Polyolefin powder capable of uniform mixing with plant small piece and preparation method thereof
A polyolefin and powder technology, applied in the field of polyolefin powder and its preparation, can solve the problems of low utilization efficiency of refrigerants, large differences in ambient temperature, easy to cause frostbite, etc., and achieves weight reduction, large solvent loss, and enhanced solubility. Effect
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Embodiment 1
[0031] Put 1 kg of polyethylene pellets and 15 liters of xylene into a reflux stirring heating kettle, raise the temperature of the system to 140°C under stirring conditions, and reflux at this temperature until the polyethylene dissolves. After the temperature of the system was lowered to 100° C., it was slowly poured into a stirred mixing tank containing 15 liters of absolute ethanol, and the mixture was closed and stirred until the system dropped to room temperature. The material in the mixing kettle is suction-filtered under reduced pressure, the filter cake is crushed by a stone mill, and then dry-blended into powder. Put the obtained powder in a vacuum distillation kettle, add 10 liters of tap water at the same time, raise the temperature to 95°C under stirring conditions, depressurize with a water pump, and gradually increase the vacuum degree to ensure that the distillation process is carried out smoothly until there is no more xylene until steamed. The material in th...
Embodiment 2
[0038] Put 1 kg of recycled polyethylene film and bottle material and 20 liters of toluene into a reflux stirring heating kettle, raise the temperature of the system to 160°C under stirring conditions, and reflux at this temperature until the polyethylene dissolves. After the temperature of the system was reduced to 110° C., the floating impurities on the surface were floated off, and slowly poured into a stirring mixing kettle with 35 liters of absolute ethanol, and the bottom precipitated impurities were retained in the reflux stirring heating kettle when pouring. After pouring, close and stir until the system drops to room temperature. The material in the mixing kettle is suction filtered under reduced pressure, the filter cake is crushed by a stone mill, and then dry-stirred into powder with a four-leaf stick stirring device. Put the obtained powder in a vacuum distillation kettle, add 20 liters of tap water at the same time, raise the temperature to 95°C under stirring co...
Embodiment 3
[0040] Put 1 kg of recovered polyethylene, polystyrene, polypropylene mixed film and bottle material, 10 liters of toluene and 10 liters of xylene into the reflux stirring heating kettle, and raise the temperature of the system to 160 ° C under stirring conditions, and in this Reflux at temperature until the polyethylene dissolves. After the temperature of the system is reduced to 110° C., the impurities floating on the surface are floated off, and slowly poured into a stirring mixing kettle with 40 liters of absolute ethanol, and the precipitated impurities at the bottom are retained in the reflux stirring heating kettle when pouring. After pouring, close and stir until the system drops to room temperature. The material in the mixing kettle is suction-filtered under reduced pressure, the filter cake is crushed by a stone mill, and then dry-blended into powder. Put the obtained powder in a vacuum distillation kettle, add 15 liters of tap water at the same time, raise the temp...
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