Method for preparing indium tin oxide-indium oxide thin film thermocouple with crystal face preferred orientation
A preferred orientation, thermocouple technology, applied in thermometers, mechanical equipment, heat measurement and other directions that use directly heat-sensitive electrical/magnetic components, can solve problems that affect heat conduction efficiency, cannot measure transient temperature, and difficult thermal balance, etc., Achieve the effects of not easy to fall off, high stability, high Seebeck coefficient and sensitivity
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Embodiment 1
[0030] Embodiment 1 provides a method for preparing a crystal plane preferred orientation film thermocouple on a metal surface, comprising the following steps:
[0031] Step 1, deposit yttrium-stabilized zirconia (YSZ) bonding coating on the metal workpiece surface by physical vapor deposition process, Al in the evaporated powder of described physical vapor deposition process 2 o 3 The mole percentage is more than 3%, so that the bonding coating is an insulating coating;
[0032] Step 2. Prepare a thin-film thermocouple with a preferred crystal plane orientation on the bonding coating by a magnetron sputtering process. The thin-film thermocouple includes two thermoelectric arms and two electrodes; one of the thermoelectric arms is deposited on an indium tin oxide target. The other part of the thermoelectric arm is deposited from an indium oxide target, and the electrode is deposited from a platinum target and an iridium target;
[0033] Step 3, heat-treating the metal workpi...
Embodiment 2
[0041] Embodiment 2 provides a method for preparing a crystal plane preferred orientation film thermocouple on a metal surface, comprising the following steps:
[0042] Step 1, deposit yttrium-stabilized zirconia (YSZ) bonding coating on the metal workpiece surface by physical vapor deposition process, Al in the evaporated powder of described physical vapor deposition process 2 o3 The mole percentage is more than 3%, so that the bonding coating is an insulating coating;
[0043] Step 2. Prepare a thin-film thermocouple with a preferred crystal plane orientation on the bonding coating by a magnetron sputtering process. The thin-film thermocouple includes two thermoelectric arms and two electrodes; one of the thermoelectric arms is deposited on an indium tin oxide target. The other part of the thermoelectric arm is deposited from an indium oxide target, and the electrode is deposited from a platinum target and an iridium target;
[0044] Step 3, heat-treating the metal workpiec...
Embodiment 3
[0052] Embodiment 3 provides a method for preparing a crystal plane preferred orientation film thermocouple on a metal surface, comprising the following steps:
[0053] Step 1, deposit yttrium-stabilized zirconia (YSZ) bonding coating on the metal workpiece surface by physical vapor deposition process, Al in the evaporated powder of described physical vapor deposition process 2 o 3 The mole percentage is more than 3%, so that the bonding coating is an insulating coating;
[0054] Step 2. Prepare a thin-film thermocouple with a preferred crystal plane orientation on the bonding coating by a magnetron sputtering process. The thin-film thermocouple includes two thermoelectric arms and two electrodes; one of the thermoelectric arms is deposited on an indium tin oxide target. The other part of the thermoelectric arm is deposited from an indium oxide target, and the electrode is deposited from a platinum target and an iridium target;
[0055] Step 3, heat-treating the metal workpi...
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