Automatic center adjusting polycrystalline die of high-speed vertical enameling machine
An automatic adjustment, polycrystalline mold technology, applied in the direction of insulating conductors/cables, etc., can solve problems such as poor thermal stability performance
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Embodiment 1
[0035] The present embodiment is the preparation method of intermediate 3, comprising the following steps:
[0036] A1: Add the catalyst to a three-neck flask equipped with a condensing reflux tube, a constant pressure dropping funnel, and a stirrer, raise the temperature to 100°C, then continue heating to 180°C, and control the heating rate to 10°C / h, then add silicon powder , stirring and dispersing for 20 min under the condition of a stirring rate of 50 r / min, then adding methanol which has been treated with 3A molecular sieves dropwise while stirring, controlling the dropping rate to 1 drop / s, and then collecting the condensate to obtain intermediate 1; Control the consumption of described catalyst to be 8% of silicon powder mass, described catalyst is the mixture of ethylene glycol butyl ether and sodium methylate according to 100mL: 10g, and described silicon powder particle size is 400 meshes;
[0037]A2: Add magnesium powder, mixed solvent and benzene bromide to a four...
Embodiment 2
[0040] This embodiment is the preparation method of intermediate 3, comprising the following steps:
[0041] A1: Add the catalyst to a three-necked flask equipped with a condensing reflux tube, a constant pressure dropping funnel, and a stirrer, raise the temperature to 100°C, then continue heating to 180°C, control the heating rate to 15°C / h, and then add silicon powder , stirring and dispersing for 30min under the condition of a stirring rate of 100r / min, then adding methanol after 3A molecular sieve treatment dropwise while stirring, controlling the dropping rate to 2 drops / s, and then collecting the condensate to obtain intermediate 1; The consumption of controlling described catalyst is 10% of silicon powder mass, and described catalyst is the mixture of ethylene glycol butyl ether and sodium methylate according to 100mL: 30g, and described silicon powder particle size is 500 meshes;
[0042] A2: Add magnesium powder, mixed solvent and benzene bromide to a four-necked fla...
Embodiment 3
[0045] The present embodiment is the preparation method of mold core raw material, comprises the following steps:
[0046] Add the intermediate 3 and heat-resistant filler from Example 1 into the mixer, and mix evenly under the condition of a stirring rate of 550r / min to obtain a high-temperature-resistant adhesive, and add diamond to the high-temperature-resistant adhesive Continue to mix the micropowder, and mix evenly to obtain the core material; control the mass ratio of the intermediate 3 to the heat-resistant filler to be 3:1, and the heat-resistant filler is a mixture of zirconium diboride and nickel at a ratio of 4:1.
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