The invention discloses a preparation method of a
calcium molybdate /
molybdenum disulfide composite
luminescent material. The preparation method specifically comprises the following steps: dissolving 0.85g of
sodium molybdate into 30mL of water, stirring for 5 minutes so as to generate a
sodium molybdate water solution, pouring the
sodium molybdate water solution into a
polytetrafluoroethylene liner, soaking two egg shells into water, taking off inner membranes attached to the egg shells, and putting the inner membranes into the
sodium molybdate water solution; and putting the
polytetrafluoroethylene liner into a reaction kettle, sealing the reaction kettle, putting the reaction kettle into a
drying oven to react at 160-240 DEG C for 24 hours, taking out the product, cleaning the product to be neutral by virtue of deionized water and absolute
ethanol, and
drying at 40 DEG C for 6-48 hours, so as to obtain the
calcium molybdate /
molybdenum disulfide composite
luminescent material. The composite
luminescent material can emit
blue light and
green light under an
ultraviolet excitation condition. The simultaneous emission of the
blue light and the
green light is realized by virtue of compounding of
molybdenum disulfide for the first time on the premise that a
rare earth element is not introduced, and a synthetic process is relatively simple and low in cost.