Atomization spray disc, spherical silicon boride ceramic powder, and preparation method and application of spherical silicon boride ceramic powder
A technology of ceramic powder and atomization spraying, applied in the direction of spray evaporation, etc., can solve the problems of inconvenient research and application of electronic functional materials, uneven thickness of coating surface, uneven coating state, etc.
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[0020] The existing preparation methods of silicon boride powder materials such as ball milling, vapor deposition or thermal phase sintering, etc., the obtained powders are all non-spherical, the friction between the piled state is large, and the fluidity is poor. The gravity conveying applied on the spraying equipment In the air-flow conveying method, the powder is in the conveying pipeline, which is prone to jams and pauses, intermittent powder feeding, and in severe cases, flow interruption will occur; resulting in uneven thickness of the coating surface during the spraying process, and uneven coating status at different positions , it is expected that the corresponding function of the coating will be seriously affected, and even cause the workpiece to be scrapped. The composition uniformity of the powder prepared by the above method is also poor, the deviation is large and the controllability is poor, which will also affect the performance of the coating to varying degrees;...
Embodiment 1
[0023] In order to solve the above technical problems, such as figure 1 As shown, the present invention firstly provides a kind of atomizing spraying plate, comprises: liquid guide tube 3; Enter the catheter tube 3; and the atomized gas inlet pipe 1 located on both sides of the catheter tube 3, which is provided with a spray hole 2 near the end of the catheter tube 3; the atomized gas is suitable for spraying holes from both sides 2 spraying to crush the melt to form powder particles.
[0024] Specifically, the atomizing spray pan can obtain converging high-speed and high-kinetic airflow, and the intersection of the airflow is close to the outlet of the catheter melt, and the high-speed airflow obtained by the airflow leaving the nozzle hole can quickly contact and crush the melt before the kinetic energy is weakened, Obtain ultra-fine powder particles.
[0025] Optionally, the nozzle hole 2 may include, but is not limited to, several closely coupled nozzle holes with an ato...
Embodiment 2
[0030] On the basis of Example 1, the present invention also provides a method for preparing spherical silicon boride ceramic powder, comprising the following steps: step S1, preparing silicon-boron composite block; step S2, heat-melting the silicon-boron composite block After the melt is formed, it is injected into the atomizing spray pan as described in Example 1, and the melt is atomized into fine powder particles under the effect of the protective air flow, and shrinks into balls under the action of surface tension during the atomization flight process. After cooling, it forms spherical silicon boride ceramic powder particles.
[0031] Wherein, optionally, the silicon-boron composite block may include, but not limited to, the following components in parts by mass: Si is 96.2-98.5 parts; B is 1.5-3.8 parts.
[0032] Optionally, the step of preparing the silicon-boron composite material block in the step S1 may be: using arc energy to melt silicon and boron in a vacuum non-c...
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