensitive layer, a second buffer layer and a high-reflectivity electrode layer are sequentially laminated at one side of the transparent insulating layer; and a lower transition layer is formed at the other side of the transparent insulating layer. The mixture heterojunction and the lower transition layer are combined together, so that the solar spectrum utilization ratio of the organic solar cell and exciton dissociation efficiency can be improved; meanwhile, the high-reflectivity electrode is reasonable utilized, the optical field distribution in the device can be adjusted, therefore, the solar cell can work at an optimum state. The invention also relates to a preparation method of the solar cell.
Owner:OCEANS KING LIGHTING SCI&TECH CO LTD +1

Rolling bearing fault feature extraction method based on CEEMD and FastICA

InactiveCN110146291ASolve underdetermined problemsTroubleshoot poor processing resultsMachine part testingFrequency spectrumFeature extraction
The invention relates to a rolling bearing fault feature extraction method based on CEEMD and FastICA and belongs to the technical field of fault diagnosis and signal processing and analysis. The method comprises the following steps that: vibration signals are decomposed into IMF components with different frequencies through the CEEMD algorithm, corresponding IMF components are selected accordingto kurtosis criteria so as to be reconstructed into observation signals, and the residual IMF components are reconstructed into virtual noise channel signals; unmixing and denoising processing is performed on the observation signals and the virtual noise channel signals through the FastICA algorithm; demodulation processing is performed on the denoised signals through the Teager energy operator; and FFT (fast Fourier transformation) is performed on the demodulated signals, the frequency spectrum characteristics of the transformed signals are analyzed, the fault characteristic frequencies of the signals are extracted, and a fault diagnosis result is obtained. With the method adopted, the problem of fault information loss during a denoising process and the problem that noises cannot be completely removed due to modal aliasing can be solved; fault fundamental frequencies and frequency multiplication information can be extracted clearly and accurately; and the fault diagnosis result can beobtained.
Owner:KUNMING UNIV OF SCI & TECH

Dual-position multifunctional online plate separator with adjustable rail

A dual-position multifunctional online plate separator with adjustable rail comprises an installation machine case; the middle of an upper platform of the installation machine case is provided with a first and a second sliding rails; the first sliding rail is provided with a first tray which is able to slide thereon; the second sliding rail is provided with a second tray which is able to slide thereon; the external sides of the two sliding rails are provided with a left and right mounting brackets; the left and right mounting brackets are provided with a cross beam; the cross beam is provided with a slide transmission rod and a sucking device; a front platform of the left mounting bracket is provided with a feeding device; an upper platform in front of the right mounting bracket is provided with a plate edge discharging slot; an external side of the plate edge discharging slot is provided with a discharge conveying belt; an upper platform behind the left and the right mounting brackets is symmetrically provided with guide rails; the guide rails are provided with a second cross beam which is able to slide along the guide rails; the second cross beam is provided with a plate separating mechanism which is able to slide on the second cross beam. The dual-position multifunctional online plate separator with adjustable rail integrates functions such as automatic feeding, positioning, plate cutting, plate edge fetching, and blanking of PCB plates in one machine, thus the plate separating efficiency is high.
Owner:KELI ELECTRONICS EQUIP

Monolayer organic solar cell and preparation method thereof

The invention discloses a single-layer organic solar cell, which comprises a transparent insulating substrate, a transparent anode electrode layer, a metal nanoparticle layer, a photosensitive layer and a cathode electrode layer sequentially stacked on the transparent insulating substrate. The work function value of the metal nanoparticles in the particle layer is higher than that of the transparent anode electrode layer. The metal nanoparticle layer is set in the single-layer organic solar cell of the present invention, thereby further enhancing the built-in electric field of the single-layer organic solar cell device, thereby improving the exciton splitting efficiency of the pair, and finally improving the efficiency of the single-layer organic solar cell. Energy conversion efficiency; the preparation method of a single-layer organic solar cell device uses stable sputtering and vacuum evaporation to form each layer of the solar cell device in sequence, so that the connections between the layers are tight and firm, so that the solar cell device The performance is stable, the production efficiency is high, and it is suitable for industrial production.
Owner:OCEANS KING LIGHTING SCI&TECH CO LTD +1

