Application of lead or copper ion test paper in detection of bleaching toner residue
A technology of copper ions and color enhancers, which is applied in the field of physical and chemical analysis of chemical substances, can solve the problems of safe use of traditional Chinese medicinal materials, hidden dangers of Chinese herbal decoction pieces, high processing conditions of toxic reagent tetrachloro amalgam, and high requirements for detection environment, and achieves elimination of background. Color interference, reduced processing complexity, low-cost effects
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Embodiment 1
[0041] Example 1: Using lead acetate test paper to prepare a kit for detecting residual bleaching and coloring agents in Chinese medicinal materials and Chinese medicinal pieces
[0042] This embodiment is a preferred embodiment of using lead acetate test paper to prepare a kit for detecting residual bleaching and coloring agents in Chinese medicinal materials and Chinese medicinal pieces. The kit includes a cecillin bottle containing sodium hydroxide solution, A cecillin bottle with arsenic-free zinc particles, hydrochloric acid solution and lead acetate test paper. Wherein, the mass volume percentage concentration of the sodium hydroxide solution is 0.125%, and its volume is 10 ml. The specification of the cecillin bottle containing the sodium hydroxide solution is 15 ml. The specification of the cecillin bottle with arsenic-free zinc particles is 10ml, and the total mass of arsenic-free zinc particles is 0.2 grams. The lead acetate test paper is a qualitative filter paper wit...
Embodiment 2
[0043] Example 2: Use the kit in Example 1 to perform color reaction of standard products
[0044] In this embodiment, sodium sulfite and sodium bisulfite are used as standard products. Take about 10g each of sodium sulfite and sodium bisulfite standards and put them in a 100ml measuring flask, add purified water or distilled water to dissolve and dilute to the mark, as the respective standard stock solutions.
[0045] Take the above-mentioned stock solutions to prepare the mass volume percentage concentrations of 0.0001%, 0.0002%, 0.0005%, 0.001%, 0.002%, 0.005%, 0.01%, 0.02%, 0.05%, 0.1%, 0.2%, 0.5%, 1% respectively , 2%, 5%, 10% and other standard solutions, and take 2ml respectively for color reaction according to the following steps:
[0046] (1) Sample processing
[0047] The sampling amount of Chinese herbal medicines and Chinese herbal medicine pieces is about 1g. Cut (or grind) the sample into fine particles with scissors (or grinding) and set aside.
[0048] (2) Preparation...
Embodiment 3
[0053] Example 3: Use the kit in Example 1 to perform the color reaction of the sample
[0054] First, prepare the test solution. Place the processed sample in a sescillin bottle containing 10ml of 0.125% sodium hydroxide solution, the size of the bottle is 15ml, tighten the stopper, shake vigorously for 1-2 minutes, let it stand for a while, wait for layering , Take 2ml of the upper solution (filter if necessary) as the test solution. Then proceed to color reaction. Put 2ml of the above test solution in a vial containing arsenic-free zinc granules. Among them, there are 2 arsenic-free zinc granules, about 0.2g, the size of the vial is 10ml, then add 2ml of hydrochloric acid solution, gently Shake to mix evenly, and immediately put the lead acetate test paper on the bottle mouth. The final judgment result. If it turns yellowish-brown to silver-black within 10 minutes, it can be judged that the sample may contain bleaching color enhancing agents such as sulfur dioxide, sulfite...
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