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A titanium alloy part with different microstructure distribution and its preparation method

A technology of microstructure and titanium alloy, applied in the field of titanium alloy parts and their preparation, can solve the problems of difficulty in precise control of deformation, difficulty in controlling the distribution of microstructure of parts, and difficulty in forming macroscopic gradient structure, etc., to achieve applicability and flexible, easy-to-implement effects

Active Publication Date: 2022-06-17
HUAZHONG UNIV OF SCI & TECH
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  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Gradient heat treatment generally pretreats the material to a certain extent, and then performs different heat treatment operations on different parts of the material according to performance requirements. During the cooling process, different regions present different microstructures. Gradient heat treatment has extremely high requirements on the structure and process operation of heat treatment equipment. , generally used in the production of titanium alloy parts with symmetrical or regular distribution of microstructure; deformation heat treatment is the combination of deformation and heat treatment, that is, a certain heat treatment is performed on the titanium alloy blank to obtain the same structure (such as a basket structure), and then the blank Different parts are deformed with different deformation amounts, and finally different tissue distributions are obtained. However, it is relatively difficult to accurately control the deformation amount during the deformation process; the main method of thermal hydrogen treatment is gradient hydrogenation. In the past, gradient hydrogenation was usually heated. In the furnace, the billet is heated and hydrogenated as a whole, and finally a certain hydrogen concentration gradient is formed in different parts of the billet. It is generally difficult to control the microstructure distribution of parts at specific positions in gradient heat treatment, and it is difficult to form a macroscopic gradient structure.

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  • A titanium alloy part with different microstructure distribution and its preparation method
  • A titanium alloy part with different microstructure distribution and its preparation method

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preparation example Construction

[0026] see figure 1 and figure 2 , the preparation method of titanium alloy parts with different structure distribution provided by the present invention mainly comprises the following steps:

[0027] In step 1, the titanium alloy billet is placed in a hydrogen treatment furnace, and the furnace is evacuated and then filled with a certain amount of hydrogen; then, the furnace temperature is increased to make the hydrogen have a certain diffusivity.

[0028] Specifically, first, put a piece of surface-treated titanium alloy billet into a thermal hydrogen treatment furnace, and vacuumize the furnace, then fill a certain amount of hydrogen into the furnace, and keep it at a certain temperature, Make hydrogen have a certain diffusivity.

[0029] Wherein, the titanium alloy billet is a near-α-type titanium alloy billet or an α+β-type titanium alloy billet; at low temperature, the diffusion of hydrogen in the titanium alloy billet is mainly controlled by diffusion kinetics, and t...

Embodiment 1

[0042] Selecting a Ti65 slab, the method for preparing titanium alloy parts with different microstructure distributions based on laser-assisted heating provided in Example 1 mainly includes the following steps:

[0043] S1, select a 2mm thick Ti65 slab, clean the surface of the Ti65 slab and put it into a hydrogen furnace, then vacuum the furnace and fill it with a certain amount of hydrogen, and raise the furnace temperature to 400°C. Hydrogen has a certain diffusivity and is in a relatively active state.

[0044]S2, turn on the laser to emit a laser beam to heat the middle area of ​​the titanium alloy slab. When the infrared temperature measuring head detects that the temperature of the laser heating zone plate is 750°C, stop increasing the power of the laser beam and keep the current temperature unchanged for 15 minutes. hydrogenation treatment.

[0045] S3, reduce the heating power of the laser beam until zero, move the laser to repeat the operation process of step S2, an...

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Abstract

The invention belongs to the technical field related to the preparation of structural materials, and discloses a titanium alloy part with different microstructure distribution and a preparation method thereof. The method includes the following steps: (1) after placing the titanium alloy blank in a hydrogen treatment furnace, Vacuumize and fill the hydrogen treatment furnace with hydrogen, and raise the temperature of the furnace; (2) emit a laser beam to locally heat an area of ​​the titanium alloy billet that needs hydrogen, and heat it to a predetermined temperature and maintain it for a predetermined time. The current heated region of the titanium alloy blank is subjected to hydrogenation treatment; (3) gradually reducing the power of the laser beam until zero, and re-emitting the laser beam to heat and hydrogenate other areas of the titanium alloy blank that need to be hydrogenated; (4 ) sequentially carry out isothermal heat treatment and vacuum dehydrogenation on the titanium alloy blank after hydrogenation, and then obtain titanium alloy parts. The invention performs laser-assisted heating and hydrogen placement on the region where hydrogen needs to be placed on the titanium alloy, and can accurately control the distribution of microstructures through laser beams.

Description

technical field [0001] The invention belongs to the technical field related to the preparation of structural materials, and more particularly, relates to a titanium alloy part with different microstructure distributions and a preparation method thereof. Background technique [0002] As a new structural material, titanium alloy has comprehensive properties such as good heat resistance, high specific strength, and excellent corrosion resistance, and is widely used in aerospace, biomedical and other industries. According to the composition of the titanium alloy phase and the types of stable alloying elements, titanium alloys are usually divided into three categories: α-type, β-type and α+β-type titanium alloys. In addition, titanium alloys usually have different microstructures. Generally, the microstructure types of titanium alloys are divided into equiaxed structure, basket structure, dual-state structure and lamellar structure. In engineering research, the diversification of...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C22F1/18C22F1/02C21D3/06C21D1/34
CPCC22F1/183C22F1/02C21D3/06C21D1/34C21D2221/00
Inventor 邓磊田壵王新云金俊松张茂龚攀
Owner HUAZHONG UNIV OF SCI & TECH
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