Video file splitting method and device, electronic equipment and storage medium

Embodiments of the invention provide a video file splitting method and device, an electronic device and a storage medium. The method comprises the steps of determining a frame image segmentation pointof a to-be-split video file; according to the frame image segmentation point, obtaining a key frame of each video segment corresponding to the frame image segmentation point; inputting the key frameinto a pre-trained host identification model to obtain host category information; if the host category information meets a preset screening condition, determining a key frame corresponding to the hostcategory information as a video segmentation point set; according to the video segmentation point set, splitting the to-be-split video files. The video files can be automatically split in batches, manual intervention is not needed, the video splitting efficiency is improved, and meanwhile the production efficiency of short videos is improved.
Owner:BEIJING QIYI CENTURY SCI & TECH CO LTD

Laser radar apparatus that measures direction and distance of an object

A laser radar including laser beam generating means, photo detecting means, a mirror, light deflecting means, and rotation driving means. The laser beam generating means emits a laser beam having an axis thereof. The photo detecting means detects a reflected laser beam that is reflected back by an object. The mirror includes a through-hole that passes the laser beam and a reflecting surface that reflects a reflected laser beam reflected back by the object toward the photo detecting means. The light deflecting means deflects the laser beam toward a measuring region and reflects the reflected laser beam from the object toward the mirror. The rotation driving means rotates the light deflecting means so as to direct the laser beam toward the measuring region.
Owner:DENSO WAVE INC

Method and system for fast semantic annotation of e-book

The invention relates to a method and a system for fast semantic annotation of an e-book. The method is characterized by comprising the following steps that: (1) a directory structure file for describing a structure of the e-book in a way independent of the e-book is created, a chapter list of the e-book is extracted, and a tree hierarchy relationship is created, and simultaneously, each chapter element contains the property of page number information; (2) the semantic annotation of list elements is carried out based on the directory structure file; (3) the e-book is divided into multiple page files, and each page file is a page of the e-book; and (4) the directory structure file, book CIP (cataloging in publication) data, a copyright statement and the multiple page files are packaged to form a complete e-book file package.
Owner:BEIJING HOPE SOFTWARE

Method, device and equipment for splitting large-scale application service into micro services

The invention discloses a method for splitting a large-scale application service into micro services. The method comprises the steps that a request instruction for extracting a target micro service isreceived; a corresponding target code is split from a code set through a method tracking technology; the target code is classified to generate the module of a corresponding category; the module is encapsulated into an image file; and a target micro service is extracted from the image file. According to the method, device and equipment for splitting the large-scale application service into micro services, on the basis of the received request instruction for extracting the target micro service, the corresponding target code is split, the target code is classified, the module of the corresponding category is generated, the module is encapsulated into the image file, and the target micro service is extracted from the image file. The method, device and equipment for splitting the large-scale application service into micro services have the advantages that the large-scale application service can be automatically split into micro services, the workload is greatly reduced, the work cost is reduced, and the splitting efficiency is improved. The invention further discloses a device, equipment and storage medium, for splitting the large-scale application service into micro services, which all have the corresponding technical effects.

