Capacitor
A technology for capacitors and electrodes, which is applied in the field of capacitors and can solve problems such as the difficulty in forming conductive polymer layers uniformly
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Embodiment 1
[0018] Put 5,000 grams of potassium fluoroniobate fully vacuum-dried at 80°C and sodium whose molar mass is 10 times that of potassium fluoroniobate into a nickel crucible, and make it undergo a reduction reaction at 1,000°C for 20 hours under an argon atmosphere . After the reaction was complete, the reduced product was cooled, washed successively with water, 95% sulfuric acid, and then water, dried in vacuum and pulverized for 40 hours using an alumina jar ball mill containing silica alumina balls. The pulverized product was immersed and stirred in a 3:2 (by mass) mixed solution of 50% nitric acid and 10% aqueous hydrogen peroxide solution. Then, the pulverized product was sufficiently washed with water until the pH value reached 7 to remove impurities, and then vacuum-dried. The average particle size of the raw niobium powder was 1.2 microns.
[0019] In a niobium tank, 500 g of this raw niobium powder was placed and 50 g of polybutylmethacrylate and 1 liter of toluene we...
Embodiment 2
[0024] Embodiment 2: the preparation of formula I compound crystal
[0025] 106 g of benzaldehyde, 400 g of o-fluoroaniline, 450 g of hydrochloric acid (about 30%) and 800 ml of water were heated in an autoclave at 120-140° C. for 6 hours. The reaction mixture was poured on 1 kg of ice and 500 g of sodium hydroxide solution (30%). The organic layer was separated and the excess o-fluoroaniline was separated with toluene. The residue was recrystallized from toluene and the filter cake was washed with cold ethanol. The compound of formula I was obtained; yield: 41%. Accurately weigh the above compound with an analytical balance, put the weighed compound into an agate grinding body in a fume hood, grind it thoroughly to mix it evenly, and then put the sample into a platinum crucible. In order to make the post-reaction go smoothly, put it into a box furnace for pre-calcination and grinding at 90°C. Finally, keep the temperature at 70°C for 5h, and cool slowly to room temperatur...
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