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Suction combined type electrochemical micro-additive preparation method and device

An electrochemical and combined technology, applied in the field of additive manufacturing, can solve problems affecting dimensional accuracy, unevenness, meniscus instability, etc.

Active Publication Date: 2021-03-19
SUN YAT SEN UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] In the prior art, the meniscus-based electrochemical additive manufacturing technology has the following problems: (1) The meniscus is unstable, and it is easy to break and leak liquid, and the size of the meniscus is not easy to control, which affects the size of the meniscus. precision control
(2) The ions consumed in the meniscus cannot be replenished, and the ion concentration in the meniscus continues to decrease during the printing process, resulting in poor and uneven morphology of the printed product

Method used

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  • Suction combined type electrochemical micro-additive preparation method and device
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  • Suction combined type electrochemical micro-additive preparation method and device

Examples

Experimental program
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Effect test

Embodiment 1

[0039] Example 1 A suction-combined electrochemical micro-additive device

[0040] like figure 1As shown, the suction combined electrochemical micro-additive device includes a sealed electrolytic cell 1, a liquid storage tank 2, a substrate 3, an electrochemical workstation 4, a nozzle, an electrode, a pump and a three-dimensional translation platform 9, and the substrate 3 is fixed on the three-dimensional displacement stage 9, and the electrodes include a reference electrode 10, a counter electrode 11 and a working electrode with the substrate 3 as electrodes arranged in the sealed electrolytic cell 1, the reference electrode 10, the counter electrode 11 and the The working electrodes are all electrically connected to the electrochemical workstation 4 (that is, the reference electrode 10, the counter electrode 11, and the working electrode are electrically connected to the reference electrode clip, the counter electrode clip, and the working electrode clip of the electrochem...

Embodiment 2

[0044] Example 2 A method for preparing a suction-combined electrochemical micro-additive material using DC voltage

[0045] Using the additive device of Example 1, the preparation method of this example specifically includes the following steps:

[0046] (1) Cut the polished copper sheet to a size of 3cm×3cm as the substrate 3, paste it on the glass sheet and place it on the XY plane of the three-dimensional translation stage 9, and connect it to the working electrode clamp of the electrochemical workstation 4.

[0047] (2) Fill 2 / 3 of the electrolyte in the sealed electrolytic cell 1, insert the reference electrode 10, the counter electrode 11, and the inlet and outlet conduit 12 and then tighten the cover to ensure tightness. The reference electrode 10 and the counter electrode 11 are respectively connected to the electrochemical The reference electrode clamp and the counter electrode clamp of the workstation 4 are first connected with the liquid storage tank 2, the No. 1 p...

Embodiment 3

[0052] Example 3 A preparation method of pumping combined electrochemical micro-addition using pulse voltage

[0053] Using the additive device of Example 1, the preparation method of this example specifically includes the following steps:

[0054] (1) Cut the insulated PET plate on which the Cu seed layer with a thickness of 150nm was evaporated to a size of 3cm × 3cm as the substrate 3, paste it on the glass slide and place it on the XY plane of the three-dimensional displacement stage 9, and connect the electrochemical workstation 4 Working electrode clip.

[0055] (2) Fill 2 / 3 of the electrolyte in the sealed electrolytic cell 1, insert the reference electrode 10, the counter electrode 11, and the inlet and outlet conduit 12 and then tighten the cover to ensure tightness. The reference electrode 10 and the counter electrode 11 are respectively connected to the electrochemical The reference electrode clamp and the counter electrode clamp of the workstation 4 are first conn...

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Abstract

The invention belongs to the technical field of additive manufacturing, particularly relates to a suction combined type electrochemical micro-additive preparation method and device, and provides a suction combined type electrochemical micro-additive device. The suction combined type electrochemical micro-additive device comprises a sealed electrolytic tank, a liquid storage tank, a base plate, anelectrochemical workstation, a spray head, an electrode, an infusion pump and a three-dimensional displacement table. The electrochemical micro-additive preparation method is provided on the basis ofthe micro-additive device, and the problems that in the meniscus electrochemical micro-additive manufacturing technology, when a syringe needle moves, the meniscus stability is poor, and liquid overflowing and liquid leakage are likely to happen are solved by introducing the mode of the suction combined type spray head, and therefore, the stability of the meniscus and the printing fluency are improved; and meanwhile, the technology increases the ion flow rate in the meniscus, supplements ions consumed in the printing process, and enables a printed finished product to have a uniform surface, aclear edge and relatively low roughness, thereby improving the printing morphology.

Description

technical field [0001] The invention belongs to the technical field of additive manufacturing, and in particular relates to a suction-combined electrochemical micro-additive preparation method and a device thereof. Background technique [0002] Micro-sized metal parts play an irreplaceable role in communication and other fields. The current mainstream metal additive manufacturing methods have their limitations, such as low forming precision, high production cost, and certain residual stress and thermal deformation in the finished product. Electrochemical additive manufacturing technology is a new type of additive manufacturing technology that can be used to produce micro-nano-sized metal parts, mainly through electroplating (metal ions in the electrolyte are precipitated from the electrolyte through a reduction reaction and deposited on the conductive substrate. Above) for layered processing, and then complete the three-dimensional forming of micro-nano parts. Since the el...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C25D17/00C25D5/08B22F12/00B22F12/53B22F10/10C25D21/18C25D3/38C25D5/18B33Y10/00B33Y30/00B33Y80/00
CPCC25D17/00C25D5/08B22F3/003C25D21/18C25D3/38C25D5/18B33Y10/00B33Y30/00B33Y80/00
Inventor 杨亚斌郭亚文
Owner SUN YAT SEN UNIV
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