The invention relates to a preparation method of gold nanometer array
electrode, which the substrate is
polycarbonate filter membrane, after the processes of the pretreatment of
chemical plating to the
polycarbonate filter membrane,
chemical plating,
chemical plating after acid leaching, such as cleaning and
processing, the former treatment, post acid leaching and rinsing, and assisted by the ultrasonic wave process in the steps of pretreatment, acid leaching and rinsing, using
degreasing cotton soaked with dilute
sodium cyanide to softly wipe the surface of the filter membrane after chemical plating, then rinsing with
methanol, using the
combined method of mechanical effect and chemical effect to effectively remove a
gold layer on the surface to form the gold nanometer array, then pasting the filter membrane to the collector, assembling into the gold nanometer array
electrode. The
diameter of a single gold nanometer disk in the array is 10 to 100 nanometers measured by scanning electronic
microscope, the component of the array group is pure gold measured with energy dispersive X-
ray spectrum. The
electrode has the advantages of high
mass transfer speed, low double-layer
charge current, effectively improving
signal-to-
noise ratio and the
detection limit. The preparation method of gold nanometer array electrode has the advantages of ingenious design, simple operation and good
reproduction.