Method for making steel container steel slab containing copper by using accurate determination of copper content in nickel-copper alloy
A technology of nickel-copper alloy and copper content, which is applied in the field of metallurgy, can solve the problems of insufficient corrosion resistance and surface quality, achieve good precision, improve the quality of steelmaking billets and the quality of final rolled products, and avoid The effect of fluctuations in copper content
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[0077] EXAMPLES: The method of determining the copper content in the nickel copper alloy in the present invention employs the following specific steps:
[0078] Using dilute nitric acid dissolved samples, ammonia water separation iron interference elements, regulate pH = 5.5 in the filtrate, add excess ethylenediamine tetracetic acid EDTA solution to enable all complexation of the element, then add from thiourea, 1.10-two Nitrogen (neighboria) and ascorbic acid composition of combined masking agent selective decomposition Cu-EDTA complex, and finally the released EDTA released by zinc standard solution is calculated by calculating the content of copper.
[0079] (1) Samples of samples: Weigh 0.5004 g of nickel-copper alloy samples in 200 ml beaker, add 20 mL (1 + 2, 1 parts of concentrated nitric acid + 2 parts water) nitric acid, heating to completely dissolve, remove cooling, and A sample solution was obtained in a 250 ml capacity bottle.
[0080] (2) Interference separation: fr...
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