Method for preparing photoactived amino acid through resolution

In the invention, the method comprises the steps of: employing a combined AES (1-Arylethanesulfonic acids) resolving agent composed of photoactivated 1-phenyl ethanesulfonic acid as a main resolving agent and racemized substituted phenyl ethanesulfonic acid as an assistant resolving agent to resolve racemized amino acid in an aqueous solution or organic solvent or organic solvent / aqueous solution, heating the mixture to reflux until the solution is clarified, stirring and cooling the solution, separating out crystals, filtering the crystals, washing the filter cake, and stoving the filter cake, thus obtaining a configured photoactived amino acid. And treating the filtrate in the same way can generate another configured photoactived amino acid. The resolving agent, after ion exchange, concentration and recovery, can be used circularly. The combined AES resolving agent of the invention has good selectivity and high resolution efficiency for racemized amino acid, and the two types of configured photoactived amino acid obtained have high purity, and the optical purity can be over 97%o.p. Besides, the yield of product is high, about more than 95%. As the resolving agent has high utilization rate and recovery rate, the production cost can be reduced.
Owner:河北凯力昂生物科技有限公司

Laser radar apparatus that measures direction and distance of an object

There is provided a laser radar apparatus including laser beam generating means, photo detecting means, a mirror assembly, light deflecting means, and rotation driving means. The laser beam generating means emits a laser beam having an axis thereof. The photo detecting means detects a reflected laser beam that is reflected back by an object. The mirror assembly includes a through-hole that transmits the laser beam and a reflecting surface that reflects a reflected laser beam reflected back by the object toward the photo detecting means. The light deflecting means has a flat mirror surface and a concave-shaped mirror surface, and reflects the laser beam toward a measurement range and deflects the reflected laser beam from the object toward the mirror assembly. The rotation driving means rotates the light deflecting means so as to direct the laser beam toward the measurement range.
Owner:DENSO WAVE INC

Video news splitting method and device

The invention discloses a video news splitting method and device. The video news splitting method comprises the following steps: breaking a news video to be processed into at least one scene, recording the start time point and end time point of each scene in the news video, extracting m key frames of the scenes according to a preset time interval, analyzing the m key frames of the scenes to obtainanchor category information of the scenes, and recording the start time point and end time point of news headline; generating news headline marking information for marking the scenes; and splitting the news video into N pieces of news information according to preset splitting rules based on the start time point and end time point of each scene in the news video, the anchor category information ofthe scene, and the news headline marking information of the scenes. Through the video news splitting method and device, the video news can be split automatically based on the anchor information and news headline information in the video news, therefore, the efficiency of splitting the video news is improved.
Owner:BEIJING QIYI CENTURY SCI & TECH CO LTD

Oil well production automatic splitting device and method

The invention provides an oil well production automatic splitting device and method. The oil well production automatic splitting method comprises the following steps of 1, loading well history data of an oil well; 2, loading production data of the oil well; 3, dividing a production stage of the oil well; 4, selecting a production splitting method; 5, performing batch oil well automatic production splitting according to the selected production splitting method; and 6, drawing an oil well production measure curve by using the production splitting result. The oil well production automatic splitting device and method have the characteristics that the oil well production stage is automatically divided; and the oil well production is automatically split by many methods, and the like. The device and the method have the advantages that the batch oil well production splitting efficiency is high; the oil well production splitting methods are many; the oil well production splitting result is precise; and the operation by a user is simple, and the like.
Owner:CHINA PETROLEUM & CHEM CORP +1

Processing workbench and processing system for PCBs (printed circuit boards)

The invention provides a processing workbench and a processing system for PCBs (printed circuit boards). The processing workbench comprises a rotatable rotating disc, a fetching manipulator, a laser cutting machine, a splitting manipulator and a collecting manipulator are uniformly distributed above the rotating disc along the clockwise direction of the rotating disc, and a rotating device for rotating the PCBs to a specified processing position is arranged below the rotating disc. The rotatable rotating disc is adopted for various processes like fetching, cutting, spitting and collecting, sothat compared with conventional board splitting modes, the processing workbench has the advantage that board splitting efficiency can be improved by higher than 10 times.
Owner:TIANJIN MEISEN ELECTRONICS CO LTD

