Novel preparation process of surface coating layer of rod electrode in environment-friendly gas
A preparation process and surface coating technology, applied in metal material coating process, device for coating liquid on the surface, coating, etc., can solve potential safety hazards, increase equipment pressure bearing capacity and other problems, and achieve insulation performance improvement , increase thermal stability, improve the effect of dielectric properties
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Embodiment 1
[0041] When the insulating layer is a nano-SiO2 / EP coating, the preparation method is as follows:
[0042] a1. Select epoxy resin EP and nano-SiO 2 Particles, curing agent, accelerator, choose SiO with a size of 20–30nm 2 particles;
[0043] b1, using a centrifugal stirrer to mix nano-SiO 2 The particles are evenly mixed in the epoxy resin EP;
[0044] c1. Accurately weigh epoxy resin EP and nano-SiO according to the mass calculated in advance 2 Pellet mixture, hardener, accelerator and pour them into clean containers;
[0045] d1. The above-mentioned container passes through the Thinky ARE-310 centrifugal agitator, first at 1000r·min –1 Stir for 5 minutes, then at 2000r·min –1 Stir for 10 minutes, then ultrasonically vibrate for 20 minutes;
[0046] e1. Put the above container into a vacuum drying oven to remove the air bubbles introduced by centrifugal stirring and material addition;
[0047] f1. The fully mixed epoxy colloid obtained from step e is divided into two ...
Embodiment 2
[0050] When the insulating layer is nano-Al 2 o 3 / EP coating, the preparation method is as follows:
[0051] a2. Weigh EP, curing agent, accelerator and Al in sequence in proportion 2 o 3 , the Al 2 o 3 The particle size is 30–40nm;
[0052] b2, fully centrifuging and ultrasonically oscillating the materials in step a;
[0053] c2, the finished product obtained in step b is transferred to a vacuum drying oven for defoaming treatment;
[0054] d2, after being processed in step c2, divide into two parts, prepare the electrode coating by the pulling coating method respectively, test the thickness of the fully cured coating by a multi-thickness meter, nanometer Al 2 o 3 The thickness of the / EP coating is 75 μm.
Embodiment 3
[0056] When the insulating layer is a ceramic coating, the preparation method is as follows:
[0057] a3. Clean and dry the stainless steel rod electrode substrate with an ultrasonic cleaner, and sandblast the surface of the rod electrode with alumina powder. The surface roughness of the rod electrode after sandblasting is about 6.3 μm;
[0058] b3, using supersonic atmospheric plasma spraying SAPS technology to 14wt%Y 2 o 3 / ZrO 2 (YSZ) spherical particles and 20wt% Al 2 o 3 / ZrO 2 (ASZ) Spherical particles are evenly sprayed on the surface of the rod electrode;
[0059] The 14wt% Y 2 o 3 / ZrO 2 (YSZ) spherical particle size is 500μm, the 20wt% Al 2 o 3 / ZrO 2 (ASZ) spherical particles with a size of 500 μm,
[0060] The SAPS system is equipped with a gun with a Laval nozzle, the length and diameter of the Laval nozzle are 44 mm and 6 mm respectively, the spray powder is injected into the plasma fixture by a syringe with a diameter of 2 mm, and the thickness of t...
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