Method for preparing photocatalyst Cu2O based on recovering copper cutting waste
A technology for cutting waste and photocatalysts, applied in chemical instruments and methods, physical/chemical process catalysts, metal/metal oxides/metal hydroxide catalysts, etc., can solve the waste of resources and safety of electrochemical methods, raw materials for precipitation methods Huge, expensive equipment and other problems, to achieve the effect of low cost, low cost, high cost
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Embodiment 1
[0063] Preparation of photocatalyst Cu based on recycling copper cutting waste 2 O and the method for degrading methyl orange thereof are carried out in the following steps: in the present embodiment, the molten salt used is a chloride molten salt, specifically NaCl-CaCl 2 The mixture, by molar ratio, NaCl:CaCl 2 =0.479:0.521.
[0064] Step 1: NaCl and CaCl 2 salt pretreatment
[0065] (1) NaCl and CaCl 2 Grinding separately to obtain NaCl powder with a particle size of 2mm and CaCl with a particle size of 2mm 2 The powder is ground and poured into a beaker, placed in a muffle furnace and sealed;
[0066] (2) In a vacuum state, heat up to 300°C at a heating rate of 5°C / min and perform pretreatment at a constant temperature for 12 hours to obtain molten salt after dehydration treatment, and then cool down to room temperature to take out the molten salt to obtain dehydrated NaCl and dehydrated After CaCl 2 ;
[0067] Step 2: Pretreatment of Copper Cutting Scrap
[0068]...
Embodiment 2
[0084] Preparation of photocatalyst Cu based on recycling copper cutting waste 2 O and the method for degrading methylene blue thereof are carried out as follows: in the present embodiment, the molten salt used is a chloride molten salt, specifically NaCl-CaCl 2 The mixture, by molar ratio, NaCl:CaCl 2 =0.479:0.521.
[0085] Step 1: NaCl and CaCl 2 salt pretreatment
[0086] (1) NaCl and CaCl 2 Grinding separately to obtain NaCl powder with a particle size of 2mm and CaCl with a particle size of 2mm 2 The powder is ground and poured into a beaker, placed in a muffle furnace and sealed;
[0087] (2) In a vacuum state, at a heating rate of 3°C / min, the temperature was raised to 300°C and kept at a constant temperature for 12 hours for pretreatment to obtain dehydrated molten salt, and then cooled to room temperature to take out the molten salt to obtain dehydrated NaCl and CaCl after dehydration 2 ;
[0088] Step 2: Pretreatment of Copper Cutting Scrap
[0089]Place 1g ...
Embodiment 3
[0105] Preparation of photocatalyst Cu based on recycling copper cutting waste 2 The method of O comprises the following steps:
[0106] Step 1: Pretreatment of molten salt raw material
[0107] Place the molten salt raw material powder sodium carbonate with a particle size of 1mm in a muffle furnace, seal it, and in a vacuum state, raise the temperature to 300°C at a heating rate of 5°C / min and keep the temperature for 12h for dehydration treatment, and then cool the furnace To room temperature, sodium carbonate after dehydration is obtained;
[0108] Step 2: Pretreatment of Copper Cutting Scrap
[0109] Place the copper cutting waste in a muffle furnace, heat it to 1100°C in the air, and oxidize it at a constant temperature for 12 hours to obtain copper oxide powder;
[0110] Step 3: Assembly of reaction system and experimental process
[0111] (1) 100g of dehydrated molten salt raw material is placed in a cleaned and dried corundum crucible, and then the corundum crucib...
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