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Manufacturing method of ultra-fine grain high-temperature alloy plate blanks

A technology of high temperature resistant alloy and high temperature alloy, which is applied in the field of manufacturing of high temperature resistant alloy disc blanks, can solve the problems of small process window, as-cast alloy segregation, difficult realization, etc., and achieves the effect of excellent high temperature strength and fatigue resistance.

Active Publication Date: 2013-04-03
BAOSHAN IRON & STEEL CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

Due to the continuous increase of strengthening elements, the thermal process performance deteriorates, and it can no longer be deformed by thermal processing. It can only be used in the as-cast state, and the as-cast alloy has serious segregation, which cannot meet the needs of new engines.
[0004] Chinese patent CN101307402 introduces thermal deformation processing technology, and the process window is small
Since there is no large-tonnage extrusion equipment in our country, the extrusion + superplastic forging process cannot be implemented; for isothermal forging and superplastic forging, fully enclosed forging equipment and devices under the protection of vacuum or inert gas and large-tonnage special presses for isothermal forging are required. huge investment
Therefore, foreign methods are currently difficult to implement in my country. The lack of large-tonnage extruders, isothermal forging presses, and fully enclosed forging equipment has become a major obstacle restricting the development of my country's large-scale powder superalloy disc manufacturing technology.

Method used

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  • Manufacturing method of ultra-fine grain high-temperature alloy plate blanks
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  • Manufacturing method of ultra-fine grain high-temperature alloy plate blanks

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Embodiment 1

[0038] see figure 1 , the manufacturing method of ultra-fine-grained high-temperature-resistant alloy disc blank of the present invention, it comprises the steps:

[0039] 1) Preparation of superalloy powder,

[0040] Superalloy powder is prepared by vacuum melting, argon or helium atomization method, using argon or helium as the atomizing gas, the purity of argon or helium is required to be greater than 99.999%; the superalloy melting process is required in the powder making process The superheat range of the liquid is 150, the powder is spherical, and the particle size range is: 5-25μm;

[0041] 2) heat treatment of superalloy powder,

[0042] After the superalloy powder is prepared, put the powder into a vacuum atmosphere furnace for heat treatment, firstly carry out reduction annealing treatment at 600°C under the protection of 4000°C hydrogen; control the oxygen content of the final powder to less than 20ppm; then pump out the hydrogen in the furnace, vacuum Degree Req...

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Abstract

The invention discloses a manufacturing method of ultra-fine grain high-temperature alloy plate blanks. The manufacturing method comprises the following steps of 1, preparation of high-temperature alloy powder; 2, heat treatment of the high-temperature alloy powder; 3, selection of a high-temperature alloy core tube; 4, high-temperature spray deposition and composite recrystallization of plate blanks; and 5, heat treatment of the plate blanks, and finally forming the high-temperature alloy plate blanks in ultra-fine microstructures. According to the manufacturing method disclosed by the invention, the high-temperature alloy powder is prepared by adopting a gas atomization technology, and the obtaining of an oxygen-free and segregation-free well-closed formation is controlled through a heat treatment system; the element composition is controlled by selecting the high-temperature alloy core tube, and the real-time control for the temperature during a forming process is controlled; and the forming of high-temperature alloy is carried out on the outer surface of the high-temperature alloy core tube by adopting the high-temperature spray deposition technology, the composite recrystallization is synchronously carried out, the growth of grains in the microstructure is controlled as a large temperature gradient is simultaneously formed, and the high-temperature alloy plate blanks in the ultra-fine microstructures are finally formed through the heat treatment. According to the manufacturing method disclosed by the invention, the microstructure of the plate blanks is compact, the size is large, and most of all, a forging machine or an extrusion device in large tonnage is not needed.

Description

technical field [0001] The invention relates to a manufacturing technology of a high-temperature-resistant alloy blank, in particular to a manufacturing method of an ultra-fine-grained high-temperature alloy blank. Background technique [0002] Superalloys are important metal materials necessary for modern aero-engines, rocket engines, and gas turbines. It can withstand greater stress and be used for a long time under high temperature (generally 600-900°C), oxidizing atmosphere and gas corrosion conditions. High-temperature alloy turbine discs are high-temperature alloy products, and the most used ones are gas turbine discs and aircraft turbine discs. [0003] Turbine discs for aircraft, the center of the disc is subject to low temperature and high stress, and requires fine-grained structure to ensure sufficient tensile strength and fatigue resistance, while the edge is subjected to high temperature and low stress, requiring coarse grains to ensure sufficient creep and dura...

Claims

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Application Information

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IPC IPC(8): B22F3/115
Inventor 张俊宝张宇军梁永立
Owner BAOSHAN IRON & STEEL CO LTD
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