Preparation technology of catalyst used for high temperature catalytic decomposition of N2O
A high-temperature catalysis and preparation technology, which is applied in metal/metal oxide/metal hydroxide catalysts, physical/chemical process catalysts, nitrous oxide capture, etc. Component loss and other problems, to achieve the effect of uniform appearance, low resistance, and not easy to lose
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Embodiment 1
[0029] A high-temperature catalytic decomposition of N 2 The preparation technology of the catalyst of O is characterized in that, described production technology comprises the steps:
[0030] (1) 10 parts of zirconium nitrate, 75 parts of cerium nitrate, 4 parts of cobalt nitrate, 0.5 part of lanthanum nitrate, 0.1 part of nickel nitrate and 0.1 part of magnesium nitrate are dissolved in deionized water to form nitrate Mixed solution, the dissolution temperature is 60°C; the concentration of the nitrate mixed solution is 200g / L; then dropwise add ammonia water with a mass percentage concentration of 15% in the nitrate mixed solution until the pH of the mixed solution is 7.0; After completion, the mixed solution was heated up to 70°C, kept at 70°C and stirred for 2 hours, then added aluminum hydroxide and stirred evenly, then pressed and dehydrated to obtain a precipitate with a water content of 40% by mass;
[0031] (2) Dry the precipitate with a water mass percentage of 40%...
Embodiment 2
[0034] A high-temperature catalytic decomposition of N 2 The preparation technology of the catalyst of O is characterized in that, described production technology comprises the steps:
[0035] (1) 15 parts of zirconium nitrate, 85 parts of cerium nitrate, 10 parts of cobalt nitrate, 2 parts of lanthanum nitrate, 1 part of nickel nitrate and 0.5 part of magnesium nitrate are dissolved in deionized water to form nitrate Mixed solution, the dissolution temperature is 100°C; the concentration of the nitrate mixed solution is 220g / L; then dropwise add ammonia water with a mass percentage concentration of 20% in the nitrate mixed solution until the pH of the mixed solution is 10.0; After completion, the mixed solution was heated up to 90°C, kept at 90°C and stirred for 5 minutes, then added aluminum hydroxide and stirred evenly, then pressed and dehydrated to obtain a precipitate with a water content of 60% by mass;
[0036] (2) Dry the precipitate with a water mass percentage of 6...
Embodiment 3
[0039] A high-temperature catalytic decomposition of N 2 The preparation technology of the catalyst of O is characterized in that, described production technology comprises the steps:
[0040] (1) 80 parts of cerium nitrate, 12.5 parts of zirconium nitrate, 7 parts of cobalt nitrate, 1.25 parts of lanthanum nitrate, 0.5 part of nickel nitrate and 0.3 part of magnesium nitrate are dissolved in deionized water to form nitrate For the mixed solution, the dissolution temperature is 80°C; the concentration of the mixed nitrate solution is 210g / L; then, dropwise add ammonia water with a concentration of 17.5% by mass in the mixed solution until the pH of the mixed solution is 8.0; After completion, the mixed solution was heated up to 80°C, kept at 80°C and stirred for 3.5 hours, then added aluminum hydroxide and stirred evenly, then pressed and dehydrated to obtain a precipitate with a water content of 50% by mass;
[0041] (2) Dry the precipitate obtained in step (1) with a water ...
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