A kind of flat polyester fiber fdy yarn and preparation method thereof
A polyester fiber, flat technology, applied in the field of flat polyester fiber FDY yarn and its preparation, can solve the problems of poor product shape retention, weakening extrusion expansion ratio, reducing export expansion, etc., and achieves good protection. shape effect, reduce extrusion expansion ratio, reduce the effect of outlet expansion
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Embodiment 1
[0047] A preparation method of flat polyester fiber FDY filaments, the spinning melt is metered, extruded, cooled, oiled, stretched, heat-set and wound to obtain polyester fiber FDY filaments;
[0048] First prepare the spinning melt, make the monomer of terephthalic acid and ethylene glycol into slurry, wherein the molar ratio of terephthalic acid and ethylene glycol is 1:1.2, then add catalyst, stabilizer and saturated fatty acid After the metal salt is mixed evenly, the esterification reaction is carried out. The esterification reaction is pressurized in a nitrogen atmosphere. The pressurized pressure is normal pressure, and the temperature of the esterification reaction is 250°C. When the value is above 90%, it is the end point of the esterification reaction; then after the end of the esterification reaction, the polycondensation reaction in the low vacuum stage starts under the condition of negative pressure. At 260°C, the reaction time is 30 minutes; then continue to vac...
Embodiment 2
[0067] A preparation method of flat polyester fiber FDY filaments, the spinning melt is metered, extruded, cooled, oiled, stretched, heat-set and wound to obtain polyester fiber FDY filaments;
[0068] First prepare the spinning melt, make the monomer of terephthalic acid and ethylene glycol into slurry, wherein the molar ratio of terephthalic acid and ethylene glycol is 1:2.0, then add catalyst, stabilizer and saturated fatty acid After the metal salt is mixed evenly, the esterification reaction is carried out. The esterification reaction is pressurized in a nitrogen atmosphere. The pressurized pressure is 0.3MPa, and the temperature of the esterification reaction is 260°C. When the value is above 90%, it is the end point of the esterification reaction; then after the end of the esterification reaction, the polycondensation reaction in the low vacuum stage starts under the condition of negative pressure. At 270°C, the reaction time is 50 minutes; then continue to vacuumize, c...
Embodiment 3
[0089] A preparation method of flat polyester fiber FDY filaments, the spinning melt is metered, extruded, cooled, oiled, stretched, heat-set and wound to obtain polyester fiber FDY filaments;
[0090] First prepare the spinning melt, make the monomer of terephthalic acid and ethylene glycol into slurry, wherein the molar ratio of terephthalic acid and ethylene glycol is 1:1.6, then add catalyst, stabilizer and saturated fatty acid After the metal salt is mixed evenly, the esterification reaction is carried out. The esterification reaction is pressurized in a nitrogen atmosphere. The pressurized pressure is 0.2MPa, and the temperature of the esterification reaction is 255°C. When the value is above 90%, it is the end point of the esterification reaction; then after the end of the esterification reaction, the polycondensation reaction in the low vacuum stage starts under the condition of negative pressure. At 265°C, the reaction time is 40 minutes; then continue to vacuumize, c...
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