The invention provides an
oxygen bomb
combustion method for testing the content of halogens and the content of sulphur in industrial
solid waste. The concentration-spectrum
peak area working curve of to-be-measured element series
standard solution is drawn, a proper amount of sample is added to an
oxygen bomb based on the principle that the amount of sample increases with the reduction of calorific value, absorption liquid the volume of which is 0.05 time that of the
oxygen bomb and a proper amount of H2O2 with
mass fraction of 10-30% are also added, the sample is burnt and oxidized in the oxygen bomb to obtain a substance which is then absorbed by the absorption liquid so as to generate
test sample solution, the spectrum
peak area of the sample solution is measured by means of an
ion chromatograph, and the content of halogens and the content of sulphur in waste are calculated according to the spectrum
peak area and the series
standard solution working curve. According to the method, by adding a certain amount of H2O2, oxidation of sulphur in the
combustion process can be promoted, complete
combustion of sulphur during testing is ensured, loss is reduced, and test results are more accurate; meanwhile, the weight of the sample added each time is determined based on the principle that the amount of sample increases with the reduction of calorific value, so that complete combustion of the sample during testing is guaranteed and testing time is shortened.