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Preparation method of material with good wave-absorbing effect

A good, wave-absorbing agent technology, applied in the field of material preparation with good wave-absorbing effect, can solve the problems of network collapse, increased internal stress in the composite system, easy to agglomerate, etc., to improve utilization, increase wave-absorbing performance and The effect of heat resistance

Pending Publication Date: 2020-07-10
苏州中亿兴新材料科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] The prior art uses rubber such as polysulfide rubber, hydroxy-terminated butyl rubber, etc. to modify epoxy resins, but this method will cause a great loss of mechanical properties and high-temperature performance of the resin; Dielectric properties can improve toughness and high temperature resistance and reduce internal stress, but the compatibility between silicone resin and epoxy resin is poor; the method of adding rigid particles to epoxy resin can reduce material cost and control the thermal expansion and Shrinkage can increase the tensile elastic modulus of the material, but it will increase the internal stress of the epoxy resin composite system, and the base materials of the existing wave-absorbing materials include FR-4 materials, ceramic materials, ferroelectric materials, iron Oxygen materials, etc. Some patent documents disclose the use of transition metal-based aerogels, transition metal oxide aerogels, and composite transition metal oxide aerogels as wave-absorbing materials, and iron oxide aerogels are typically used Realized iron-based materials
FR-4 material is heavy and cannot meet the "lightweight" requirements in many environments. For ferric oxide airgel, if it is directly used as a wave-absorbing material, the absorbing effect will not be good. If the ferric oxide If the aerogel is directly reduced to nano-iron, the network will collapse with the loss of oxygen during the reduction process, and the nanopores will disappear, and the remaining iron is also prone to agglomeration due to its own magnetic field, so it is impossible to realize the nano-sized iron and Lightweight of the entire absorbing material

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0026] A method for preparing a material with good wave-absorbing effect, comprising the following raw materials in parts by weight: 90-110 parts of epoxy resin, 10-30 parts of plastic microspheres, 4-10 parts of curing agent, 5-15 parts of accelerator, Wave agent 50-150 parts, airgel 50-70 parts, thermoplastic resin 10-30 parts, magnetic metal powder 30-50 parts, water 60-80 parts, including the following steps:

[0027] S1. Weighing materials: 70 parts of water, 20 parts of plastic microspheres, 60 parts of airgel, 20 parts of thermoplastic resin, 40 parts of magnetic metal powder;

[0028] S2, beating and dispersing: pour the raw materials into the dispersing and beating machine for beating and dispersing treatment, and beat different types of classification;

[0029] S3. Material transportation: move the material after beating and dispersion treatment to the inside of the grinder;

[0030] S4. Material grinding: turn on the grinder, and the grinder runs to efficiently gri...

Embodiment 2

[0045] A method for preparing a material with good wave-absorbing effect, comprising the following raw materials in parts by weight: 90-110 parts of epoxy resin, 10-30 parts of plastic microspheres, 4-10 parts of curing agent, 5-15 parts of accelerator, Wave agent 50-150 parts, airgel 50-70 parts, thermoplastic resin 10-30 parts, magnetic metal powder 30-50 parts, water 60-80 parts, including the following steps:

[0046] S1. Weighing materials: 60 parts of water, 10 parts of plastic microspheres, 50 parts of airgel, 10 parts of thermoplastic resin, 30 parts of magnetic metal powder;

[0047] S2, beating and dispersing: pour the raw materials into the dispersing and beating machine for beating and dispersing treatment, and beat different types of classification;

[0048] S3. Material transportation: move the material after beating and dispersion treatment to the inside of the grinder;

[0049] S4. Material grinding: turn on the grinder, and the grinder runs to efficiently gri...

Embodiment 3

[0064] A method for preparing a material with good wave-absorbing effect, comprising the following raw materials in parts by weight: 90-110 parts of epoxy resin, 10-30 parts of plastic microspheres, 4-10 parts of curing agent, 5-15 parts of accelerator, Wave agent 50-150 parts, airgel 50-70 parts, thermoplastic resin 10-30 parts, magnetic metal powder 30-50 parts, water 60-80 parts, including the following steps:

[0065] S1. Weighing materials: 80 parts of water, 30 parts of plastic microspheres, 70 parts of airgel, 30 parts of thermoplastic resin, and 50 parts of magnetic metal powder;

[0066] S2, beating and dispersing: pour the raw materials into the dispersing and beating machine for beating and dispersing treatment, and beat different types of classification;

[0067] S3. Material transportation: move the material after beating and dispersion treatment to the inside of the grinder;

[0068] S4. Material grinding: turn on the grinder, and the grinder runs to efficiently...

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Abstract

The invention discloses a preparation method of a material with a good wave-absorbing effect. The wave-absorbing material comprises the following raw materials in parts by weight: 90-110 parts of epoxy resin, 10-30 parts of plastic microspheres, 4-10 parts of a curing agent, 5-15 parts of an accelerant, 50-150 parts of a wave-absorbing agent, 50-70 parts of aerogel, 10-30 parts of thermoplastic resin, 30-50 parts of magnetic metal powder and 60-80 parts of water. Through formulations by neutralization, an aerogel material is used as a carrier; magnetic metal powder, such as an iron material, is deposited into the aerogel; then thermoplastic resin is added; the insulation characteristic of the thermoplastic resin is utilized; the thermoplastic wave-absorbing material is prepared; the composite wave-absorbing material substrate with high resistivity is prepared, thermoset of epoxy resin and plastic microspheres is utilized; the curing reaction of the epoxy resin is improved by adding thecuring agent and the accelerant, so that the overall wave-absorbing performance and heat resistance of the wave-absorbing material are improved, the density of the composite material is reduced, theantistatic effect is improved, the material is lightened, and the utilization rate of the material is increased.

Description

technical field [0001] The invention relates to a production process of a wave-absorbing material, more specifically, to a method for preparing a material with a good wave-absorbing effect. Background technique [0002] With the development of modern science and technology, the impact of electromagnetic radiation on the environment is increasing. At airports and airplanes, flights are delayed due to electromagnetic wave interference, and in hospitals and mobile phones often interfere with the normal work of various electronic diagnostic and therapeutic instruments. Electromagnetic radiation causes direct and indirect damage to the human body through thermal effects, non-thermal effects, and cumulative effects. Research It is confirmed that ferrite absorbing material has the best performance, and it has the characteristics of high absorption frequency band, high absorption rate, and thin matching thickness. Applying this material to electronic equipment can absorb leaked ele...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09D163/00C09D5/32C09D5/24C09D5/38C09D7/61
CPCC08L2201/04C08L2201/08C08L2205/03C08L2205/18C09D5/24C09D5/32C09D5/38C09D7/61C09D7/70C09D163/00C08L101/00C08L23/06C08L27/06C08L25/06C08L77/00C08L69/00C08K3/08C08K7/26C08K3/04
Inventor 侯腾腾冯楠
Owner 苏州中亿兴新材料科技有限公司
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