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Antistatic anti-aging polyimide explosion-proof membrane

A polyimide and anti-static technology, applied in the field of anti-static and anti-aging polyimide explosion-proof film, can solve the problems of improving the anti-static performance and anti-aging performance of explosion-proof film, and being unable to apply to folding screens.

Inactive Publication Date: 2021-05-04
苏州欧纳克纳米科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0004] Chinese patent document CN 111394003 A discloses a curved screen explosion-proof film and its manufacturing method. The curved screen explosion-proof film includes a polyimide film, an adhesive layer and a release film, and the adhesive layer and the polyimide film Coating liquid is applied in between, the coating liquid is configured by polyester resin, silicone modified polyester resin and methyl ethyl ketone, and is used to improve the adhesion between the bonding layer and the polyimide layer, but , the explosion-proof film is only used for curved screens. Curved screens are bent and formed during the manufacturing process, and users will not bend or even fold the screen during subsequent use. Therefore, although the explosion-proof film can meet the explosion-proof requirements of curved screens, However, it cannot be applied to folding screens, and the antistatic performance and aging resistance of the explosion-proof film have not been improved.

Method used

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Examples

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preparation example Construction

[0035] The preparation method of explosion-proof film is:

[0036] (1) Weigh high-functionality urethane acrylate, antistatic flexible anti-aging agent, reactive diluent, photoinitiator, nanoparticles, anti-fingerprint agent and solvent in proportion, first disperse the nanoparticles in the solvent, grind them evenly, and then Add the remaining components and disperse evenly to obtain a hardening solution;

[0037] (2) uniformly coating the hardening solution prepared in step (1) on the polyimide film, then thermally drying to volatilize the solvent;

[0038] (3) Carry out UV curing, stick the protective film, and cut it as required.

Embodiment 1

[0040] (1) Weigh 40 parts of Etercure6145-100 (6 grades) of Changxing Chemical, 40 parts of Etercure6150-100 (6 grades) of Changxing Chemicals, 15 parts of antistatic flexible anti-aging agent (n=15), 5 parts of tripropylene glycol Diacrylate, 5 parts of trimethylolpropane triacrylate, 1 part of phenyl bis(2,4,6-trimethylbenzoyl) phosphine oxide, 10 parts of silane coupling agent KH-570 modified nano Silicon dioxide, 0.05 parts of anti-fingerprint agent, 40 parts of methyl ethyl ketone, 40 parts of isopropanol, first add the nano-silica modified by silane coupling agent KH-570 into the solvent and grind it evenly, then add the rest of the components Divide and disperse evenly to obtain hardening solution;

[0041] (2) Evenly coat the hardening solution on the polyimide film, and dry at 80-85°C for 7 minutes to evaporate the solvent;

[0042] (3) according to the illuminance 300mW / cm 2 , light intensity 600mJ / cm 2 , The film surface temperature is 40 ℃ UV curing conditions f...

Embodiment 2

[0044] (1) Weigh 60 parts of Etercure6150-100 (6 parts) of Changxing Chemical, 30 parts of Etercure_DR-U591 (10 parts) of Changxing Chemical, 20 parts of antistatic flexible anti-aging agent (n=14), 10 parts of tripropylene glycol Diacrylate, 5 parts of isobornyl methacrylate, 1 part of phenylbis(2,4,6-trimethylbenzoyl)phosphine oxide, 1 part of 2,4,6-trimethylbenzoyl di Phosphine phenoxide, 10 parts of nano silicon dioxide modified by silane coupling agent KH-570, 6 parts of nano titanium dioxide modified by silane coupling agent KH-570, 0.4 part of anti-fingerprint agent, 60 parts of propylene glycol monomethyl ether, 40 parts 1 part of n-butyl acetate, 20 parts of methyl ethyl ketone, first add nano-silica modified by silane coupling agent KH-570 and nano-titanium dioxide modified by silane coupling agent KH-570 into the solvent and grind evenly, and then add the remaining components Divide, disperse evenly to obtain hardening solution;

[0045] (2) Evenly coat the hardeni...

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Abstract

The invention belongs to the technical field of explosion-proof membranes, and particularly relates to an antistatic anti-aging polyimide explosion-proof membrane which comprises a polyimide layer and a hardened layer. The hardened layer is prepared from the following components in parts by weight: 80 to 100 parts of high-functionality polyurethane acrylate, 15 to 25 parts of an antistatic flexible anti-aging agent, 10 to 20 parts of a reactive diluent, 1 to 3 parts of a photoinitiator, 10 to 20 parts of nanoparticles, 0.05 to 1 part of an anti-fingerprint agent and 80 to 150 parts of a solvent. According to the explosion-proof membrane, the hardened layer is coated on the polyimide layer; polyimide is good in foldability but not good in hardness, and high-functionality polyurethane acrylate in the hardened layer can effectively improve the hardness and abrasion resistance of the hardened layer; and the antistatic flexible anti-aging agent not only can ensure that the hardened layer can be well bent along with the polyimide layer, but also can improve the antistatic performance and aging resistance of the anti-explosion membrane, so that the explosion-proof membrane is high in hardness and foldability, can effectively reduce static electricity generated in the production and use process, and is long in service life.

Description

technical field [0001] The invention belongs to the technical field of explosion-proof membranes, and in particular relates to an antistatic and aging-resistant polyimide explosion-proof membrane. Background technique [0002] Polyimide has excellent mechanical properties, heat resistance, low temperature resistance, flame retardancy, solvent resistance and electrical properties, and can be used as structural composite materials, electrical insulation materials, adhesives and coating materials, and is widely used in electronic micro Electronics, aerospace, optics, electromechanical and other fields. Especially in the field of microelectronics, polyimide is often used as a dielectric layer for interlayer insulation, as a buffer layer to reduce stress, as a protective layer to reduce environmental damage, and as a shielding layer to reduce device errors. Used in various electronic components such as substrates of flexible printed wiring circuits and alignment films for liquid...

Claims

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Application Information

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IPC IPC(8): C08J7/046C08J7/044C09D175/14C09D7/63C09D7/62C07C213/08C07C217/84
CPCC08J7/046C08J7/044C08J7/0427C09D175/14C09D7/63C09D7/62C07C213/00C07C213/04C07C213/06C07C213/08C08J2379/08C08J2475/14C08K2201/011C08K2003/2241C07C2601/14C08K5/18C08K9/06C08K3/36C08K3/22C07C217/84C07C215/12C07C217/10
Inventor 张玉贞
Owner 苏州欧纳克纳米科技有限公司
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