Single-layer organic solar cell and making method thereof

The invention discloses a single-layer organic solar cell, which comprises a transparent insulating substrate, and a transparent anode electrode layer, a photosensitive layer and a cathode electrode layer which are sequentially formed on the transparent insulating substrate in an overlapped manner; a metal nano-particle layer is formed on at least one surface of the cathode electrode layer in the overlapped manner; and the power function value of metal nano particles in the metal nano-particle layer is less than the power function value of the cathode electrode layer. The metal nano-particle layer is arranged in the single-layer organic solar cell, so a built-in electric field of a single-layer organic solar cell device is enhanced, the separation efficiency of right excitons is improved, and the energy transfer efficiency of the right excitons is finally enhanced; by a making method for the single-layer organic solar cell device, all the layers of the single-layer organic solar cell device are sequentially formed and tightly and firmly connected, so the single-layer organic solar cell device is stable in performance, high in production efficiency and applicable for industrialized production.
Owner:OCEANS KING LIGHTING SCI&TECH CO LTD +1

Intelligent nanometer chiral selector material, as well as preparation and application thereof

ActiveCN108299651AEfficient temperature sensitivityEfficient Magnetic ResponseOther chemical processesAlkali metal oxides/hydroxidesTemperature responseChiral selectivity
The invention discloses an intelligent nanometer chiral selector material, as well as preparation and application thereof. The preparation comprises the steps of firstly preparing Fe3O4 magnetic nanoparticles; then modifying the obtained Fe3O4 magnetic nanoparticles through polydopamine; and the like. The material provided by the invention has thermosensitivity, temperature-response chiral selectivity, and magnetic responsiveness, and is capable of quickly and simply decomposing an enantiomer molecule and regenerating the material after splitting an amino acid enantiomer.
Owner:SOUTHWEST UNIVERSITY FOR NATIONALITIES

Splitting and fast taking device for soft magnetic ferrite cores

The invention discloses a splitting and fast taking device for soft magnetic ferrite cores, which comprises a base plate. A push plate parallel to the base plate is installed at the bottom of the baseplate. Ejector pins are welded in an array on one side of the push plate near the base plate. A bearing plate fixedly connected with the top of the base plate is installed at one end of the ejector pins extending out of the top of the base plate. The bearing plate is provided with through holes which sleeve the ejector pins in a sliding manner. A sintering plate is placed on the top of the base plate. A bracket is installed on the top of the base plate. A driving mechanism is installed along the length direction of the base plate on one side of the bracket near the base plate. A first cylinder is installed vertically on one side of the driving mechanism near the base plate. A rectangular cover is welded vertically to one end of the first cylinder near the base plate. The device of the invention is simple in structure and convenient to operate. By using the device, sintered soft magnetic ferrite cores can be conveniently split and taken, batch operation on soft magnetic ferrite cores is realized, the efficiency of soft magnetic ferrite core splitting and taking after sintering is improved, and the production efficiency of soft magnetic ferrite cores is improved.
Owner:中山市天文电子有限公司

Crane arm loading and unloading method and crane arm

The invention provides a crane arm loading and unloading method and a crane arm. The to-be hoisted crane arm comprises a first arm section and a second arm section installed in the first arm section, and the tail part of the second arm section is provided with an upper sliding block. The crane arm loading and unloading method comprise: a step of installing and adjusting the first arm section, namely, enabling the first arm section to stretch out according to a first stretching quantity and changing the amplitude of the first arm section to be 0 DEG; a step of installing and adjusting the second arm section, namely, hoisting the second arm section through a hoisting assembly, adjusting the hoisting assembly to enable the head part of the second arm section to be lifted upwards by a first angle Pi, adjusting the second arm section to enable the upper sliding block of the second arm section to have a height capable of exactly entering the head part of the first arm section at the height direction, and adjusting the gap between the sidewall of the second arm section and the sidewall of the first arm section; and a step of putting the second arm section into the first arm section, namely hoisting and installing the second arm section into the first arm section, and fixing the second arm section to the first arm section. The crane arm loading and unloading method is capable of rapidly loading the crane arm.
Owner:ZOOMLION HEAVY IND CO LTD

