The invention belongs to the technical field of carbon material preparation, and discloses a
graphene preparation method based on a
liquid phase stripping method and a hydrothermal method. The
graphene preparation method comprises the following steps: adding powdered
graphite and water into a reaction kettle; sealing, then stirring, heating to a
reaction temperature, keeping constant temperature, continuously stirring and reacting; after ending reaction, cooling, taking out a
mixed solution in the reaction kettle so as to carry out
centrifugal separation, wherein solids at a lower layer are unreacted powered
graphite, and supernatant liquid is
graphene dispersion liquid; and carrying out
centrifugal separation on the graphene dispersion liquid so as to obtain solids, namely graphene. According to the graphene preparation method, water is used as a
solvent so as to overcome the shortcomings that an
organic solvent is high in
boiling point and difficult to remove and has
toxicity, or as Hansen
solubility parameters of the
organic solvent cannot meet the
solubility parameters of graphene, the concentration of the dispersion liquid is relatively low. The yield of the prepared graphene is high; the prepared graphene has very few defects and is very low in
oxygen content; and the intrinsic electrical property of the graphene is maintained.