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Alloy design method for reducing directionally-solidified titanium aluminum alloy interface reaction

A technology of directional solidification, titanium-aluminum alloy, used in self-solidification methods, chemical instruments and methods, single crystal growth, etc.

Inactive Publication Date: 2016-05-25
CHINA UNIV OF MINING & TECH
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Problems solved by technology

[0007] Technical issues: This paper focuses on the titanium-aluminum alloy castings with different Nb contents obtained by directional solidification, and faces the problems of contamination and reaction with the casting coating material due to high temperature during the entire directional solidification process. Phase change and hardness distribution are used to evaluate the degree of interface reaction of corresponding castings, in order to find the best alloy composition ratio, thereby improving the quality of titanium-aluminum alloy castings and reducing the cost of subsequent processing

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  • Alloy design method for reducing directionally-solidified titanium aluminum alloy interface reaction
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  • Alloy design method for reducing directionally-solidified titanium aluminum alloy interface reaction

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Embodiment Construction

[0020] A method to measure the reaction degree of the interface between the titanium aluminum alloy and the casting coating.

[0021] (1) Master ingot casting. The experimental raw materials are sponge Ti, Al powder, Cr powder, AlV and AlNb particles (granular 325 mesh). The proportion of ingredients is selected according to the parameters of the composition part. The final proportion obtained is shown in Table 1. The experiment uses a vertical centrifugal vacuum induction melting and casting furnace for casting. The vacuum in the furnace is maintained at about 0.5Pa and then protected by Ar gas. After repeated three times, the vacuum is maintained at about 0.08Pa, and the pressure relief rate is <0.1Pa / mm. After melting and casting, put the ingot upside down and cast it again, repeat three times to make the ingot element distribution evenly, and take points to check the composition distribution. The ingots that meet the requirements are used as master ingots for directional soli...

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Abstract

The invention discloses an alloy design method for reducing directionally-solidified titanium aluminum alloy casting member and casting mold coating interface reaction, and belongs to a method for improving titanium aluminum alloy casting quality. The specific steps are as follows: designing TiAl alloys with different Nb contents for directional solidification process to obtain casting members; and using a microhardness tester to test Vickers microhardness to determine interface reaction layer thickness. A German brooke Quantax400-10 energy dispersive spectrometer is used for sample interface element distribution analysis, a German Brook D8AdanceX ray diffractometer is used for sample surface phase analysis, and a United States FEIQuanta TM250 scanning electron microscope is used for casting memberreaction layer and casting member matrix tissue morphology observation and analysis. Through corresponding analysis and test of the directionally-solidified titanium aluminum alloy casting members obtained by the alloy design, interfacial reaction degree can be obtained specifically and vividly, corresponding titanium aluminum alloy casting member quality can be well evaluated, and a TiAl alloy casting member with optimized Nb content can be obtained.

Description

Technical field [0001] This design studies an alloy design method that reduces the interface reaction between the directionally solidified titanium aluminum alloy castings and the mold coating, which is a method to improve the casting quality of titanium aluminum alloy. Background technique [0002] TiAl alloy has low density, high specific strength, high specific stiffness, good heat resistance, high temperature creep resistance and oxidation resistance. It is a lightweight superalloy with the best comprehensive performance, and is a super-high-speed aircraft and the next generation The material of choice for advanced aero-engines has therefore become the focus of research in lightweight alloys. [0003] At present, most TiAl-based alloys are produced by powder metallurgy technology, casting and ingot metallurgy technology. TiAl is a brittle intermetallic compound. The biggest obstacle to the practical use of TiAl alloys is the room temperature brittleness and difficult deformab...

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C30B29/52C30B11/00
CPCC30B29/52C30B11/006
Inventor 隋艳伟冯坤程成戚继球何业增委福祥孟庆坤孙智
Owner CHINA UNIV OF MINING & TECH
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