Bag folding machine and bag folding method

The invention discloses a bag folding machine and a bag folding method. A left folding mechanism and a right folding mechanism of the bag folding machine repeatedly use a feeding mechanism and a discharging mechanism, so that the occupied space of the bag folding machine is not multiplied while the number of passes of the folding mechanisms is increased and the production efficiency is improved. In the bag folding process, when one folding mechanism is folding a bag while the other folding mechanism has already folded a bag and is idle, a bag on the feeding mechanism can be conveyed to the idle folding mechanism through a bag distribution mechanism, and the cycle is repeated. According to the scheme, when the feeding mechanism feeds materials to the folding mechanisms, the feeding mechanism needs to wait until the folding mechanisms fold the bags well, and the production efficiency is improved.
Owner:ZHONGSHAN TAILI HOUSEHOLD PROD MFG

Plate snapping machine and aerated concrete blank manufacturing device

The invention provides a plate snapping machine and an aerated concrete blank manufacturing device and relates to the technical field of aerated concrete blank manufacturing equipment. The plate snapping machine comprises a plate snapping assembly, a driving assembly and an installation structure. The plate snapping assembly comprises a first plate snapping piece and a second plate snapping piecewhich are oppositely arranged, and the first plate snapping piece and the second plate snapping piece are movably connected with the installation structure. The driving assembly is connected with theplate snapping assembly and is used for driving the first plate snapping piece and the second plate snapping piece to tilt in the same direction, so that the first plate snapping piece and the secondplate snapping piece are matched to snap a plurality of blanks in the direction of the blank cutting surface. According to the plate snapping machine, a plurality of adhered blanks can be snapped apart by one-time operation, so that the snapping efficiency is improved; and a small amount of oil cylinders are required in the driving assembly, so that the structural complexity and cost of the platesnapping machine can be reduced, and the difficulty in maintenance and repair can be reduced.
Owner:HUNAN SANY KUAIERJU RESIDENTIAL IND CO LTD

Automatic segmenting device and method for orange fruits

The invention discloses an automatic segmenting device and method for orange fruits. The device includes orange fruit positioning equipment, orange fruit segmenting equipment and a frame; the orange fruits are positioned by the orange fruit positioning equipment, image data information of orange fruit segmenting lines are collected, stored and analyzed by using an image data acquisition system toobtain the orange fruit segmenting lines, and the orange fruits are segmented by using the orange fruit segmenting equipment. According to the device and method, after the orange fruits are put into the segmenting equipment, the automatic orange segmenting operation can be realized, and multiple sets of orange fruit positioning equipment and orange fruit segmenting equipment can be arranged in parallel on the device frame, so that the labor cost investment can be reduced, and the orange segmentation is more efficient; by using the image data acquisition system to control the position of orangefruit segmentation, the device can improve the accuracy of the orange segmentation; and by using a combination of a segmentation bow and support knife equipment to segment the orange fruits, the device can automatically segment the orange fruit according to the segmenting lines, so that automatic segmentation and complete cutting of the orange fruits with different specifications can be realized,and the device does not have the phenomenon of orange segment adhesion.
Owner:CHANGZHOU MINGSHI AUTOMATION EQUIP CO LTD

Resolving agent for 1, 1'-bi-2-naphthol and resolving method thereof

The invention provides a resolving agent for racemized 1, 1'-bi-2-naphthol and a resolving method thereof. The resolving agent is a dehydroabietylamine. The resolving method comprises the following steps of: leading the racemized 1, 1'-bi-2-naphthol and optically pure resolving agent (+)-dehydroabietylamine to react in a solvent to generate a diastereomer salt; carrying out the separation by utilizing the difference of solubility in the selected solvent; subsequently carrying out dissolving and purifying, thus obtaining the optically active 1, 1'-bi-2-naphthol single enantiomer. The method hashigh resolving efficiency, simple operation, short process flow, economic resolving method and low cost, the resolving agent (+)-dehydroabietylamine has easy source and low price, is easy to be reclaimed, has high reclaiming rate and can be used repeatedly.
Owner:GUANGXI RES INST OF CHEM IND CO LTD

