Composite film with high-temperature resistance layer, preparation method thereof and battery
A high-temperature-resistant layer and composite film technology, which is applied to battery components, circuits, electrical components, etc., can solve problems such as high-temperature resistance decline, shedding, and impact on battery performance, so as to improve peel strength, reduce battery short circuit, and improve The effect of peel strength
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[0031] The present application provides a method for preparing the above-mentioned composite membrane with a high temperature resistant layer. The method comprises: grafting amino groups on the surface of inorganic ceramic particles, grafting carboxyl groups on the surface of the thermoplastic resin porous membrane; preparing inorganic ceramic particles with amino groups on the surface. The coating slurry is applied to at least one surface of the porous thermoplastic resin film grafted with carboxyl groups on the surface. During the preparation process, the carboxyl groups grafted on the surface of the thermoplastic resin porous film and the amino groups grafted on the surface of the inorganic ceramic particles undergo polymerization reaction, so that the inorganic ceramic layer is fixed on at least one surface of the thermoplastic resin porous film through polymerization.
[0032] In a specific embodiment of the present application, the grafting of amino groups on the surface of ...
Embodiment 1
[0039] The thermoplastic resin porous film is a polypropylene film with a thickness of 16μm
[0040] (1) Aminosilane coupling agent modifies the surface of inorganic ceramic particles
[0041] Add 6.0g of aluminum oxide with an average particle size of 300nm to the ethanol dispersion and stir and heat to about 45°C, adjust the pH to about 6.5, and then slowly add 1.2g of 3-aminopropyltriethoxy to the ethanol dispersion Base silane, keeping the temperature of the ethanol dispersion at about 45°C and the pH value at about 6.5, react for 1 hour, wash with acetone to obtain the aluminum oxide grafted with the coupling agent on the surface, and dry at room temperature under vacuum.
[0042] (2) The surface of the thermoplastic resin porous membrane is grafted with carboxyl groups
[0043] 2wt% of benzophenone was dissolved in tetrahydrofuran to prepare a coated photosensitizer solution, the polypropylene film was immersed in the photosensitizer solution for 2 minutes, then taken out and dr...
Embodiment 2
[0048] The thermoplastic resin porous film is a polyethylene film with a thickness of 12μm
[0049] (1) Aminosilane coupling agent modifies the surface of inorganic ceramic particles
[0050] Add 8.0g of aluminum oxide with an average particle size of 500nm into the ethanol dispersion and stir and heat to about 55°C, adjust the pH to about 7.5, slowly add 1g of 3-aminopropyltriethoxysilane to maintain the temperature of the ethanol dispersion At about 55°C, the pH value is about 7.5, react for 1 hour, wash with acetone to obtain the aluminum oxide grafted with the coupling agent on the surface, and dry in vacuum at room temperature.
[0051] (2) The surface of the thermoplastic resin porous membrane is grafted with carboxyl groups
[0052] 2wt% of benzophenone by weight was dissolved in tetrahydrofuran to prepare a coated photosensitizer solution, the polyethylene film was immersed in the photosensitizer solution for 2 minutes, then taken out and dried, and exposed to ultraviolet ligh...
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