Dental repairing and filling composition, and preparation method thereof

A filling composition, dental technology, applied in dental preparations, dentistry, dental prosthesis and other directions, can solve the problems of low hardness, unstable teeth, poor wear resistance, etc., achieve excellent mechanical properties, maintain beautiful appearance, and comprehensive performance. Effect

Inactive Publication Date: 2016-12-14
林春梅
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the bonding property of light-cured composite resin is poor, and the volume and thermal expansion coefficient of light-cured composite resin are inconsistent with those of the tooth body, so it is prone to instability between teeth, gaps on the period...

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0020] A dental restorative filling composition, made of the following components by weight: 23 parts of fluorapatite, 5 parts of calcium phosphite, 4 parts of epoxy acrylate, 3 parts of diethyl acetonyl phosphonate, poly 4 parts of ethylene glycol diacrylate, 1-3 parts of hydroxyethylene phosphonic acid, 2 parts of calcium silicate hydrate, 3 parts of hyaluronic acid, 2 parts of polyether ether ketone, 1.1 parts of strontium hydrogen phosphate, 0.6 parts of bismuth oxide 0.4 parts of beryllium oxide, 1 part of talc, 3 parts of barium sulfate, 1 part of benzoyl peroxide, 2.8 parts of methyl-β-cyclodextrin, 1 part of sodium carboxymethyl cellulose, 1 part of gelatin, phosphorus Acylcholine 2 parts, boron trifluoride amine 1.2 parts.

[0021] The preparation method of described dental restoration filling composition comprises the following preparation steps:

[0022] Step (1) Mix fluorapatite, calcium phosphite, talcum powder, bismuth oxide, beryllium oxide, barium sulfate and ...

Embodiment 2

[0027] A dental restorative filling composition, made of the following components by weight: 35 parts of fluorapatite, 14 parts of calcium phosphite, 11 parts of epoxy acrylate, 8 parts of diethyl acetonyl phosphonate, poly 8 parts of ethylene glycol diacrylate, 3 parts of hydroxyethylene phosphonic acid, 6 parts of calcium silicate hydrate, 7 parts of hyaluronic acid, 5.5 parts of polyether ether ketone, 3.2 parts of strontium hydrogen phosphate, 1.8 parts of bismuth oxide, 2.2 parts of beryllium oxide, 4 parts of talc, 6 parts of barium sulfate, 5 parts of benzoyl peroxide, 6 parts of methyl-β-cyclodextrin, 4 parts of sodium carboxymethyl cellulose, 6 parts of gelatin, phosphoryl choline 5 parts of alkali, 3.5 parts of boron trifluoride amine.

[0028] The preparation method of described dental restoration filling composition comprises the following preparation steps:

[0029] Step (1) Mix fluorapatite, calcium phosphite, talcum powder, bismuth oxide, beryllium oxide, bariu...

Embodiment 3

[0034] A dental restorative filling composition, made of the following components by weight: 26 parts of fluorapatite, 6 parts of calcium phosphite, 5 parts of epoxy acrylate, 3.5 parts of diethyl acetonyl phosphonate, poly 4.5 parts of ethylene glycol diacrylate, 1.2 parts of hydroxyethylene phosphonic acid, 2.4 parts of calcium silicate hydrate, 3.4 parts of hyaluronic acid, 2.4 parts of polyether ether ketone, 1.4 parts of strontium hydrogen phosphate, 0.7 parts of bismuth oxide, 0.6 parts of beryllium oxide, 1.32 parts of talc powder, 3.4 parts of barium sulfate, 1.6 parts of benzoyl peroxide, 3 parts of methyl-β-cyclodextrin, 1.6 parts of sodium carboxymethyl cellulose, 1.3 parts of gelatin, phosphoryl choline 2.4 parts of alkali, 1.8 parts of boron trifluoride amine.

[0035] The preparation method of described dental restoration filling composition comprises the following preparation steps:

[0036] Step (1) Mix fluorapatite, calcium phosphite, talcum powder, bismuth o...

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Abstract

The invention discloses a dental repairing and filling composition and the preparation method thereof. The dental repairing and filling composition is prepared from the following components: fluorapatite, calcium phosphite, epoxy acrylate, diethyl(2-oxopropyl)phosphonate, poly(ethylene glycol) diacrylate, HEDP, tobermorite, hyaluronic acid, polyether-ether-ketone, strontium hydrogen phosphate, bismuth oxide, beryllium oxide, talcum powder, barium sulfate, benzoyl peroxide, methylated beta-cyclodextrin, sodium carboxymethylcellulose, gelatin, phosphorylcholine and boron trifluoride amine. The bending intensity of the dental repairing and filling composition can reach 86-94 MPa, the flexural modulus can reach 9.8-11.3 GPa, the modulus of compression can reach 6.9-7.5 MPa, the mechanical property is excellent, appearance and color stability to strong tea is higher than 4.5, the appearance beauty can be kept enduringly, the comprehensive performance is excellent, and the dental repairing and filling composition is very suitable for serving as a dental repairing and filling material to be popularized and used extensively.

Description

technical field [0001] The invention belongs to the technical field of biomedical materials, and in particular relates to a dental restoration filling composition and a preparation method thereof. Background technique [0002] Nowadays, with the changes in people's life, eating habits and structure, the wear and tear of oral teeth is becoming more and more serious, and it is more and more common for people to suffer from oral diseases. In many dental restorations, a restorative filling is used. At present, the restoration and filling materials mainly include light-curing composite resin and glass ionomer cement. Among them, the main mechanism of light-curing composite resin is to perform acid etching and decalcification treatment on the surface of dentin and enamel, and then use resin to fill and restore the tooth, and then light-cure layer by layer to form a tooth body with a natural tooth appearance. However, light-cured composite resins have poor adhesion, and the volum...

Claims

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Application Information

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IPC IPC(8): A61K6/027A61K6/033A61K6/087A61K6/097A61K6/838A61K6/891A61K6/898
CPCA61K6/831A61K6/838A61K6/891A61K6/898C08L5/08C08L5/16C08L1/286C08L71/02C08L61/16
Inventor 林春梅
Owner 林春梅
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