Preparation method of superfine ceramic powder injection molding mixture
A ceramic powder and injection molding technology, which is applied in ceramic molding machines, clay preparation devices, chemical instruments and methods, etc., can solve problems such as cracking and bubbling, difficulty in dispersing, and difficult control of degreasing rate
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Embodiment 1
[0017] The ratio of ceramic powder and organic binder is shown in the table below (percentage by weight):
[0018] Zirconia
ceramic powder
butyral
polyethylene two
oxidation
olefin wax
sour
Microcrystalline Paraffin
terephthalate
Formic acid two
Butyl ester
87
1.5-2.0
6.5-8.5
0.6-1.7
0.65
0.65-0.80
0.5
[0019] Take the preparation of 1kg injection mixture as an example. Fully dissolve 6.5g of stearic acid into an appropriate amount of ethanol solution, the temperature of ethanol is 40°C, and then add 870g of zirconia ceramic powder into the solution. Then ultrasonically disperse for 30 minutes, ultrasonic power, and then stir for 2 hours; or ball mill for 12 hours, rotating speed r / min. Then the slurry is dried and the etha...
Embodiment 2
[0022] The ratio of ceramic powder and organic binder is shown in the table below (percentage by weight):
[0023] Aluminum oxide
ceramic powder
Polymethylpropane
polyethylene
Polyoxygen
Chemical B
ene
Oxidized poly
vinyl wax
sour
Ceramic stone
the wax
terephthalate
Formic acid two
Butyl ester
89
0.9-1.2
0.9-1.2
5.0-7.0
0.55-1.65
0.75
0.65-0.8
0.45
[0024] The surface modification method of alumina powder is the same as Example 1. The surface-modified powder is mixed with polymethyl methacrylate, polymethyl methacrylate open mill or twin-screw mixer for 10 minutes, and the mixing temperature is 180°C. Then the temperature of the kneader was lowered to 130°C, and the oxidized polyethylene wax, polyethylene wax and microcrystalline paraffin wax w...
Embodiment 3
[0027] The ratio of ceramic powder and organic binder is shown in the table below (percentage by weight):
ceramic powder
polyethylene
butyral
vinyl ester co
polyethylene two
oxidation
polyethylene
olefin wax
Terephthalate
dioctyl ester
83
1.3-2.2
0.8-1.6
8.5-11.1
0.7-2.0
0.8
0.7
[0029] The surface modification method of the silicon nitride powder is the same as that of Example 1. The surface-modified powder is mixed with polyvinyl butyral and ethylene vinyl acetate copolymer for 10 minutes on an open mill or a twin-screw mixer, and the mixing temperature is 170°C. Then lower the temperature of the mixer to 130° C., add oxidized polyethylene wax and polyethylene glycol, and knead for 15 minutes. Then lower the temperature...
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