Industrial preparation process for key intermediate sulfonated saccharide of Gemcitabine

The invention relates to a preparation method for a compound represented by a formula (I) shown in the description, i.e., a key intermediate sulfonated saccharide of Gemcitabine. The final product is prepared through subjecting a compound represented by a formula (II) shown in the description to sodium borohydride reduction, hydroxyl protection and resolution. The method is simple in process, high in yield and high in product purity and has no need of harsh reaction conditions, thereby being very suitable for industrial production.
Owner:连云港恒运药业有限公司

Plate splitting device

The invention discloses a plate splitting device, which is provided with a bracket, wherein a moving part which can move up and down is respectively arranged at two opposite sides of the bracket, a guide rod is transversely arranged on each moving part, two guide grooves through which two free ends of the guide rods are inserted respectively are vertically arranged on a stander, each moving part is provided with a through groove, an adjusting part is movably inserted into each through groove, the inner free end of each adjusting part is a support head, the outer free end of each adjusting part extends out of the corresponding through groove, the bracket is vertically provided with an adjusting groove, the inner side wall and the outer side wall of the adjusting groove respectively comprise an upper groove section, an oblique section and a lower groove section which correspond to each other, wherein the two oblique sections are oblique from top to bottom and from inside to outsides, the two oblique sections are staggered to each other up and down, and the oblique section at the outer side is higher than the oblique section at the inner side. The plate splitting device disclosed by the invention is simple in integral structure, easy to operate, continuous and reliable in plate splitting action, high in plate splitting efficiency, extremely little in damage to bricks in the plate splitting manner and flexible and adjustable for splitting plates and provides a brand-new operation mode for plate splitting operation of the plates with the bricks.
Owner:FUJIAN EXCELLENCE HONCHA BUILDING MATERIAL EQUIP

Method for separating caprylic acid from mixture of caprylic acid and capric acid

The invention discloses a method for separating octanoic acid from a mixture of octanoic acid and decanoic acid. The separating method is as follows: in a resolution solvent, substitute pyridine fully reacts with the mixture of the octanoic acid and the decanoic acid at reflux temperature, and a compound crystal is separated out after cooling; after being recrystallized, the compound crystal crude product obtained after filtration is hydrolyzed by diluted hydrochloric acid the concentration of which is 2 percent to 10 percent, and is separated to obtain an aqueous layer A and an organic layer A which is washed and dried to obtain the monomer octanoic acid. Compared with the prior art, the method has the advantage of higher resolution efficiency. Due to the high selectivity of molecular recognition, the yield of the monomer octanoic acid can be between 80 and 95 percent and the purity can be between 95 percent and 99 percent only by crystallizing once. Besides, the method has simple operation, good repeatability and low implementation cost, and is advantageous to industrial expansion.
Owner:ZHEJIANG UNIV OF TECH

Method for preparing D-valine by asymmetric transformation process

The invention belongs to the technical field of preparation of D-amino acid compounds, and particularly relates to a method for preparing D-valine by an asymmetric transformation process. The method comprises the following steps: carrying out asymmetric transformation on a chiral resolution reagent D-diacetyl tartaric acid and DL-valine in a glyoxalic acid solution, and crystallizing to precipitate the target double salt; and separating the double salt, washing, and dissociating to obtain the D-valine, wherein the total yield is greater than 92%, and the resolution reagent D-diacetyl tartaric acid can be recycled. The method saves the step of DL step in the chemical resolution simple to operate, has the advantage of high resolution efficiency, avoids the phenomenon of entrapped precipitation in the chemical resolution method, and ensures the high optical purity of the D-valine (>99.5%ee). The recycling of the chiral reagent greatly lowers the production cost, and is suitable for industrial production.
Owner:濮阳天健生物科技有限公司
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